CN104073206B - Modified epoxy glue paste formula and preparation technology thereof - Google Patents
Modified epoxy glue paste formula and preparation technology thereof Download PDFInfo
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- CN104073206B CN104073206B CN201410286164.5A CN201410286164A CN104073206B CN 104073206 B CN104073206 B CN 104073206B CN 201410286164 A CN201410286164 A CN 201410286164A CN 104073206 B CN104073206 B CN 104073206B
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Abstract
Modified epoxy glue paste formula and preparation technology thereof, comprise epoxy resin, nitrile rubber-40,2-ethyl-4-methylimidazole, aluminum oxide powder, this diamines, diethylenetriamine, tritolyl phosphate, essence, 40% caustic-soda aqueous solution.Epoxy resin, nitrile rubber-40 are added in agitator, obtains mixing solutions; 2-ethyl-4-methylimidazole is poured in stirred pot, dissolve; Diethylenetriamine, tritolyl phosphate are added in agitator two, stirs 10 minutes, obtain mixing solutions two; Get in mixing solutions and mixing solutions two to reactor in the ratio of 100:8; Heat, temperature controls at 70 DEG C, heats 30 minutes; Get 40% caustic-soda aqueous solution to regulate pH value, pH value is controlled at 4-7; Finally add essence.The present invention is nontoxic, nonflammable, and technique is simple, and property favorable rates is honest and clean, of many uses, practical.
Description
Technical field:
The present invention relates to a kind of sizing agent, be specifically related to modified epoxy glue paste formula and preparation technology thereof.
Background technology:
Chemical industry is development in modern times mainstay of the national economy industry very rapidly, and fine chemistry industry tail gas important component part, obtain the development of advancing by leaps and bounds in 20th century, the clothing, food, lodging and transportion--basic necessities of life of the unresolved mankind and the energy, resource and environment problem make significant contribution.
Sizing agent is that development of modern industry and human living standard improve requisite important materials, and sizing agent and bonding technology, with the incomparable special warfare of other mode of connection, play great effect in modern economy, modern national defense, modern science and technology.
Summary of the invention:
Technical problem to be solved by this invention is the defect overcoming prior art, provides a kind of modified epoxy glue paste formula and preparation technology thereof.
Technical problem to be solved by this invention realizes by the following technical solutions.
Modified epoxy glue paste is filled a prescription, and it is characterized in that: its composition mainly comprises:
Modified epoxy glue paste preparation technology, is characterized in that: specifically comprise the following steps:
1) epoxy resin, nitrile rubber-40 are added in agitator, stir 10 minutes, obtain mixing solutions;
2) pour in stirred pot by 2-ethyl-4-methylimidazole, heat, temperature controls, at 60-70 DEG C, 10-20 minute, to dissolve completely with mixing solutions;
3) diethylenetriamine, tritolyl phosphate are added in agitator two, stir 10 minutes, obtain mixing solutions two;
4) get in mixing solutions and mixing solutions two to reactor in the ratio of 100:8;
5) heat, temperature controls at 70-80 DEG C, heats 30 minutes;
6) get 40% caustic-soda aqueous solution to regulate pH value, pH value is controlled at 4-7;
7) finally add essence, be uniformly mixed and obtain finished product.
Feature of the present invention: nontoxic, nonflammable, technique is simple, and property favorable rates is honest and clean, of many uses, practical.
Embodiment:
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with specific embodiment, setting forth the present invention further.
Specific embodiment: modified epoxy glue paste is filled a prescription, and its composition mainly comprises:
Modified epoxy glue paste preparation technology, specifically comprises the following steps: add in agitator by epoxy resin, nitrile rubber-40, stirs 10 minutes, obtains mixing solutions; Poured into by 2-ethyl-4-methylimidazole in stirred pot, heat, temperature controls, at 60 DEG C, 10 minutes, to dissolve completely with mixing solutions; Diethylenetriamine, tritolyl phosphate are added in agitator two, stirs 10 minutes, obtain mixing solutions two; Get in mixing solutions and mixing solutions two to reactor in the ratio of 100:8; Heat, temperature controls at 70 DEG C, heats 30 minutes; Get 40% caustic-soda aqueous solution to regulate pH value, pH value is controlled at 4-7; Finally add essence, be uniformly mixed and obtain finished product.
More than show and describe ultimate principle of the present invention, principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (1)
1. modified epoxy glue paste preparation technology, is characterized in that: specifically comprise the following steps:
1) epoxy resin, paracril-40 are added in agitator, stir 10 minutes, obtain mixing solutions;
2) pour in agitator by 2-ethyl-4-methylimidazole, heat, temperature controls, at 60-70 DEG C, 10-20 minute, to dissolve completely with mixing solutions;
3) diethylenetriamine, tritolyl phosphate are added in agitator two, stir 10 minutes, obtain mixing solutions two;
4) get in mixing solutions and mixing solutions two to reactor in the ratio of 100:8;
5) heat, temperature controls at 70-80 DEG C, heats 30 minutes;
6) get 40% caustic-soda aqueous solution to regulate pH value, pH value is controlled at 4-7;
7) finally add essence, be uniformly mixed and obtain finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410286164.5A CN104073206B (en) | 2014-06-23 | 2014-06-23 | Modified epoxy glue paste formula and preparation technology thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410286164.5A CN104073206B (en) | 2014-06-23 | 2014-06-23 | Modified epoxy glue paste formula and preparation technology thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104073206A CN104073206A (en) | 2014-10-01 |
| CN104073206B true CN104073206B (en) | 2015-09-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410286164.5A Expired - Fee Related CN104073206B (en) | 2014-06-23 | 2014-06-23 | Modified epoxy glue paste formula and preparation technology thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN104073206B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105695124A (en) * | 2016-02-29 | 2016-06-22 | 安徽海德石油化工有限公司 | Faint scent plant mixed cleaning agent and preparation method thereof |
| CN107474915A (en) * | 2017-07-29 | 2017-12-15 | 巢湖鹏远金属焊管有限公司 | A kind of metal tube stretching reduces lubricating oil of friction cut and preparation method thereof |
| CN107354780A (en) * | 2017-08-01 | 2017-11-17 | 界首市宏利塑料有限公司 | A kind of surface of plastic products dyeing |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102101934B (en) * | 2009-12-17 | 2013-05-29 | 比亚迪股份有限公司 | Reinforcing rubber sheet base composition, reinforcing rubber sheet base and steel plate composite material |
| CN102417804B (en) * | 2010-09-28 | 2013-12-18 | 比亚迪股份有限公司 | Adhesive, its preparation method and application method |
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2014
- 2014-06-23 CN CN201410286164.5A patent/CN104073206B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
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| CN104073206A (en) | 2014-10-01 |
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| C06 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Zeng Sui Inventor before: Ding Wenchang Inventor before: Jiang Yilong Inventor before: Xu Lang Inventor before: Feng Junchao Inventor before: Feng Shusong Inventor before: Feng Junbiao Inventor before: Pei Jianjun |
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| CB03 | Change of inventor or designer information | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170424 Address after: Faldan Industrial Zone, Futian Town Guangdong city of Huizhou province Boluo County 516131 Patentee after: Boluo evergreen Adhesive Products Co., Ltd. Address before: 239200 Anhui city of Chuzhou province to County town at Nanjing Road West Tower Patentee before: ANHUI SHENZHOU SPACESHIP ADHESIVE CO., LTD. |
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| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150930 Termination date: 20170623 |
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| CF01 | Termination of patent right due to non-payment of annual fee |