CN102246827A - Compound pesticide - Google Patents
Compound pesticide Download PDFInfo
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- CN102246827A CN102246827A CN2011102329306A CN201110232930A CN102246827A CN 102246827 A CN102246827 A CN 102246827A CN 2011102329306 A CN2011102329306 A CN 2011102329306A CN 201110232930 A CN201110232930 A CN 201110232930A CN 102246827 A CN102246827 A CN 102246827A
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- recompounded pesticide
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- banlangen
- Prior art date
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- 239000000575 pesticide Substances 0.000 title claims abstract description 53
- 150000001875 compounds Chemical class 0.000 title abstract 8
- 229940082880 azadirachta indica flower extract Drugs 0.000 claims description 43
- 239000010231 banlangen Substances 0.000 claims description 41
- 239000003795 chemical substances by application Substances 0.000 claims description 36
- 239000000203 mixture Substances 0.000 claims description 33
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 32
- 239000003960 organic solvent Substances 0.000 claims description 32
- 239000003755 preservative agent Substances 0.000 claims description 32
- 230000002335 preservative effect Effects 0.000 claims description 32
- 239000003381 stabilizer Substances 0.000 claims description 32
- 239000000516 sunscreening agent Substances 0.000 claims description 32
- 239000004094 surface-active agent Substances 0.000 claims description 31
- ALYNCZNDIQEVRV-UHFFFAOYSA-N 4-aminobenzoic acid Chemical compound NC1=CC=C(C(O)=O)C=C1 ALYNCZNDIQEVRV-UHFFFAOYSA-N 0.000 claims description 28
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 24
- 229960004050 aminobenzoic acid Drugs 0.000 claims description 22
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 20
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 18
- 230000003750 conditioning effect Effects 0.000 claims description 18
- 239000002131 composite material Substances 0.000 claims description 15
- 239000002253 acid Substances 0.000 claims description 14
- 239000004359 castor oil Substances 0.000 claims description 14
- 235000019438 castor oil Nutrition 0.000 claims description 14
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 14
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
- 244000046052 Phaseolus vulgaris Species 0.000 claims description 12
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 12
- 238000009472 formulation Methods 0.000 claims description 9
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 8
- 238000005660 chlorination reaction Methods 0.000 claims description 8
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- 235000019198 oils Nutrition 0.000 claims description 6
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 6
- 239000008158 vegetable oil Substances 0.000 claims description 6
- FIPWRIJSWJWJAI-UHFFFAOYSA-N Butyl carbitol 6-propylpiperonyl ether Chemical compound C1=C(CCC)C(COCCOCCOCCCC)=CC2=C1OCO2 FIPWRIJSWJWJAI-UHFFFAOYSA-N 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 239000003610 charcoal Substances 0.000 claims description 4
- 239000013530 defoamer Substances 0.000 claims description 4
- 229960005235 piperonyl butoxide Drugs 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 239000008267 milk Substances 0.000 claims description 2
- 210000004080 milk Anatomy 0.000 claims description 2
- 235000013336 milk Nutrition 0.000 claims description 2
- 125000005375 organosiloxane group Chemical group 0.000 claims description 2
- 229920000570 polyether Polymers 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000003995 emulsifying agent Substances 0.000 claims 1
- 239000003814 drug Substances 0.000 abstract description 9
- 229940079593 drug Drugs 0.000 abstract description 7
- 240000005343 Azadirachta indica Species 0.000 abstract description 5
- 235000013500 Melia azadirachta Nutrition 0.000 abstract description 5
- 239000004480 active ingredient Substances 0.000 abstract description 4
- 238000002474 experimental method Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000000853 biopesticidal effect Effects 0.000 abstract description 2
- 239000000284 extract Substances 0.000 abstract 4
- 238000013329 compounding Methods 0.000 abstract 2
- 206010059866 Drug resistance Diseases 0.000 abstract 1
- 241000607479 Yersinia pestis Species 0.000 abstract 1
- 230000000361 pesticidal effect Effects 0.000 abstract 1
- 230000003285 pharmacodynamic effect Effects 0.000 abstract 1
- 239000012752 auxiliary agent Substances 0.000 description 15
- 238000000034 method Methods 0.000 description 9
- 239000004495 emulsifiable concentrate Substances 0.000 description 6
- 239000000839 emulsion Substances 0.000 description 6
- 239000002917 insecticide Substances 0.000 description 6
- 241000238631 Hexapoda Species 0.000 description 4
- 150000002170 ethers Chemical class 0.000 description 4
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 4
- 229920000053 polysorbate 80 Polymers 0.000 description 4
- 230000036039 immunity Effects 0.000 description 3
- 241001124076 Aphididae Species 0.000 description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 2
- ZSBXGIUJOOQZMP-UHFFFAOYSA-N Isomatrine Natural products C1CCC2CN3C(=O)CCCC3C3C2N1CCC3 ZSBXGIUJOOQZMP-UHFFFAOYSA-N 0.000 description 2
- 241000409991 Mythimna separata Species 0.000 description 2
- 229920001213 Polysorbate 20 Polymers 0.000 description 2
- 241001145009 Sophora alopecuroides Species 0.000 description 2
- NWGKJDSIEKMTRX-MDZDMXLPSA-N Sorbitan oleate Chemical group CCCCCCCC\C=C\CCCCCCCC(=O)OCC(O)C1OCC(O)C1O NWGKJDSIEKMTRX-MDZDMXLPSA-N 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 229930014456 matrine Natural products 0.000 description 2
- -1 matrine compound Chemical class 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- 239000003495 polar organic solvent Substances 0.000 description 2
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 description 2
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 2
- 239000000600 sorbitol Substances 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 description 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 240000000233 Melia azedarach Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000246044 Sophora flavescens Species 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002481 ethanol extraction Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000003808 methanol extraction Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- NHOIBRJOQAYBJT-IMGVWCFESA-N nimbin Chemical compound C=1([C@@H]2C[C@H]3O[C@H]4[C@](C3=C2C)(C)[C@@H]([C@]2(C(=O)C=C[C@](C)([C@@H]2[C@H]4OC(C)=O)C(=O)OC)C)CC(=O)OC)C=COC=1 NHOIBRJOQAYBJT-IMGVWCFESA-N 0.000 description 1
- ZQIYJHBQRBBBRZ-UHFFFAOYSA-N nimbin Natural products COC(=O)CC1C2C(C(OC(=O)C)C3OC4CC(C(=C4C13C)C)c5cocc5)C(C)(C=CC2=O)C(=O)OC ZQIYJHBQRBBBRZ-UHFFFAOYSA-N 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a compound pesticide, in particular to a pesticide prepared by compounding azadirachta indica extracts and total matrines, belonging to the technical field of biopesticide preparation. The compound pesticide is characterized in that the compound pesticide is prepared by compounding the active ingredients such as azadirachta indica extracts and total matrines, wherein the mass ratio of the azadirachta indica extracts to the total matrines is (1-10):(0.01-1). The compound pesticide has the following beneficial effects: the compound pesticide is prepared by using the azadirachta indica extracts and total matrines as the active ingredients and then adding certain amount of auxiliaries; the compound pesticide is not a chemical drug, thus being environmentally-friendly; the pharmacodynamics experiments prove that the compound pesticide has good pesticidal effect; and because the active ingredients of the drug belong to the natural drugs, the pests are not easy to have drug resistance.
Description
Technical field
The present invention relates to a kind of Recompounded pesticide, relate in particular to the composite insecticide of a kind of neem extract and Banlangen.Belong to the biopesticide preparing technical field.
Background technology
Because the human long-term single type insecticide that relies on, insect is easy to generate pesticide resistance, cause the consumption of chemical insecticide sharply increase as, not only increase the weight of peasant's financial burden, and can cause environment and pollution of agricultural products, have a large amount of compounded pesticides in the market, but great majority are big to people and animals' harmfulness for being mixed between the chemical pesticide, easily cause pollution, and after long-time the use, insect can develop immunity to drugs to them.
Summary of the invention
The objective of the invention is provides a kind of Recompounded pesticide for solving the problems of the technologies described above, and this Recompounded pesticide has desinsection and tires high and free from environmental pollution being not easy is the advantage that insect develops immunity to drugs.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
To be that effective component is composite by neem extract and Banlangen form for a kind of Recompounded pesticide, this Recompounded pesticide, and wherein the mass ratio of neem extract and Banlangen is (1～10) ︰ (0.01～1).
Preferred as technique scheme, neem extract content is 1～10wt% in this Recompounded pesticide, and Banlangen content is 0.01～1wt%, and the formulation of this Recompounded pesticide is the missible oil formulation.
Further preferred as technique scheme, it also contains surfactant 5～10wt%, sun-screening agent 1.2～2.5wt%, stabilizing agent 1.0～3.0wt%, preservative 1.0～1.2wt%, synergist content are 0.5～3.0wt%, pH regulator agent 0.1～0.2wt%, surplus is an organic solvent.
Further preferred again as technique scheme, sun-screening agent is selected from any one or two kinds of mixture in p-aminobenzoic acid, the castor oil; Stabilizing agent is selected from epoxidized vegetable oil, 2, any one or two kinds of mixture among the 6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from any one or more the mixture in charcoal, active carbon, the aminobenzoic acid; Synergist is selected from any one or more the mixture in dregs of beans, chlorination fat, the Butacide; PH value conditioning agent is selected from any one or more the mixture in sodium hydroxide, potassium hydroxide, the hydrochloric acid; Organic solvent is selected from any one or more the mixture in methyl alcohol, ethanol, the acetone.
Further preferred again as technique scheme, neem extract content is 10wt% in this Recompounded pesticide, Banlangen content is 0.03wt%.
Another kind as technique scheme is preferred, and neem extract content is 1～10wt% in this Recompounded pesticide, and Banlangen content is 0.01～1wt%, and the formulation of this Recompounded pesticide is the water and milk formulation.
Further preferred as technique scheme, described Recompounded pesticide oil phase part is divided into neem extract, Banlangen, antifreezing agent, defoamer and organic solvent; Aqueous portion is sun-screening agent, stabilizing agent, preservative, synergist, synergist, pH value conditioning agent.
Further preferred again as technique scheme, surfactant is selected from nonionic class surfactant; The aqueous portion sun-screening agent is selected from any one or two kinds of mixture in p-aminobenzoic acid, the castor oil, stabilizing agent is selected from epoxidized vegetable oil, 2, any one or two kinds of mixture among the 6-di-t-butyl Pyrogentisinic Acid, preservative is selected from any one or more the mixture in charcoal, active carbon, the aminobenzoic acid, synergist is selected from any one or more the mixture in dregs of beans, chlorination fat, the Butacide, and pH value conditioning agent is selected from any one or more the mixture in sodium hydroxide, potassium hydroxide, the hydrochloric acid; Oil phase part organic solvent is selected from any one or more the mixture in methyl alcohol, ethanol, ethyl acetate, the solvent naphtha, and antifreezing agent is selected from one or more in ethylene glycol, the glycerine, and defoamer is selected from organosiloxane, polyethers etc.
In the technique scheme of the present invention, neem extract is that the kind benevolence of seal chinaberry (Azadirachta indica) is pulverized, after one or more degreasings in weakly polar organic solvent such as benzinum, n-hexane or the cyclohexane, refining forming behind polar organic solvent such as ethanol or methanol extraction again, wherein nimbin content is about 0.1～5wt%.
In the technique scheme of the present invention, Banlangen is to extract the alkaloids substance that obtains from Sophora alopecuroide (SopHora alopecuroide) or kuh-seng (SopHora flavescens).
The present invention has following beneficial effect:
The present invention utilizes neem extract and Banlangen as effective component, adds that a certain amount of auxiliary agent is prepared from again.Owing to be medicine non-chemically, so environmental protection; Confirm that through effect experiment it has good insecticidal action; Because the effective component of this medicine is to belong to natural drug, so insect is difficult to develop immunity to drugs.
Embodiment
This specific embodiment only is an explanation of the invention; it is not a limitation of the present invention; those skilled in the art can make the modification that does not have creative contribution to present embodiment as required after reading this specification, but as long as all are subjected to the protection of Patent Law in claim scope of the present invention.
Embodiment one
A kind of Recompounded pesticide, it is to be the composite emulsifiable concentrate that forms of effective component by neem extract and Banlangen.It also contains multiple auxiliary agent, is specially surfactant 5wt%, sun-screening agent 1.2wt%, and stabilizing agent 1.0wt%, preservative 1.0wt%, synergist content are 0.5wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 1wt%, and Banlangen content is 0.01wt%.Described surfactant is selected from the sorbitol in the polyethenoxy ether class of nonionic; Sun-screening agent is selected from p-aminobenzoic acid; Stabilizing agent is selected from epoxidized vegetable oil; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from sodium hydroxide; Organic solvent is selected from ethanol.
Embodiment two
A kind of Recompounded pesticide, it is to be the composite emulsifiable concentrate that forms of effective component by neem extract and Banlangen.It also contains multiple auxiliary agent, is specially surfactant 6wt%, sun-screening agent 1.4wt%, and stabilizing agent 1.2wt%, preservative 1.0wt%, synergist content are 0.6wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 2wt%, and Banlangen content is 0.02wt%.Described surfactant is selected from the Tween-20 of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from chlorination fat; PH value conditioning agent is selected from sodium hydroxide; Organic solvent is selected from ethanol.
Embodiment three
A kind of Recompounded pesticide, it is to be the composite emulsifiable concentrate that forms of effective component by neem extract and Banlangen.It also contains multiple auxiliary agent, is specially surfactant 7wt%, sun-screening agent 1.8wt%, and stabilizing agent 1.6wt%, preservative 1.0wt%, synergist content are 1.0wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 5wt%, and Banlangen content is 0.02wt%.Described surfactant is selected from the Tween-80 of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from chlorination fat; PH value conditioning agent is selected from potassium hydroxide; Organic solvent is selected from acetone.
Embodiment four
A kind of Recompounded pesticide, it is to be the composite emulsifiable concentrate that forms of effective component by neem extract and Banlangen.It also contains multiple auxiliary agent, is specially surfactant 8wt%, sun-screening agent 2.0wt%, and stabilizing agent 2.0wt%, preservative 1.0wt%, synergist content are 2.0wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 8wt%, and Banlangen content is 0.05wt%.Described surfactant is selected from the Tween-80 of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from hydrochloric acid; Organic solvent is selected from ethanol.
Embodiment five
A kind of Recompounded pesticide, it is to be the composite emulsifiable concentrate that forms of effective component by neem extract and Banlangen.It also contains multiple auxiliary agent, is specially surfactant 10wt%, sun-screening agent 2.0wt%, and stabilizing agent 2.0wt%, preservative 1.0wt%, synergist content are 2.0wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 10wt%, and Banlangen content is 0.03wt%.Described surfactant is a sorbester p17; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from hydrochloric acid; Organic solvent is selected from ethanol.
Embodiment six
A kind of Recompounded pesticide, it is to be the composite emulsifiable concentrate that forms of effective component by neem extract and Banlangen.It also contains multiple auxiliary agent, is specially surfactant 10wt%, sun-screening agent 2.5wt%, and stabilizing agent 3.0wt%, preservative 1.2wt%, synergist content are 3.0wt%, pH regulator agent 0.2wt%, surplus is an organic solvent.Wherein neem extract content is 10wt%, and Banlangen content is 0.1wt%.Described surfactant is selected from the TritonX X100 of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from hydrochloric acid; Organic solvent is selected from ethanol.
Embodiment seven
A kind of Recompounded pesticide, it is to be the composite aqueous emulsion that forms of effective component by neem extract and Banlangen.Aqueous portion is selected from surfactant, and its multiple auxiliary agent is specially surfactant 5wt%, sun-screening agent 1.2wt%, and stabilizing agent 1.0wt%, preservative 1.0wt%, synergist content are 0.5wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 1wt%, and Banlangen content is 0.01wt%.Described surfactant is selected from the sorbitol in the polyethenoxy ether class of nonionic; Sun-screening agent is selected from p-aminobenzoic acid; Stabilizing agent is selected from epoxidized vegetable oil; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from sodium hydroxide; Organic solvent is selected from ethanol.
Embodiment eight
A kind of Recompounded pesticide, it is to be the composite aqueous emulsion that forms of effective component by neem extract and Banlangen.Its multiple auxiliary agent is specially surfactant 6wt%, sun-screening agent 1.4wt%, and stabilizing agent 1.2wt%, preservative 1.0wt%, synergist content are 0.6wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 2wt%, and Banlangen content is 0.02wt%.Described surfactant is selected from the Tween-20 in the polyethenoxy ether class of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from chlorination fat; PH value conditioning agent is selected from sodium hydroxide; Organic solvent is selected from ethanol.
Embodiment nine
A kind of Recompounded pesticide, it is to be the composite aqueous emulsion that forms of effective component by neem extract and Banlangen.Its multiple auxiliary agent is specially surfactant 7wt%, sun-screening agent 1.8wt%, and stabilizing agent 1.6wt%, preservative 1.0wt%, synergist content are 1.0wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 5wt%, and Banlangen content is 0.02wt%.Described surfactant is selected from the Tween-80 in the polyethenoxy ether class of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from chlorination fat; PH value conditioning agent is selected from potassium hydroxide; Organic solvent is selected from acetone.
Embodiment ten
A kind of Recompounded pesticide, it is to be the composite aqueous emulsion that forms of effective component by neem extract and Banlangen.Its multiple auxiliary agent is specially surfactant 8wt%, sun-screening agent 2.0wt%, and stabilizing agent 2.0wt%, preservative 1.0wt%, synergist content are 2.0wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 8wt%, and Banlangen content is 0.05wt%.Described surfactant is selected from the isomery tridecanol of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from hydrochloric acid; Organic solvent is selected from ethanol.
Embodiment 11
A kind of Recompounded pesticide, it is to be the composite aqueous emulsion that forms of effective component by neem extract and Banlangen.Its multiple auxiliary agent is specially surfactant 10wt%, sun-screening agent 2.0wt%, and stabilizing agent 2.0wt%, preservative 1.0wt%, synergist content are 2.0wt%, pH regulator agent 0.1wt%, surplus is an organic solvent.Wherein neem extract content is 10wt%, and Banlangen content is 0.03wt%.Described surfactant is a sorbester p17; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from hydrochloric acid; Organic solvent is selected from ethanol.
Embodiment 12
A kind of Recompounded pesticide, it is to be the composite aqueous emulsion that forms of effective component by neem extract and Banlangen.Its multiple auxiliary agent is specially surfactant 10wt%, sun-screening agent 2.5wt%, and stabilizing agent 3.0wt%, preservative 1.2wt%, synergist content are 3.0wt%, pH regulator agent 0.2wt%, surplus is an organic solvent.Wherein neem extract content is 10wt%, and Banlangen content is 0.1wt%.Described surfactant is selected from the Tween-80 of nonionic; Sun-screening agent is selected from castor oil; Stabilizing agent is selected from 2,6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from aminobenzoic acid; Synergist is selected from dregs of beans; PH value conditioning agent is selected from hydrochloric acid; Organic solvent is selected from ethanol.
The inventor has carried out the Toxicity Determination examination with the neem extract of different content allocation plan and Banlangen and other auxiliary agent to the oriental armyworm larva, and the result is as shown in the table
Neem extract and matrine compound kill the mythimna separata experiment
The inventor has carried out the Toxicity Determination examination with the neem extract of different content allocation plan and Banlangen and other auxiliary agent to aphid, and the result is as shown in the table
Neem extract and the experiment of matrine compound killing aphids
Need to prove that the inventor uses after 10 times of this Recompounded pesticide dilutions when carrying out the test of pesticide effectiveness.Such as when desinsection is carried out in an experimental field, the concentration of insecticidal effect and insecticide must not concern, with the formulation relation of insecticide neither be very big, and relevant with the total amount of the insecticide that sprays, close with the proportion relation of active ingredient.And consider for peasant's use habit and safety in utilization and bottled effective dose, usually be to use after 10 times of the dilutions, but use of the present invention is not limited thereto.
Claims (8)
1. Recompounded pesticide is characterized in that: to be that effective component is composite by neem extract and Banlangen form this Recompounded pesticide, and wherein the mass ratio of neem extract and Banlangen is (1～10) ︰ (0.01～1).
2. a kind of Recompounded pesticide according to claim 1 is characterized in that: neem extract content is 1～10wt% in this Recompounded pesticide, and Banlangen content is 0.01～1wt%, and the formulation of this Recompounded pesticide is the missible oil formulation.
3. a kind of Recompounded pesticide according to claim 2, it is characterized in that: it also contains surfactant 5～10wt%, sun-screening agent 1.2～2.5wt%, stabilizing agent 1.0～3.0wt%, preservative 1.0～1.2wt%, synergist content is 0.5～3.0wt%, pH regulator agent 0.1～0.2wt%, and surplus is an organic solvent.
4. a kind of Recompounded pesticide according to claim 3 is characterized in that: sun-screening agent is selected from any one or two kinds of mixture in p-aminobenzoic acid, the castor oil; Stabilizing agent is selected from epoxidized vegetable oil, 2, any one or two kinds of mixture among the 6-di-t-butyl Pyrogentisinic Acid; Preservative is selected from any one or more the mixture in charcoal, active carbon, the aminobenzoic acid; Synergist is selected from any one or more the mixture in dregs of beans, chlorination fat, the Butacide; PH value conditioning agent is selected from any one or more the mixture in sodium hydroxide, potassium hydroxide, the hydrochloric acid; Organic solvent is selected from any one or more the mixture in methyl alcohol, ethanol, the acetone.
5. a kind of Recompounded pesticide according to claim 3 is characterized in that: neem extract content is 10wt% in this Recompounded pesticide, and Banlangen content is 0.03wt%.
6. a kind of Recompounded pesticide according to claim 1 is characterized in that: neem extract content is 1～10wt% in this Recompounded pesticide, and Banlangen content is 0.01～1wt%, and the formulation of this Recompounded pesticide is the water and milk formulation.
7. a kind of Recompounded pesticide according to claim 6 is characterized in that: described Recompounded pesticide oil phase part is divided into neem extract, Banlangen, emulsifier, antifreezing agent, defoamer and organic solvent; Aqueous portion is sun-screening agent, stabilizing agent, preservative, synergist, pH value conditioning agent.
8. a kind of Recompounded pesticide according to claim 7 is characterized in that: surfactant is selected from nonionic class surfactant; The aqueous portion sun-screening agent is selected from any one or two kinds of mixture in p-aminobenzoic acid, the castor oil, stabilizing agent is selected from epoxidized vegetable oil, 2, any one or two kinds of mixture among the 6-di-t-butyl Pyrogentisinic Acid, preservative is selected from any one or more the mixture in charcoal, active carbon, the aminobenzoic acid, synergist is selected from any one or more the mixture in dregs of beans, chlorination fat, the Butacide, and pH value conditioning agent is selected from any one or more the mixture in sodium hydroxide, potassium hydroxide, the hydrochloric acid; Oil phase part organic solvent is selected from any one or more the mixture in methyl alcohol, ethanol, ethyl acetate, the solvent naphtha, and antifreezing agent is selected from one or more in ethylene glycol, the glycerine, and defoamer is selected from organosiloxane, polyethers etc.
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| CN201110232930.6A CN102246827B (en) | 2011-08-15 | 2011-08-15 | Compound pesticide |
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| CN102246827B CN102246827B (en) | 2014-06-25 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016008039A1 (en) * | 2014-07-14 | 2016-01-21 | Novicol International Holding Inc. | Microbicidal composition comprising an octoxynol and a quinolizidine alkaloid compound or a source thereof |
| CN106363734A (en) * | 2016-11-16 | 2017-02-01 | 徐州得铸生物科技有限公司 | Wood preservative containing compound AinsliadimerA |
| CN106577705A (en) * | 2016-11-22 | 2017-04-26 | 恒大园林集团有限公司 | Compounded ecological pesticide and preparing method thereof |
| CN106614777A (en) * | 2016-12-19 | 2017-05-10 | 重庆医学检验试剂研究所 | Composition and application thereof in preventing and treating diseases in grafted citrus branches |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1296753A (en) * | 2000-09-30 | 2001-05-30 | 苗振东 | Plant insecticide and its preparing process |
| CN1568145A (en) * | 2001-10-10 | 2005-01-19 | Sk化学株式会社 | Pesticide formulation composed of natural components |
| CN1706248A (en) * | 2004-07-26 | 2005-12-14 | 袁贞国 | Synergistic botanical orange terpene pesticide |
-
2011
- 2011-08-15 CN CN201110232930.6A patent/CN102246827B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1296753A (en) * | 2000-09-30 | 2001-05-30 | 苗振东 | Plant insecticide and its preparing process |
| CN1568145A (en) * | 2001-10-10 | 2005-01-19 | Sk化学株式会社 | Pesticide formulation composed of natural components |
| CN1706248A (en) * | 2004-07-26 | 2005-12-14 | 袁贞国 | Synergistic botanical orange terpene pesticide |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016008039A1 (en) * | 2014-07-14 | 2016-01-21 | Novicol International Holding Inc. | Microbicidal composition comprising an octoxynol and a quinolizidine alkaloid compound or a source thereof |
| US9884049B2 (en) | 2014-07-14 | 2018-02-06 | Orion Biotechnology Canada Ltd. | Microbicidal composition comprising an octoxynol and a quinolizidine alkaloid compound or a source thereof |
| CN106363734A (en) * | 2016-11-16 | 2017-02-01 | 徐州得铸生物科技有限公司 | Wood preservative containing compound AinsliadimerA |
| CN106577705A (en) * | 2016-11-22 | 2017-04-26 | 恒大园林集团有限公司 | Compounded ecological pesticide and preparing method thereof |
| CN106614777A (en) * | 2016-12-19 | 2017-05-10 | 重庆医学检验试剂研究所 | Composition and application thereof in preventing and treating diseases in grafted citrus branches |
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| Publication number | Publication date |
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| CN102246827B (en) | 2014-06-25 |
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