CN102250514A - Solvent-resistant halogen-free two-component screen printing ink - Google Patents
Solvent-resistant halogen-free two-component screen printing ink Download PDFInfo
- Publication number
- CN102250514A CN102250514A CN2011100218135A CN201110021813A CN102250514A CN 102250514 A CN102250514 A CN 102250514A CN 2011100218135 A CN2011100218135 A CN 2011100218135A CN 201110021813 A CN201110021813 A CN 201110021813A CN 102250514 A CN102250514 A CN 102250514A
- Authority
- CN
- China
- Prior art keywords
- solvent
- screen printing
- halogen
- component
- ink
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000007650 screen-printing Methods 0.000 title claims abstract description 45
- 239000002904 solvent Substances 0.000 title claims abstract description 44
- 229910052736 halogen Inorganic materials 0.000 claims abstract description 42
- 150000002367 halogens Chemical class 0.000 claims abstract description 41
- 229920000728 polyester Polymers 0.000 claims abstract description 35
- 239000007788 liquid Substances 0.000 claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 22
- 230000008719 thickening Effects 0.000 claims description 20
- 239000013530 defoamer Substances 0.000 claims description 19
- 239000006185 dispersion Substances 0.000 claims description 13
- 239000007787 solid Substances 0.000 claims description 12
- 239000012296 anti-solvent Substances 0.000 claims description 9
- 150000002148 esters Chemical class 0.000 claims description 6
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 6
- 239000012948 isocyanate Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 238000009775 high-speed stirring Methods 0.000 claims description 4
- 150000002513 isocyanates Chemical class 0.000 claims description 4
- 239000011347 resin Substances 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 4
- 229910002012 Aerosil® Inorganic materials 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 229920001577 copolymer Polymers 0.000 claims description 3
- 229920001296 polysiloxane Polymers 0.000 claims description 3
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical group COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims description 3
- 229920006395 saturated elastomer Polymers 0.000 claims description 3
- 238000007639 printing Methods 0.000 abstract description 12
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 230000007547 defect Effects 0.000 abstract 1
- 239000002562 thickening agent Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 208000034189 Sclerosis Diseases 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 2
- 239000004417 polycarbonate Substances 0.000 description 2
- -1 polyethylene terephthalate Polymers 0.000 description 2
- 229920000139 polyethylene terephthalate Polymers 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 239000004926 polymethyl methacrylate Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229920000515 polycarbonate Polymers 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Abstract
The invention discloses solvent-resistant halogen-free two-component screen printing ink. The printing ink comprises: by weight, 85 to 98% of polyester liquid, 0.2 to 6% of a defoaming agent, and 0.1 to 10% of a thickening agent. The printing ink overcomes the defects of the existing screen printing ink for a hardened surface. The solvent-resistant halogen-free two-component screen printing ink does not contain halogens, has a solvent-resistant property and contains an appropriate amount of accessory agents thus has excellent use performances, a wide scope of an adhesive force effecting on a hardened surface, and excellent multiple resistance properties.
Description
Technical field
The present invention relates to printing ink, relate in particular to a kind of two component ink for screen printing of anti-solvent of Halogen compliance with environmental protection requirements.
Background technology
Develop rapidly along with electronics and IT products, the surface add as hard as material, as the PC(polycarbonate that hardens), sclerosis PMMA(polymethylmethacrylate sclerosis PET(polyethylene terephthalate)) etc., obtained using widely, and this type of material is also more and more higher with the performance requriements of printing ink, as: Halogen, anti-solvent etc.In traditional complete processing, though employed printing ink sticking power can reach, halogen-containing, and anti-solvent (alcohol, gasoline etc.) performance do not reach standard yet, can not satisfy the demand of product performance.
Therefore, prior art awaits improving and development.
Summary of the invention
In view of above-mentioned the deficiencies in the prior art, the object of the present invention is to provide a kind of pair of component ink for screen printing, it is halogen-containing to be intended to solve existing hardened face ink for screen printing, and the relatively poor problem of solvent resistance.
In order to solve the problems of the technologies described above, technical scheme of the present invention is as follows:
The two component ink for screen printing of a kind of Halogen of anti-the solvent by weight percentage, comprise following component:
Polyester liquid 85-98;
Defoamer 0.2-6;
Thickening material 0.1-10.
The two component ink for screen printing of the described Halogen of anti-the solvent, wherein, by weight percentage, the two component ink for screen printing of the described Halogen of anti-the solvent comprise following component:
Polyester liquid 97;
Defoamer 0.5;
Thickening material 2.5.
The two component ink for screen printing of the described Halogen of anti-the solvent, wherein, described polyester liquid is that solid polyester, esters solvent mix after 1200 rpms rotating speed high-speed stirring gained resin liquid, described polyester liquid solid content is 60%, described solid polyester is a saturated polyester, hydroxyl value is 80 hydroxyl polyester, and described esters solvent is a 1-Methoxy-2-propyl acetate.
The two component ink for screen printing of the described Halogen of anti-the solvent, wherein, described defoamer is a silicone antifoam agent.
The two component ink for screen printing of the described Halogen of anti-the solvent, wherein, described thickening material is an aerosil.
The two component ink for screen printing of the described Halogen of anti-the solvent, wherein, described dispersion agent is the amino acid ester copolymer solution.
The two component ink for screen printing of the described Halogen of anti-the solvent wherein, need to add isocyanate curing agent before the two component ink for screen printing of the described Halogen of anti-the solvent use, and add-on is 10% of an ink by weight.
The two component ink for screen printing of the described Halogen of anti-the solvent, wherein, the viscosity of the two component ink for screen printing of the described Halogen of anti-the solvent is 20000～25000cps under 20 ℃ of room temperatures.
The two component ink for screen printing of a kind of Halogen of anti-the solvent by weight percentage, comprise following component:
Polyester liquid 80-95;
Dispersion agent 0.1-3;
Toner 1-20;
Defoamer 0.1-5;
Thickening material 0.1-6.
The two component ink for screen printing of the described Halogen of anti-the solvent, wherein, by weight percentage, the two component ink for screen printing of the described Halogen of anti-the solvent comprise following component:
Polyester liquid 87.5;
Dispersion agent 0.5;
Toner 10;
Defoamer 0.8;
Thickening material 1.2.
Beneficial effect of the present invention: it has effectively overcome the existing problem of existing hardened face ink for screen printing.Since of the present invention pair of not halogen-containing, the anti-solvent of component ink for screen printing, and, make it to have good use properties owing to contain an amount of auxiliary agent, its sticking power to hardened face is very extensive, and the patience of each side is also quite excellent.
Embodiment
The invention provides the two component ink for screen printing of a kind of Halogen of anti-the solvent, clearer, clear and definite for making purpose of the present invention, technical scheme and effect, below the present invention is described in more detail.Should be appreciated that specific embodiment described herein only in order to explanation the present invention, and be not used in qualification the present invention.
The two component ink for screen printing of a kind of Halogen of anti-the solvent, by weight percentage, this printing ink comprises following component:
Polyester liquid 85-98;
Defoamer 0.2-6;
Thickening material 0.1-10.
The preferable weight percent of the two component ink for screen printing of the present invention's Halogen of anti-the solvent consists of:
Polyester liquid 97;
Defoamer 0.5;
Thickening material 2.5.
The two component ink for screen printing of the present invention's Halogen of anti-the solvent can also add dispersion agent and toner, by weight percentage, are grouped into by following one-tenth:
Polyester liquid 80-95;
Dispersion agent 0.1-3;
Toner 1-20;
Defoamer 0.1-5;
Thickening material 0.1-6.
The optimum weight percentage composition of the two component ink for screen printing of the present invention's Halogen of anti-the solvent is:
Polyester liquid 87.5;
Dispersion agent 0.5;
Toner 10;
Defoamer 0.8;
Thickening material 1.2.
Specifically, described polyester liquid is that solid polyester and esters solvent mix after the resin liquid that 1200 rpms rotating speed high-speed stirring gets.Described polyester is a saturated polyester, and solid resin, hydroxyl value are about 80 hydroxyl polyester.Described esters solvent is a 1-Methoxy-2-propyl acetate.Described polyester liquid solid content is 60%.
Described defoamer is a silicone antifoam agent, and its effect is to reduce the bubble that is produced in manufacturing and the use.
Described thickening material is an aerosil.The effect of thickening material is to improve levelling effect and coating thickness, improves levelling property, brushability, the film forming properties of printing ink, increases the stability of the storage of printing ink.
Described dispersion agent is the amino acid ester copolymer solution, and its effect is that homogeneous disperses those solid particulates that is difficult to be dissolved in liquid, and for example toner also can prevent the sedimentation and the cohesion of solid particulate simultaneously.
The two component ink for screen printing of the present invention's Halogen of anti-the solvent are under 20 ℃ of room temperatures, and its viscosity is 20000～25000cps.Printing ink of the present invention is not halogen-containing, compliance with environmental protection requirements, and excellent to hardened face sticking power, the patience of each side such as anti-solvent is good, is a kind of anti-solvent ink that is applicable to hardened face.
Printing ink of the present invention is the two component printing ink of the Halogen of anti-the solvent, needs to add solidifying agent before using, and could use after mixing.Described isocyanate curing agent is the aliphatic isocyanates solidifying agent, and solid content is absolutely.The following example is that further explanation of the present invention and explanation are not constituted any limitation the present invention.
Embodiment 1
Get 97 parts of polyester liquid (weight), add thickening material 2.5 parts of (weight) and 0.5 part of defoamer (weight), formed mixture gets product after being uniformly dispersed through 1200 rpms rotating speed high-speed stirring 30-40 minute.
Embodiment 2
Get 89 parts of polyester liquid (weight), add 0.5 part of dispersion agent, thickening material 1 part of (weight) and 10 parts of toners (weight), with 600 rpms rotating speed stirring at low speed 15 minutes, cross three-roller six times after stirring, add 0.5 part of defoamer again, 1200 rpms rotating speed stirred 20 minutes then, got product after being uniformly dispersed.
Embodiment 3
Get 87.5 parts of polyester liquid (weight), add 0.5 part of dispersion agent, thickening material 2.5 parts of (weight) and 10 parts of toners (weight), with 600 rpms rotating speed stirring at low speed 15 minutes, cross three-roller six times after stirring, add 0.5 part of defoamer again, 1200 rpms rotating speed stirred 20 minutes then, got product after being uniformly dispersed.
Embodiment 4
Get 86 parts of polyester liquid (weight), add 0.5 part of dispersion agent, thickening material 4 parts of (weight) and 10 parts of toners (weight), with 600 rpms rotating speed stirring at low speed 15 minutes, cross three-roller six times after stirring, add 0.5 part of defoamer again, 1200 rpms rotating speed stirred 20 minutes then, got product after being uniformly dispersed.
The two component ink for screen printing of the above embodiment gained Halogen of anti-the solvent on hardened face printing effect and the physical and chemical index state referring to table 1, wherein the addition of isocyanate curing agent is 10%.
Table 1
| ? | Print stream is parallel | Sticking power | Solvent resistance |
| Embodiment 1 | Excellent | Excellent | Excellent |
| Embodiment 2 | Excellent | Generally | Generally |
| Embodiment 3 | Excellent | Excellent | Excellent |
| Embodiment 4 | Generally | Generally | Generally |
Should be understood that, for those of ordinary skills, can be improved according to the above description or conversion, and all these improvement and conversion all should belong to the protection domain of claims of the present invention.
Claims (10)
1. two component ink for screen printing of the Halogen of anti-the solvent by weight percentage, comprise following component:
Polyester liquid 85-98;
Defoamer 0.2-6;
Thickening material 0.1-10.
2. the two component ink for screen printing of the Halogen of anti-solvent the according to claim 1 is characterized in that, by weight percentage, the two component ink for screen printing of the described Halogen of anti-the solvent comprise following component:
Polyester liquid 97;
Defoamer 0.5;
Thickening material 2.5.
3. require the two component ink for screen printing of the 1 or 2 described Halogens of anti-the solvent according to aforesaid right, it is characterized in that, described polyester liquid is that solid polyester, esters solvent mix after 1200 rpms rotating speed high-speed stirring gained resin liquid, described polyester liquid solid content is 60%, described solid polyester is a saturated polyester, hydroxyl value is 80 hydroxyl polyester, and described esters solvent is a 1-Methoxy-2-propyl acetate.
4. require the two component ink for screen printing of the 1 or 2 described Halogens of anti-the solvent according to aforesaid right, it is characterized in that described defoamer is a silicone antifoam agent.
5. require the two component ink for screen printing of the 1 or 2 described Halogens of anti-the solvent according to aforesaid right, it is characterized in that described thickening material is an aerosil.
6. require the two component ink for screen printing of the 1 or 2 described Halogens of anti-the solvent according to aforesaid right, it is characterized in that described dispersion agent is the amino acid ester copolymer solution.
7. the two component ink for screen printing of the Halogen of anti-solvent the according to claim 1 and 2 is characterized in that, need to add isocyanate curing agent before described pair of component ink for screen printing uses, and add-on is 10% of an ink by weight.
8. require the two component ink for screen printing of the 1 or 2 described Halogens of anti-the solvent according to aforesaid right, it is characterized in that the viscosity of described pair of component ink for screen printing is 20000～25000cps under 20 ℃ of room temperatures.
9. two component ink for screen printing of the Halogen of anti-the solvent by weight percentage, comprise following component:
Polyester liquid 80-95;
Dispersion agent 0.1-3;
Toner 1-20;
Defoamer 0.1-5;
Thickening material 0.1-6.
10. the two component ink for screen printing of the Halogen of anti-solvent the according to claim 9 is characterized in that, by weight percentage, the two component ink for screen printing of the described Halogen of anti-the solvent comprise following component:
Polyester liquid 87.5;
Dispersion agent 0.5;
Toner 10;
Defoamer 0.8;
Thickening material 1.2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110021813.5A CN102250514B (en) | 2011-01-19 | 2011-01-19 | Solvent-resistant halogen-free two-component screen printing ink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110021813.5A CN102250514B (en) | 2011-01-19 | 2011-01-19 | Solvent-resistant halogen-free two-component screen printing ink |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102250514A true CN102250514A (en) | 2011-11-23 |
| CN102250514B CN102250514B (en) | 2014-02-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110021813.5A Expired - Fee Related CN102250514B (en) | 2011-01-19 | 2011-01-19 | Solvent-resistant halogen-free two-component screen printing ink |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102250514B (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103013225A (en) * | 2012-12-25 | 2013-04-03 | 广州慧谷工程材料有限公司 | IML gloss oil and IML printing ink and preparation method and application thereof |
| CN103160226A (en) * | 2011-12-18 | 2013-06-19 | 日东电工（上海松江）有限公司 | Pressure-sensitive adhesive composition, pressure-sensitive printing ink composite and pressure-sensitive adhesive tape made thereof |
| CN103232752A (en) * | 2013-04-25 | 2013-08-07 | 深圳市美丽华油墨涂料有限公司 | Screen printing ink for UV (ultraviolet) paint surface and preparation method thereof |
| CN104371513A (en) * | 2014-10-29 | 2015-02-25 | 陈卫东 | Gloss oil, metal plate painting as well as preparation method and application thereof |
| CN105255257A (en) * | 2015-10-19 | 2016-01-20 | 芜湖春风新材料有限公司 | Thermosetting type glass screen printing ink and preparation method thereof |
| CN106280698A (en) * | 2015-05-27 | 2017-01-04 | 苏州市贝特利高分子材料股份有限公司 | High temperature resistant PI white label ink and preparation method thereof |
| CN107345093A (en) * | 2017-08-16 | 2017-11-14 | 佛山市顺德区莱尔电子材料有限公司 | A kind of and strong Halogen ink of metal adhesive power and preparation method thereof |
| CN108485373A (en) * | 2018-03-05 | 2018-09-04 | 深圳市科美达迈斯科技有限公司 | With nano-silicon dioxide modified high-pressure molding ink on two-component plastic cement |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103160226A (en) * | 2011-12-18 | 2013-06-19 | 日东电工（上海松江）有限公司 | Pressure-sensitive adhesive composition, pressure-sensitive printing ink composite and pressure-sensitive adhesive tape made thereof |
| CN103013225A (en) * | 2012-12-25 | 2013-04-03 | 广州慧谷工程材料有限公司 | IML gloss oil and IML printing ink and preparation method and application thereof |
| CN103013225B (en) * | 2012-12-25 | 2014-12-17 | 广州慧谷工程材料有限公司 | IML gloss oil and IML printing ink and preparation method and application thereof |
| CN103232752A (en) * | 2013-04-25 | 2013-08-07 | 深圳市美丽华油墨涂料有限公司 | Screen printing ink for UV (ultraviolet) paint surface and preparation method thereof |
| CN103232752B (en) * | 2013-04-25 | 2014-10-01 | 深圳市美丽华油墨涂料有限公司 | Screen printing ink for UV (ultraviolet) paint surface and preparation method thereof |
| CN104371513A (en) * | 2014-10-29 | 2015-02-25 | 陈卫东 | Gloss oil, metal plate painting as well as preparation method and application thereof |
| CN106280698A (en) * | 2015-05-27 | 2017-01-04 | 苏州市贝特利高分子材料股份有限公司 | High temperature resistant PI white label ink and preparation method thereof |
| CN105255257A (en) * | 2015-10-19 | 2016-01-20 | 芜湖春风新材料有限公司 | Thermosetting type glass screen printing ink and preparation method thereof |
| CN105255257B (en) * | 2015-10-19 | 2018-04-13 | 芜湖春风新材料有限公司 | A kind of heat curing type glass silk screen printing ink and preparation method thereof |
| CN107345093A (en) * | 2017-08-16 | 2017-11-14 | 佛山市顺德区莱尔电子材料有限公司 | A kind of and strong Halogen ink of metal adhesive power and preparation method thereof |
| CN108485373A (en) * | 2018-03-05 | 2018-09-04 | 深圳市科美达迈斯科技有限公司 | With nano-silicon dioxide modified high-pressure molding ink on two-component plastic cement |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102250514B (en) | 2014-02-26 |
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Owner name: SHENZHEN MEILIHUA INK + COATING CO., LTD. Free format text: FORMER OWNER: YIKE INKS + PAINTS (SHENGZHEN) CO., LTD. Effective date: 20120330 |
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Effective date of registration: 20120330 Address after: 518103, Feng Tong Road 243, Fuyong Town, Shenzhen, Guangdong, Baoan District Applicant after: Shenzhen Meilihua Ink & Coating Co., Ltd. Address before: 518103 Guangdong city of Shenzhen province Baoan District Fuyong Whitehead industrial district Applicant before: Yike Inks & Paints (Shengzhen) Co., Ltd. |
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Address after: 518103, Guangdong, Baoan District, Fuyong Shenzhen street, Fung Tong Avenue and Yonghe Road intersection Patentee after: Shenzhen beautiful Polytron Technologies Inc Address before: 518103, Feng Tong Road 243, Fuyong Town, Shenzhen, Guangdong, Baoan District Patentee before: Shenzhen Meilihua Ink & Coating Co., Ltd. |
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Granted publication date: 20140226 Termination date: 20190119 |