CN102154819B - Curly hair moisturizing finishing agent for wig and preparation method thereof - Google Patents
Curly hair moisturizing finishing agent for wig and preparation method thereof Download PDFInfo
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- CN102154819B CN102154819B CN2010105410911A CN201010541091A CN102154819B CN 102154819 B CN102154819 B CN 102154819B CN 2010105410911 A CN2010105410911 A CN 2010105410911A CN 201010541091 A CN201010541091 A CN 201010541091A CN 102154819 B CN102154819 B CN 102154819B
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Abstract
The invention relates to a curly hair moisturizing finishing agent for wig and a preparation method thereof. The finishing agent is prepared from the following raw materials in part by weight by compatible synthesis: 10 to 18 parts of glycerin, 1 to 4 parts of sorbitol, 5 to 8 parts of peregal O-15, 15 to 20 parts of efficient penetrating agent, 3 to 10 parts of octadecane trimethyl ammonia chloride, and 40 to 66 parts of deionized water. By using thermostatic stirring, the raw material components are completely reacted more easily, and the generated product is more stable; and the particle diameter of emulsion is smaller by homogenizing and emulsifying, the whole emulsion is uniform and is not demixed, and the whole synthesis process is simpler.
Description
Technical field
The invention belongs to chemical technology, the mutual interleaving techniques of biotechnology field, be specifically related to a kind of wig with curly hair wet keeping finishing agent and preparation method thereof.
Background technology
The finishing auxiliaries of hair products use at present is main with the amido silicon oil finishing agent, and there is following defective in it: (1), typing curvature persistent period are short, and elasticity is relatively poor, and (2), feel are bad, and be relatively drier, greasy sometimes, (3), large usage quantity, cost height.
Summary of the invention
The objective of the invention is to overcome the deficiency that exists in the above-mentioned prior art and provide a kind of good hand touch, typing curvature persistent, good springiness and nontoxic, non-stimulated, the simple wig of processing technology with curly hair wet keeping finishing agent and preparation method thereof.
The objective of the invention is to realize like this:
A kind of wig is used the curly hair wet keeping finishing agent, it is characterized in that: be fused into through compatibility according to parts by weight through following raw materials and make: 10～18 parts of glycerin, 1～4 part of sorbitol, paregal O-15 5～8 part, 15～20 parts of high-efficient penetrants, 3～10 parts of octadecane agent trimethyl ammonia chlorides, 40～66 parts of deionized waters.
Described deionization hardness of water≤0.03 milli rubs/liter.
A kind of above-mentioned wig is characterized in that: carry out according to following steps with the method for preparing of curly hair wet keeping finishing agent: in deionized water, slowly add glycerin, stirred 15 minutes, leave standstill 20 minutes after; Add octadecane agent trimethyl ammonia chloride, stirred 30 minutes, after 20 minutes, add paregal O-15 and sorbitol; Stirred 30 minutes, and added high-efficient penetrant then, heat up and stir, when temperature reaches 50 ℃; Keep constant temperature, continue to stir 30 minutes, cool to room temperature; After leaving standstill 20 minutes, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.
With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
The present invention has following advantage: utilize constant temperature to stir; Raw material components reacts completely more easily, and product is more stable, and emulsifying makes particle size of emulsion littler; Whole emulsion is evenly not stratified; Whole synthesis technique is fairly simple, can reach good hand touch, typing curvature persistent, good springiness and nontoxic, non-stimulated advantage, and its technical specification and data are: good hand touch is meant that the MIU value is 0.256; The typing curvature is meant that lastingly G/ (mN.m) value is 0.0063; Good springiness is meant that the L/m value is 0.0350.
The specific embodiment
A kind of wig is used the curly hair wet keeping finishing agent, it is characterized in that: be fused into through compatibility according to parts by weight through following raw materials and make: 10～18 parts of glycerin, 1～4 part of sorbitol, paregal O-15 5～8 part, 15～20 parts of high-efficient penetrants, 3～10 parts of octadecane agent trimethyl ammonia chlorides, 40～66 parts of deionized waters.Described deionization hardness of water≤0.03 milli rubs/liter.
A kind of above-mentioned wig is characterized in that: carry out according to following steps with the method for preparing of curly hair wet keeping finishing agent: in deionized water, slowly add glycerin, stirred 15 minutes, leave standstill 20 minutes after; Add octadecane agent trimethyl ammonia chloride, stirred 30 minutes, after 20 minutes, add paregal O-15 and sorbitol; Stirred 30 minutes, and added high-efficient penetrant then, heat up and stir, when temperature reaches 50 ℃; Keep constant temperature, continue to stir 30 minutes, cool to room temperature; After leaving standstill 20 minutes, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.
Embodiment 1: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 10 grams, sorbitol 1 gram, paregal O-15 5 gram, high-efficient penetrant 15 grams, octadecane agent trimethyl ammonia chloride 3 grams, deionized water 66 grams.
Slowly add 10 gram glycerin in the deionized waters at 66 grams, stirred 15 minutes, leave standstill 20 minutes after, add 3 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes, add 15 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 2: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 18 grams, sorbitol 1 gram, paregal O-15 5 gram, high-efficient penetrant 15 grams, octadecane agent trimethyl ammonia chloride 3 grams, deionized water 40 grams.
Slowly add 18 gram glycerin in the deionized waters at 40 grams, stirred 15 minutes, leave standstill 20 minutes after, add 3 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes, add 15 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 3: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 10 grams, sorbitol 4 grams, paregal O-15 5 gram, high-efficient penetrant 15 grams, octadecane agent trimethyl ammonia chloride 3 grams, deionized water 40 grams.
Slowly add 10 gram glycerin in the deionized waters at 40 grams, stirred 15 minutes, leave standstill 20 minutes after, add 3 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 5 gram paregal Os-15 and 4 gram sorbitol, stirred 30 minutes, add 15 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 4: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 10 grams, sorbitol 1 gram, paregal O-15 8 gram, high-efficient penetrant 15 grams, octadecane agent trimethyl ammonia chloride 3 grams, deionized water 40 grams.
Slowly add 10 gram glycerin in the deionized waters at 40 grams, stirred 15 minutes, leave standstill 20 minutes after, add 3 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 8 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes, add 15 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 5: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 10 grams, sorbitol 1 gram, paregal O-15 5 gram, high-efficient penetrant 20 grams, octadecane agent trimethyl ammonia chloride 3 grams, deionized water 40 grams.
Slowly add 10 gram glycerin in the deionized waters at 40 grams, stirred 15 minutes, leave standstill 20 minutes after, add 3 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes, add 20 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 6: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 10 grams, sorbitol 1 gram, paregal O-15 5 gram, high-efficient penetrant 15 grams, octadecane agent trimethyl ammonia chloride 10 grams, deionized water 40 grams.
Slowly add 10 gram glycerin in the deionized waters at 40 grams, stirred 15 minutes, leave standstill 20 minutes after, add 10 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes, add 20 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 7: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 10 grams, sorbitol 1 gram, paregal O-15 5 gram, high-efficient penetrant 15 grams, octadecane agent trimethyl ammonia chloride 3 grams, deionized water 40 grams.
Slowly add 10 gram glycerin in the deionized waters at 40 grams, stirred 15 minutes, leave standstill 20 minutes after, add 3 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes, add 15 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 8: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 18 grams, sorbitol 4 grams, paregal O-15 8 gram, high-efficient penetrant 20 grams, octadecane agent trimethyl ammonia chloride 10 grams, deionized water 66 grams.
Slowly add 18 gram glycerin in the deionized waters at 66 grams, stirred 15 minutes, leave standstill 20 minutes after, add 10 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 8 gram paregal Os-15 and 4 gram sorbitol, stirred 30 minutes, add 20 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 9: a kind of wig is used the curly hair wet keeping finishing agent, is fused into through compatibility according to the weight in grams number through following raw materials to make: glycerin 15 grams, sorbitol 2 grams, paregal O-15 7 gram, high-efficient penetrant 18 grams, octadecane agent trimethyl ammonia chloride 8 grams, deionized water 50 grams.
Slowly add 15 gram glycerin in the deionized waters at 50 grams, stirred 15 minutes, leave standstill 20 minutes after, add 8 gram octadecane agent trimethyl ammonia chlorides, stirred 30 minutes; After waiting 20 minutes afterwards, add 7 gram paregal Os-15 and 4 gram sorbitol, stirred 30 minutes, add 18 gram high-efficient penetrants then; Heat up and stir, when temperature reaches 50 ℃, keep constant temperature, continue to stir 30 minutes; Cool to room temperature, leave standstill 20 minutes after, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.With blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 10: slowly add 10 gram glycerin in the deionized waters at 65 grams, stirred 15 minutes, leave standstill 20 minutes after, add 4 gram octadecane agent trimethyl ammonia chlorides; Stirred 30 minutes, and after 20 minutes, added 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes; Add 15 gram high-efficient penetrants then, heat up and stir, when temperature reaches 50 ℃, keep constant temperature; Continue to stir 30 minutes, and cooled to room temperature, leave standstill 20 minutes after; Carried out emulsifying 45 minutes, and left standstill and got final product in 30 minutes. with blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 11: slowly add 10 gram glycerin in the deionized waters at 66 grams, stirred 15 minutes, leave standstill 20 minutes after, add 3 gram octadecane agent trimethyl ammonia chlorides; Stirred 30 minutes, and after 20 minutes, added 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes; Add 15 gram high-efficient penetrants then, heat up and stir, when temperature reaches 50 ℃, keep constant temperature; Continue to stir 30 minutes, and cooled to room temperature, leave standstill 20 minutes after; Carried out emulsifying 45 minutes, and left standstill and got final product in 30 minutes. with blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 12: slowly add 10 gram glycerin in the deionized waters at 64 grams, stirred 15 minutes, leave standstill 20 minutes after, add 5 gram octadecane agent trimethyl ammonia chlorides; Stirred 30 minutes, and after 20 minutes, added 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes; Add 15 gram high-efficient penetrants then, heat up and stir, when temperature reaches 50 ℃, keep constant temperature; Continue to stir 30 minutes, and cooled to room temperature, leave standstill 20 minutes after; Carried out emulsifying 45 minutes, and left standstill and got final product in 30 minutes. with blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 13: slowly add 10 gram glycerin in the deionized waters at 63 grams, stirred 15 minutes, leave standstill 20 minutes after, add 6 gram octadecane agent trimethyl ammonia chlorides; Stirred 30 minutes, and after 20 minutes, added 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes; Add 15 gram high-efficient penetrants then, heat up and stir, when temperature reaches 50 ℃, keep constant temperature; Continue to stir 30 minutes, and cooled to room temperature, leave standstill 20 minutes after; Carried out emulsifying 45 minutes, and left standstill and got final product in 30 minutes. with blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 14: slowly add 10 gram glycerin in the deionized waters at 62 grams, stirred 15 minutes, leave standstill 20 minutes after, add 7 gram octadecane agent trimethyl ammonia chlorides; Stirred 30 minutes, and after 20 minutes, added 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes; Add 15 gram high-efficient penetrants then, heat up and stir, when temperature reaches 50 ℃, keep constant temperature; Continue to stir 30 minutes, and cooled to room temperature, leave standstill 20 minutes after; Carried out emulsifying 45 minutes, and left standstill and got final product in 30 minutes. with blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 15: slowly add 10 gram glycerin in the deionized waters at 61 grams, stirred 15 minutes, leave standstill 20 minutes after, add 8 gram octadecane agent trimethyl ammonia chlorides; Stirred 30 minutes, and after 20 minutes, added 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes; Add 15 gram high-efficient penetrants then, heat up and stir, when temperature reaches 50 ℃, keep constant temperature; Continue to stir 30 minutes, and cooled to room temperature, leave standstill 20 minutes after; Carried out emulsifying 45 minutes, and left standstill and got final product in 30 minutes. with blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Embodiment 16: slowly add 10 gram glycerin in the deionized waters at 60 grams, stirred 15 minutes, leave standstill 20 minutes after, add 9 gram octadecane agent trimethyl ammonia chlorides; Stirred 30 minutes, and after 20 minutes, added 5 gram paregal Os-15 and 1 gram sorbitol, stirred 30 minutes; Add 15 gram high-efficient penetrants then, heat up and stir, when temperature reaches 50 ℃, keep constant temperature; Continue to stir 30 minutes, and cooled to room temperature, leave standstill 20 minutes after; Carried out emulsifying 45 minutes, and left standstill and got final product in 30 minutes. with blue thick PVC Plastic Drum sealing dress, shady and cool place preserves with the curly hair wet keeping finishing agent.
Claims (2)
1. a wig is used the curly hair wet keeping finishing agent, it is characterized in that: be fused into through compatibility according to parts by weight through following raw materials and make: 10～18 parts of glycerin, 1～4 part of sorbitol, paregal O-15 5～8 part, 15～20 parts of high-efficient penetrants, 3～10 parts of octadecyl trimethyl ammonia chlorides, hardness≤0.03 milli rub/liter 40～66 parts of deionized waters.
2. a wig as claimed in claim 1 is characterized in that: carry out according to following steps with the method for preparing of curly hair wet keeping finishing agent: in deionized water, slowly add glycerin, stirred 15 minutes, leave standstill 20 minutes after; Add octadecyl trimethyl ammonia chloride, stirred 30 minutes, after 20 minutes, add paregal O-15 and sorbitol; Stirred 30 minutes, and added high-efficient penetrant then, heat up and stir, when temperature reaches 50 ℃; Keep constant temperature, continue to stir 30 minutes, cool to room temperature; After leaving standstill 20 minutes, carried out emulsifying 45 minutes, leave standstill and got final product in 30 minutes.
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| CN2010105410911A CN102154819B (en) | 2010-11-12 | 2010-11-12 | Curly hair moisturizing finishing agent for wig and preparation method thereof |
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| CN2010105410911A CN102154819B (en) | 2010-11-12 | 2010-11-12 | Curly hair moisturizing finishing agent for wig and preparation method thereof |
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| CN102154819A CN102154819A (en) | 2011-08-17 |
| CN102154819B true CN102154819B (en) | 2012-05-16 |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1965793A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Hair conditioner and preparation process thereof |
| EP1800659A1 (en) * | 2005-12-22 | 2007-06-27 | L'Oréal | Cosmetic composition comprising at least one cationic polyvinyllactam, at least one fatty alcohol and at least one polyol, method for treatment of keratin fibres and use |
| CN101605528A (en) * | 2007-02-05 | 2009-12-16 | 宝洁公司 | Hair care composition |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6936735B2 (en) * | 2002-08-27 | 2005-08-30 | Emd Chemicals, Inc. | Photostable cationic organic sunscreen compounds and compositions obtained therefrom |
| US20060083702A1 (en) * | 2004-04-02 | 2006-04-20 | Thomas Fondin | Hair fiber treating method |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1800659A1 (en) * | 2005-12-22 | 2007-06-27 | L'Oréal | Cosmetic composition comprising at least one cationic polyvinyllactam, at least one fatty alcohol and at least one polyol, method for treatment of keratin fibres and use |
| CN1965793A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Hair conditioner and preparation process thereof |
| CN101605528A (en) * | 2007-02-05 | 2009-12-16 | 宝洁公司 | Hair care composition |
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| CN102154819A (en) | 2011-08-17 |
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