CN102174355B - Concentrated fragrance type distilled spirit pit mud pit-maintaining liquid, production method thereof and concentrated fragrance type distilled spirit pit mud maintenance method - Google Patents
Concentrated fragrance type distilled spirit pit mud pit-maintaining liquid, production method thereof and concentrated fragrance type distilled spirit pit mud maintenance method Download PDFInfo
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- CN102174355B CN102174355B CN201110046046A CN201110046046A CN102174355B CN 102174355 B CN102174355 B CN 102174355B CN 201110046046 A CN201110046046 A CN 201110046046A CN 201110046046 A CN201110046046 A CN 201110046046A CN 102174355 B CN102174355 B CN 102174355B
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Abstract
The invention relates to concentrated fragrance type distilled spirit pit mud pit-maintaining liquid, a production method thereof and a concentrated fragrance type distilled spirit pit mud maintenance method, and belongs to the technical field of distilled spirit making. The production method of the concentrated fragrance type distilled spirit pit mud pit-maintaining liquid comprises the following steps of: a, uniformly mixing 25 to 40 parts of yellow water, 40 to 50 parts of tail water and 10 to 20 parts of squeezed liquor by weight to obtain mixed solution, wherein the squeezed liquor is liquid obtained by dehydration squeezing after wine lees are steamed; b, adding a high-temperature starter which accounts for 4 to 6 percent of the weight of the mixed solution and concentrated fragrance type distilled spirit pit-closing mud or pit mud which accounts for 3 to 5 percent of the weight of the mixed solution into the mixed solution, and uniformly mixing; c, fermenting at 25 to 35 DEG C for 3 to 7 days in an airtight way; and d, ending the fermentation, filtering to obtain the concentrated fragrance type distilled spirit pit mud pit-maintaining liquid.
Description
Technical field
The present invention relates to aromatic Chinese spirit cellar for storing things mud and support cellar for storing things liquid and working method and the mud maintenance process of aromatic Chinese spirit cellar for storing things, belong to brewing technical field.
Background technology
In the Production of Luzhou-flavor Liquor, in order to keep and to improve constantly microbic activity in the mud of cellar for storing things, need to add nutritive medium to promote the microbial growth breeding in the mud of cellar for storing things, this nutritive medium is commonly called as to supporting cellar for storing things liquid.Support cellar for storing things liquid cellar for storing things mud is carried out maintenance, one is that cellar for storing things mud has replenished moisture; Two is that cellar for storing things mud provides abundanter microorganism species; Three for cellar for storing things mud provides a large amount of organic acids, ester material, for cellar for storing things mud functional microorganism provides nutrition, makes cellar for storing things earth earth form good soil aggregate, is beneficial to the good growth and breeding of soil microorganisms, makes cellar for storing things earth soil luck sexual development.
At present, most of liquor-making enterprises mainly adopt by product yellow water or tail water in the liquor production to support the cellar for storing things.Yellow water is to ooze formation under the redundant moisture in the fermenting process, contains a large amount of acids and the fragrance matter in the liquor such as alcohols and Ester in the yellow water, also contains a large amount of remaining starch and remaining glucide.Tail water is meant that stream wine finishes the liquid that the back forms, and its alcoholic strength is lower than 5%vol, wherein content lot of organic acids class material, and a large amount of high boiling point Esters.But no matter be to adopt yellow water to support the cellar for storing things, still adopt tail water to support the cellar for storing things, all have certain defective.Adopt yellow water to support the cellar for storing things, because the pH value of yellow water is low, acidity is high, is unfavorable for life-time service, and life-time service can have a negative impact to cellar for storing things mud functional microorganism.Adopt tail water to support the cellar for storing things, organic content also can have a negative impact to cellar for storing things mud functional microorganism not as yellow water in the tail water.
Summary of the invention
First technical problem to be solved by this invention provides a kind of method that aromatic Chinese spirit cellar for storing things mud is supported cellar for storing things liquid of producing, and the foster cellar for storing things liquid that this method is produced can improve cellar for storing things shale amount.
The method that the present invention produces the foster cellar for storing things of mud, aromatic Chinese spirit cellar for storing things liquid comprises the steps:
A, by weight ratio with 25～40 parts of yellow waters, 40～50 parts of tail water, 10～20 parts of mixings of pressed liquor, obtain mixed solution; Wherein, described pressed liquor is that vinasse steam after drinking, and the resulting liquid of extruding dewaters;
(the bent medicine of high temperature refers to that leavening temperature is controlled at the bent medicine of making about 60 degree to the bent medicine of high temperature of adding mixed solution weight 4～6% in b, the mixed solution; Adopt conventional commercially available Production of Luzhou-flavor Liquor get final product with the bent medicine of high temperature) with the aromatic Chinese spirit of mixed solution weight 3～5% with pit sealing mud or store mud (owing to storing the mud resource-constrained; Could form decades; It is non-renewable to destroy the back, preferably uses pit sealing mud), mixing;
C, in 25～35 ℃ of sealed fermentings 3～7 days;
(filtration can be removed a large amount of remaining vinasse, Mierocrystalline cellulose, lignin material, has avoided the influence to cellar for storing things mud of Mierocrystalline cellulose and lignin material) filtered in d, end fermentation, obtains the foster cellar for storing things of mud, aromatic Chinese spirit cellar for storing things liquid.
In the inventive method, yellow water can provide a large amount of acids and the fragrance matter in the liquor such as alcohols and Ester, also contains a large amount of remaining starch and remaining glucide; Tail water can provide content lot of organic acids class material, and a large amount of high boiling point Esters; Pressed liquor can provide lot of organic acids class material, also has protein, starch, glucide; Pit sealing mud can provide a large amount of cellar for storing things mud functional microorganism such as caproic acid mushroom.Starch, carbohydrate, organic acid, ester type organic matter more in the mixed solution provide nutritive substance preferably to pit mud functional bacteria, can promote the cultivation of pit mud functional bacteria.The adding of the bent medicine of high temperature, the one, for supporting cellar for storing things liquid abundant microorganism species is provided, the 2nd, a large amount of utilize starch and the glucide in the mixed solution, change abundant more acid, ester type organic into, to improve the quality of supporting cellar for storing things liquid.
Wherein, consider that the cultivation of pit mud functional bacteria needs and obtain quality to support cellar for storing things liquid preferably, the weight part of the yellow water in the above-mentioned a step, tail water, pressed liquor is respectively 25～40 parts, 40～50 parts, 10～20 parts.Further, in order to obtain the more foster cellar for storing things liquid of good quality, preferred following technical scheme: the yellow water described in a step is that 35 parts, tail water are that 45 parts, pressed liquor are 20 parts.
Further, in order to obtain the more foster cellar for storing things liquid of good quality, the aromatic Chinese spirit that adds in the above-mentioned b step is preferably 4% of mixed solution weight with pit sealing mud or cellar for storing things mud, and the bent medicine of the high temperature of adding is preferably 5% of mixed solution weight.
Wherein, better in order to make ferment effect, to obtain the more foster cellar for storing things of mud, the aromatic Chinese spirit cellar for storing things liquid of good quality, the alcoholic strength that adds in the above-mentioned b step in the mixture after bent medicine of high temperature and aromatic Chinese spirit use pit sealing mud or store mud is 2～6%vol
Wherein, better in order to make ferment effect, above-mentioned c step is preferable over 30 ℃ of sealed fermentings 5 days.
Second technical problem to be solved by this invention provides a kind of aromatic Chinese spirit cellar for storing things mud of being produced by aforesaid method and supports cellar for storing things liquid, and this supports cellar for storing things liquid can improve cellar for storing things shale amount.
The 3rd technical problem to be solved by this invention provides the method for a kind of aromatic Chinese spirit cellar for storing things mud maintenance, and this method can improve cellar for storing things shale amount.
The method of aromatic Chinese spirit of the present invention cellar for storing things mud maintenance is: adopt the above-mentioned aromatic Chinese spirit cellar for storing things mud of claim to support cellar for storing things liquid and make cellar for storing things muddy water divide content maintenance >=50wt%.
The present invention has effectively utilized by product yellow water, wine tail and the vinasse pressed liquor in the liquor production, has improved the utility value of by products such as yellow water, wine tail.Aromatic Chinese spirit of the present invention cellar for storing things mud is supported cellar for storing things liquid and can be improved cellar for storing things shale amount, reduces cellar for storing things mud maintenance cost.The present invention has broad application prospects for the maintenance of aromatic Chinese spirit cellar for storing things mud provides a kind of new selection.
Embodiment
The method that the present invention produces the foster cellar for storing things of mud, aromatic Chinese spirit cellar for storing things liquid comprises the steps:
A, by weight ratio with 25～40 parts of yellow waters, 40～50 parts of tail water, 10～20 parts of mixings of pressed liquor, obtain mixed solution; Wherein, described pressed liquor is that vinasse steam after drinking, and the resulting liquid of extruding dewaters;
(the bent medicine of high temperature refers to that leavening temperature is controlled at the bent medicine of making about 60 degree to the bent medicine of high temperature of adding mixed solution weight 4～6% in b, the mixed solution; Adopt conventional commercially available Production of Luzhou-flavor Liquor get final product with the bent medicine of high temperature) with the aromatic Chinese spirit of mixed solution weight 3～5% with pit sealing mud or store mud (owing to storing the mud resource-constrained; Could form decades; It is non-renewable to destroy the back, preferably uses pit sealing mud), mixing;
C, in 25～35 ℃ of sealed fermentings 3～7 days;
(filtration can be removed a large amount of remaining vinasse, Mierocrystalline cellulose, lignin material, has avoided the influence to cellar for storing things mud of Mierocrystalline cellulose and lignin material) filtered in d, end fermentation, obtains the foster cellar for storing things of mud, aromatic Chinese spirit cellar for storing things liquid.
In the inventive method, yellow water can provide a large amount of acids and the fragrance matter in the liquor such as alcohols and Ester, also contains a large amount of remaining starch and remaining glucide, and single yellow water drenches the cellar for storing things suppresses to store the mud mikrobe because of acidity is too high breeding; Tail water can provide content lot of organic acids class material, and a large amount of high boiling point Esters; Pressed liquor can provide lot of organic acids class material, also has protein, starch, glucide; Pit sealing mud can provide a large amount of cellar for storing things mud functional microorganism such as caproic acid mushroom.Starch, carbohydrate, organic acid, ester type organic matter more in the mixed solution provide nutritive substance preferably to pit mud functional bacteria, can promote the cultivation of pit mud functional bacteria.The adding of the bent medicine of high temperature, the one, for supporting cellar for storing things liquid abundant microorganism species is provided, the 2nd, a large amount of utilize starch and the glucide in the mixed solution, change abundant more acid, ester type organic into, to improve the quality of supporting cellar for storing things liquid.
Wherein, consider that the cultivation of pit mud functional bacteria needs and obtain quality to support cellar for storing things liquid preferably, the weight part of the yellow water in the above-mentioned a step, tail water, pressed liquor is respectively 25～40 parts, 40～50 parts, 10～20 parts.Further, in order to obtain the more foster cellar for storing things liquid of good quality, preferred following technical scheme: the yellow water described in a step is that 35 parts, tail water are that 45 parts, pressed liquor are 20 parts.
Further, in order to obtain the more foster cellar for storing things liquid of good quality, the aromatic Chinese spirit that adds in the above-mentioned b step is preferably 4% of mixed solution weight with pit sealing mud or cellar for storing things mud, and the bent medicine of the high temperature of adding is preferably 5% of mixed solution weight.
Wherein, better in order to make ferment effect, to obtain the more foster cellar for storing things of mud, the aromatic Chinese spirit cellar for storing things liquid of good quality, the alcoholic strength that adds in the above-mentioned b step in the mixture after bent medicine of high temperature and aromatic Chinese spirit use pit sealing mud or store mud is 2～6%vol
Wherein, better in order to make ferment effect, above-mentioned c step is preferable over 30 ℃ of sealed fermentings 5 days.
The present invention also provides a kind of aromatic Chinese spirit cellar for storing things mud of being produced by aforesaid method to support cellar for storing things liquid, and this supports cellar for storing things liquid can improve cellar for storing things shale amount.
The present invention also provides the method for a kind of aromatic Chinese spirit cellar for storing things mud maintenance, and this method can improve cellar for storing things shale amount.The method of aromatic Chinese spirit of the present invention cellar for storing things mud maintenance is: adopt the above-mentioned aromatic Chinese spirit cellar for storing things mud of claim to support cellar for storing things liquid and make cellar for storing things muddy water divide content maintenance >=50wt%.
Do further description below in conjunction with the embodiment specific embodiments of the invention, therefore do not limit the present invention among the described scope of embodiments.
Embodiment 1 aromatic Chinese spirit of the present invention cellar for storing things mud is supported the preparation of cellar for storing things liquid
A, with yellow water 250kg, tail water 400kg, pressed liquor 110kg mixing, obtain mixed solution; Wherein, described pressed liquor is that vinasse steam after drinking, and the resulting liquid of extruding dewaters;
The aromatic Chinese spirit that adds mixed solution weight 3% in b, the mixed solution is with the bent medicine of the commercially available high temperature of pit sealing mud and mixed solution weight 5% (the bent medicine of high temperature refers to that leavening temperature is controlled at the bent medicine of making about 60 degree), mixing (alcoholic strength in the mixture is 3%vol);
C, in 26 ℃ of sealed fermentings 7 days;
D, end fermentation are filtered, and obtain the foster liquid of storing of aromatic Chinese spirit cellar for storing things mud.
Embodiment 2 aromatic Chinese spirit of the present invention cellar for storing things mud are supported the preparation of cellar for storing things liquid
A, with yellow water 320kg, tail water 490kg, pressed liquor 200kg mixing, obtain mixed solution; Wherein, described pressed liquor is that vinasse steam after drinking, and the resulting liquid of extruding dewaters;
The aromatic Chinese spirit that adds mixed solution weight 5% in b, the mixed solution is with the bent medicine of the commercially available high temperature of pit sealing mud and mixed solution weight 6% (the bent medicine of high temperature refers to that leavening temperature is controlled at the bent medicine of making about 60 degree), mixing (alcoholic strength in the mixture is 4%vol);
C, in 35 ℃ of sealed fermentings 4 days;
D, end fermentation are filtered, and obtain the foster liquid of storing of aromatic Chinese spirit cellar for storing things mud.
Embodiment 3 aromatic Chinese spirit of the present invention cellar for storing things mud are supported the preparation of cellar for storing things liquid
A, with yellow water 400kg, tail water 490kg, pressed liquor 195kg mixing, obtain mixed solution; Wherein, described pressed liquor is that vinasse steam after drinking, and the resulting liquid of extruding dewaters;
The aromatic Chinese spirit that adds mixed solution weight 4.5% in b, the mixed solution is with the bent medicine of the commercially available high temperature of pit sealing mud and mixed solution weight 6% (the bent medicine of high temperature refers to that leavening temperature is controlled at the bent medicine of making about 60 degree), mixing (alcoholic strength in the mixture is 6%vol);
C, in 30 ℃ of sealed fermentings 5 days;
D, end fermentation are filtered, and obtain the foster liquid of storing of aromatic Chinese spirit cellar for storing things mud.
Embodiment 4 aromatic Chinese spirit of the present invention cellar for storing things mud are supported the preparation of cellar for storing things liquid
A, with yellow water 350kg, tail water 450kg, pressed liquor 200kg mixing, obtain mixed solution; Wherein, described pressed liquor is that vinasse steam after drinking, and the resulting liquid of extruding dewaters;
The aromatic Chinese spirit that adds mixed solution weight 4% in b, the mixed solution is with the bent medicine of the commercially available high temperature of pit sealing mud and mixed solution weight 5% (the bent medicine of high temperature refers to that leavening temperature is controlled at the bent medicine of making about 60 degree), mixing (alcoholic strength in the mixture is 5%vol);
C, in 30 ℃ of sealed fermentings 5 days;
D, end fermentation are filtered, and obtain the foster liquid of storing of aromatic Chinese spirit cellar for storing things mud.
The maintenance of Test Example aromatic Chinese spirit cellar for storing things mud
The aromatic Chinese spirit of the present invention cellar for storing things mud that adopts embodiment 1-4 to prepare is respectively supported and stored liquid, yellow water, tail water is foster stores 1 year (promptly keeping cellar for storing things muddy water to divide more than the 50wt%), and compares with foster cellar for storing things mud of storing, and mud subjective appreciation result is as shown in table 1 at the cellar for storing things.
Table 1 cellar for storing things mud subjective appreciation result
Can find out from table 1, adopt the present invention to support cellar for storing things liquid, can obviously improve aromatic Chinese spirit cellar for storing things shale amount.
Claims (11)
1. produce aromatic Chinese spirit cellar for storing things mud and support the method for cellar for storing things liquid, it is characterized in that comprising the steps:
A, by weight ratio with 25～40 parts of yellow waters, 40～50 parts of tail water, 10～20 parts of mixings of pressed liquor, obtain mixed solution; Wherein, described pressed liquor is that vinasse steam after drinking, and the resulting liquid of extruding dewaters;
The aromatic Chinese spirit of the bent medicine of high temperature of adding mixed solution weight 4～6% and mixed solution weight 3～5% is with pit sealing mud or cellar for storing things mud, mixing in b, the mixed solution;
C, in 25～35 ℃ of sealed fermentings 3～7 days;
D, end fermentation are filtered, and obtain the foster liquid of storing of aromatic Chinese spirit cellar for storing things mud.
2. production aromatic Chinese spirit according to claim 1 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the yellow water described in a step is that 35 parts, tail water are that 45 parts, pressed liquor are 20 parts.
3. production aromatic Chinese spirit according to claim 1 and 2 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the aromatic Chinese spirit that adds in the b step uses pit sealing mud or cellar for storing things mud to be 4% of mixed solution weight, and the bent medicine of the high temperature of adding is 5% of a mixed solution weight.
4. production aromatic Chinese spirit according to claim 1 and 2 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the alcoholic strength that adds in the b step in the mixture after bent medicine of high temperature and aromatic Chinese spirit use pit sealing mud or cellar for storing things mud is 2～6%vol.
5. production aromatic Chinese spirit according to claim 3 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the alcoholic strength that adds in the b step in the mixture after bent medicine of high temperature and aromatic Chinese spirit use pit sealing mud or cellar for storing things mud is 2～6%vol.
6. production aromatic Chinese spirit according to claim 1 and 2 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the c step was in 30 ℃ of sealed fermentings 5 days.
7. production aromatic Chinese spirit according to claim 3 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the c step was in 30 ℃ of sealed fermentings 5 days.
8. production aromatic Chinese spirit according to claim 4 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the c step was in 30 ℃ of sealed fermentings 5 days.
9. production aromatic Chinese spirit according to claim 5 cellar for storing things mud is supported the method for cellar for storing things liquid, it is characterized in that: the c step was in 30 ℃ of sealed fermentings 5 days.
10. the aromatic Chinese spirit cellar for storing things mud that the method for supporting cellar for storing things liquid by each described production aromatic Chinese spirit cellar for storing things mud of claim 1～9 is produced is supported cellar for storing things liquid.
11. the mud maintenance process of aromatic Chinese spirit cellar for storing things is characterized in that: adopt the described aromatic Chinese spirit of claim 10 cellar for storing things mud to support cellar for storing things liquid and make cellar for storing things muddy water divide content maintenance >=50wt%.
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| CN102676367B (en) * | 2012-05-10 | 2013-06-26 | 泸州品创科技有限公司 | Method for curing after opening of thick white liquor pit |
| CN102703281A (en) * | 2012-06-15 | 2012-10-03 | 泸州品创科技有限公司 | Method for replenishing nutrition of cellar mud |
| CN102766566A (en) * | 2012-08-01 | 2012-11-07 | 泸州品创科技有限公司 | White spirit brewing pit and moisturizing method thereof |
| CN105400650A (en) * | 2015-12-25 | 2016-03-16 | 宜宾金喜来酒业有限公司 | Preparation method of highly flavored type baijiu cellar mud maintenance liquid |
| CN105385644B (en) * | 2015-12-29 | 2019-02-12 | 泸州品创科技有限公司 | The functional microorganism microbial inoculum of degradation lactic acid synthesizing hexanoic acid and its application in pit mud maintenance |
| CN107177453B (en) * | 2017-07-25 | 2020-07-10 | 亳州学院 | Strong-flavor liquor pit mud maintenance liquid, preparation method and maintenance method |
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| CN109554260A (en) * | 2019-01-17 | 2019-04-02 | 北京二锅头酒业股份有限公司 | A kind of preparation method of Luzhou-flavor liquor pit mud nutrient solution |
| CN110093223A (en) * | 2019-05-09 | 2019-08-06 | 四川省宜宾市长兴酒业有限公司 | A kind of pit maintenance nutrient solution |
| CN113604306B (en) * | 2021-08-27 | 2023-08-15 | 劲牌茅台镇酒业有限公司 | Brewing method of Maotai-flavor flavoring wine |
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