CN102146592A - Regenerated cellulose fat-burning fiber and production method thereof - Google Patents
Regenerated cellulose fat-burning fiber and production method thereof Download PDFInfo
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- CN102146592A CN102146592A CN2011100260908A CN201110026090A CN102146592A CN 102146592 A CN102146592 A CN 102146592A CN 2011100260908 A CN2011100260908 A CN 2011100260908A CN 201110026090 A CN201110026090 A CN 201110026090A CN 102146592 A CN102146592 A CN 102146592A
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Abstract
The invention discloses a regenerated cellulose fat-burning fiber and a production method thereof. The production method comprises the following steps of: dissolving natural cellulose by sodium hydroxide to prepare a spinning A solution, simultaneously, performing microencapsulation treatment on compound essence with a fat-burning function, adding the microencapsulated compound essence to the spinning A solution to obtain a spinning B solution with the fat-burning function, and performing wet spinning on the spinning B solution to prepare the regenerated cellulose fiber with the fat-burning function. The prepared regenerated cellulose fiber with the fat-burning function is woven to prepare a regenerated cellulose fiber fabric with the fat-burning function. The fabric prepared from the regenerated cellulose fiber disclosed by the invention can activate adipocyte and accelerate fat metabolism, so that fat in the adipose tissues of a human body splits and loses and a person regains a fine figure and agreeable rondure. The regenerated cellulose fiber has no side effects, and simultaneously has a toxin expelling effect on the body, thus enhancing the body immunity. The fiber or the fabric is comfortable in feel and washable.
Description
Technical field
The present invention relates to a kind of functional regenerated cellulose fibre and production method thereof, especially a kind of regenerated celulose fibre and production method thereof that possesses combustion fat function.
Background technology
The pure natural plant essential oil relaxes with its character, beauty treatment, health care, and toxic and side effect is little, more and more is subjected to people's favor, so plants essential oil is developed rapidly in the function cosmetics.Its use except oral, add in the cosmetics or spread upon directly that the skin surface massage absorbs, air has occurred again plants essential oil is prepared into the nanoscale microcapsules sucking, be coated in yarn or fabric face by certain postfinishing process, its purpose all is the function of performance plants essential oil.
Possess the natural plant essential oils of combustion fat function, also more common on the market at home, do not appear in the newspapers but possess the plants essential oil capsule of nano that fires the fat function.Using the more of combustion fat function essential oil is to be prepared into paste or liquid condition, spreads upon skin surface.The plain microcapsule dressing agent of a kind of weight reducing is arranged on the market, major part is used to be artificial sintetics, its composition is CLA (Conjugated linoleic acid, abbreviation CLA) microcapsules, its effect is to reduce the body fat ratio, make physique more strong, with the domestic great majority gentle and graceful stature that the personage pursues of liking to be beautiful not be identical concept, be more suitable in personages such as sportsmen.In addition, when adopting microcapsule dressing agent that yarn or lining are carried out back arrangement, need to use adhesive to guarantee adhesive force between microcapsules and the lining, therefore to lining feel generation certain influence, the wash resistant number of times has limited the function performance of lining generally at 10 ~ 40 times.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, a kind of production method that possesses the regenerated cellulose combustion fat fiber of combustion fat function is provided, it makes spinning A liquid with the native cellulose dissolving, after simultaneously the compound essential oil that possesses combustion fat function being carried out the microencapsulation processing, add the spinning B liquid that obtains to possess combustion fat function in the spinning A liquid to, spinning B liquid is carried out wet spinning can prepare the regenerated celulose fibre that possesses combustion fat function.Again the prepared regenerated celulose fibre that possesses combustion fat function that goes out is weaved and to produce out the regenerated celulose fibre lining that possesses combustion fat function.The lining of the described regenerated celulose fibre preparation of the application of the invention can activate adipocyte, quickens fat metabolism, makes lipolysis, the loss of body fat mass in human body tissue, makes stature recover slender, and curve is exquisite to be caused.Not only be free from side effects, simultaneously health had effect of ejecting poison, increase body immunity.This fiber or lining be comfortable feel not only, and wash resistant.This fiber or lining are not only useful to health, and be more favourable to environmental protection, can natural degradation.
For realizing above technical purpose, the present invention will take following technical scheme:
A kind of production method of regenerated cellulose combustion fat fiber, may further comprise the steps: (1) carries out dissolution process to native cellulose, to prepare spinning A liquid; The compound essential oil that possesses combustion fat function is carried out microencapsulation handle, to prepare combustion fat compound essential oil microcapsules; (2) will fire fat compound essential oil microcapsules and add in the spinning A liquid, and make combustion fat compound essential oil microcapsules and spinning A liquid mix, to make spinning B liquid; In spinning B liquid, the mass ratio of combustion fat compound essential oil microcapsules and spinning A liquid is 1 ~ 15:100; (3) spinning B liquid is carried out wet spinning, to prepare the regenerated cellulose combustion fat fiber that possesses combustion fat function.
The compound essential oil that possesses combustion fat function in the described step (1) comprises Rosemary Oil, needle juniper essential oil, Salvia japonica essential oil, thyme essential oil and grape fruit essential oil, and the mass ratio of Rosemary Oil, needle juniper essential oil, Salvia japonica essential oil, thyme essential oil and grape fruit essential oil is 1:1:1:1:1.
The preparation process of spinning A liquid comprises described in the step (1): at first adopting concentration is the sodium hydroxide solution dipping pulp of 240g/L, with the native cellulose synthetic alkali cellulose in the pulp; Then add CS
2Solution is to make cellulose sulfonate with alkali cellulose; Cellulose sulfonate is dissolved in the sodium hydroxide solution that concentration is 6.4-6.6g/L at last, can makes spinning A liquid.
Another technical purpose of the present invention provides a kind of regenerated cellulose combustion fat fiber, comprise regenerated celulose fibre, combustion fat compound essential oil microcapsules, moisture and finish, described regenerated cellulose combustion fat fiber quality adds up to 100, and wherein the quality of regenerated celulose fibre, combustion fat compound essential oil microcapsules, moisture and finish respectively accounts for 79 ~ 87,5 ~ 12,7 ~ 13 and 0.1 ~ 0.3 respectively; In addition, dried fracture strength 〉=1.42cN/dtex, the wet breaking strength 〉=0.64cN/dtex of described regenerated cellulose combustion fat fiber.
According to above technical scheme, can realize following beneficial effect:
The production method of regenerated cellulose combustion fat fiber of the present invention, by adopting the dissolution of sodium hydroxide native cellulose to make spinning A liquid, and fat compound essential oil microcapsules are fired in interpolation in this spinning A liquid, to make the spinning B liquid that possesses combustion fat function, can prepare the regenerated cellulose combustion fat fiber that possesses combustion fat function by spinning B liquid being carried out wet spinning.Therefore, the present invention promptly adds combustion fat compound essential oil microcapsules in the preparation spinning solution stage, make these combustion fat compound essential oil microcapsules be distributed in cellulosic fiber surface or be coated between the fiber, therefore, the regenerated cellulose that uses the present invention to make fires in the process of fat fiber, combustion fat compound essential oil microcapsules constantly discharge, and are absorbed by the body the effect of performance combustion fat functionalization by skin.In addition, combustion fat compound essential oil is distributed between the fiber of regenerated cellulose in the mode of microcapsules, and therefore, washing durability of the present invention is good.
The specific embodiment
Explain technical scheme of the present invention below with reference to three preferred embodiments.
The production method of regenerated cellulose combustion fat fiber of the present invention, may further comprise the steps: (1) carries out dissolution process to native cellulose, to prepare spinning A liquid, the preparation process of described spinning A liquid comprises: at first adopting concentration is the sodium hydroxide solution dipping pulp of 240g/L, with the native cellulose synthetic alkali cellulose in the pulp; Then add CS
2Solution is to make cellulose sulfonate with alkali cellulose; Cellulose sulfonate is dissolved in the sodium hydroxide solution that concentration is 6.4-6.6g/L at last, can makes spinning A liquid; The compound essential oil that possesses combustion fat function is carried out microencapsulation to be handled, to prepare combustion fat compound essential oil microcapsules, the described compound essential oil that possesses combustion fat function comprises Rosemary Oil, needle juniper essential oil, Salvia japonica essential oil, thyme essential oil and grape fruit essential oil, and the mass ratio of Rosemary Oil, needle juniper essential oil, Salvia japonica essential oil, thyme essential oil and grape fruit essential oil is 1:1:1:1:1; (2) will fire fat compound essential oil microcapsules and add in the spinning A liquid, and make combustion fat compound essential oil microcapsules and spinning A liquid mix, to make spinning B liquid; In spinning B liquid, the mass ratio of combustion fat compound essential oil microcapsules and spinning A liquid is 1 ~ 15:100; (3) spinning B liquid is carried out wet spinning, to prepare the regenerated cellulose combustion fat fiber that possesses combustion fat function.
This fiber adopts regenerated cellulose preparation of product, belongs to the artificial fibre category, can not only natural degradation, also very favourable, and its used raw material can constantly regenerate to environmental protection, more can be as the used oil of chemical fibre product " exhaustion " day by day.Especially the wherein used solvent-borne type regenerated celulose fibre of the implementation case four pollutes lessly relatively in its production process, social economic value is more arranged.
The compound essential oil that possesses combustion fat function that this fiber production adopted is the pure natural plant essential oil, and prescription comprises Rosemary Oil, needle juniper essential oil, Salvia japonica essential oil, thyme essential oil and grape fruit essential oil, and ratio is 1:1:1:1:1.The pure natural plant essential oil is to obtain in the Nature, can quicken the metabolism of adipocyte, makes lipolysis, the loss of body fat tissue, excretes with seasonal vivotoxin, increases human immunity.
The combustion fat compound essential oil microcapsules that the pure natural plant essential oil microcapsulesization is made promptly add in the spinning A liquid at spinning B liquid preparatory phase, combustion fat compound essential oil microcapsule content scope is 1 ~ 15%, all the other content are regenerated cellulose, combustion fat compound essential oil microcapsules are distributed in the regenerated celulose fibre surface or are coated in the middle of the regenerated celulose fibre, in use constantly slowly-releasing comes out, be absorbed by the body performance functionalization effect by skin.In addition, because natural plant essential oils exists in the middle of the regenerated celulose fibre with the form of microcapsules, so washing fastness is good.
Because this regenerated cellulose combustion fat fiber belongs to functional regenerated cellulose fibre, can make knit fabric, shuttle-woven fabric separately, is widely used in socks, underwear, bed necessaries etc., allow human body obtain the weight reducing of combustion fat, toxin expelling health care function unconsciously.
Possess that each composition is described as follows in the compound essential oil prescription of combustion fat function:
Rosemary Oil extracts from flower and leaf.Alleviate dermohemia, edema, swelling; Restrain skin, improve dandruff; Discongest dysmenorrhoea, diuresis, fat-reducing; Stomach and intestine, the heart, lung, liver, courage all there is benifit; The needle juniper essential oil extracts from fruit.Improve pore obstruction, dermatitis, eczema, abscess; Potent diuresis, fat-reducing and functions of expelling toxin are removed uric acid;
The Salvia japonica essential oil extracts from flower and leaf.It is intensely dark to improve hair; Hemostasis, healing of wound, to improve pore thick; Improve constipation, diuresis, fat-reducing; Help the lymph toxin expelling, improve blood pressure; Help the various pain of post exercise to discongest; Strengthen memory, calm neural.
Thyme essential oil extracts from flower, leaf.Prevent alopecia, improve wound, sore, eczema; Moistening lung, cure cold, cough, have sore throat, go phlegm, low blood pressure, rheumatism, leukorrhea; Reinforcement nerve, activating brain cell, mnemonic(al) are recollected notice and are concentrated.
The grape fruit essential oil extracts from pericarp.Headache dysmenorrhoea is lost weight, is alleviated in the toxin expelling diuresis; Stimulate circulation, purify the blood; Promote digestion; Help to get rid of gall stone, nourishing the liver; Increase skin elasticity, whiten, preserve moisture, improve the colour of skin; Make in high spirits, enhancing confidence, anti-dejected.
This compound essential oil that possesses combustion fat function can be bought in market.
The invention provides a kind of regenerated cellulose combustion fat fiber, comprise regenerated celulose fibre, combustion fat compound essential oil microcapsules, moisture and finish, described regenerated cellulose combustion fat fiber quality adds up to 100, and wherein the quality of regenerated celulose fibre, combustion fat compound essential oil microcapsules, moisture and finish respectively accounts for 79 ~ 87,5 ~ 12,7 ~ 13 and 0.1 ~ 0.3 respectively; In addition, dried fracture strength 〉=1.42cN/dtex, the wet breaking strength 〉=0.64cN/dtex of described regenerated cellulose combustion fat fiber.
At first will make the raw material that regenerated celulose fibre is used---pulp (wood pulp or cotton pulp, after mixed batch of process stipulation, carry out impregnation process with sodium hydroxide solution, make is that cellulosic raw material becomes intermediate product 1---alkali cellulose originally, subsequently that it is unnecessary alkali lye is extruded by squeezing, through pulverizing, experienced after, make the reaction of this intermediate product and carbon disulfide with generation intermediate product 2---cellulose sulfonate again; The cellulose sulfonate that generates is dissolved in the sig water, can be so as to making for the stoste of spinning---viscose glue, again through mix with combustion fat compound essential oil microcapsules, filtration, deaeration, maturation), carry out wet spinning at last and make spun filament, spinning speed is about 80-100mm/min; Obtain spun filament through boundling, drawing-off, heat treatment, drowning, carry out post processing again, promptly make finished product through detecting packing at last.
The technology of preparing of combustion fat compound essential oil microcapsules is discloseder technology, domestic have relevant factory to realize, usually gained is the mixed solution state, about the about 5um of footpath grain size, essential oil content is more than 30%, high molecular polymer is more than 30%, and the pH value is between 6.0 ~ 6.5, and technological temperature is controlled at below 95 ℃.
Different according to using regenerated cellulose to require below, divide following several case study on implementation:
Case study on implementation one
Cotton type viscose staple fibre (being commonly called as artificial cotton), the relative density of fiber is 1.50 ~ 1.52, and the fiber degree of polymerization is greatly about 250 ~ 300, and degree of crystallinity is approximately about 30%; Having good hydroscopicity is 11% ~ 13%, and shearing length is 35 ~ 40mm.Adopting wood pulp (α-content of cellulose 〉=89%) or cotton pulp (α-content of cellulose 〉=96%), be approximately 240g/L with NaOH(concentration) solution makes alkali cellulose, with CS
2Solution is made cellulose sulfonate, is dissolved in the sig water that concentration is 6.4-6.6g/L, makes spinning solution; To carry out blend with combustion fat compound essential oil microcapsules through the spinning solution that three roads filter,, obtain spun filament, cut off falling into current (H after boundling, drawing-off, the heat treatment through spinning after vacuum (0.094Mpa) deaeration
2SO
4), carry out post processing again, promptly make finished product through detecting packing at last.Prepared finished product regenerated cellulose combustion fat fiber, obtaining wherein by the detection of chemical solvent dissolution method, the mass fraction of each component consists of: 84.6 parts of cotton type viscose staple fibres; Combustion fat compound essential oil microcapsules are for accounting for 5.4 parts; 9.8 parts of water accounts, finish account for 0.2 part.The finish that adopts that oils is that common viscose fiber is used.
Case study on implementation two
(modal), the fiber degree of polymerization is greatly about 350 ~ 500 for polynosic, polynosic, and fibre crystallinity is approximately 40% ~ 48% for high humidity high-modulus viscose; Have good absorbability, official regain is 9%-11%.Adopt cotton pulp (α-content of cellulose 〉=96%), make alkali cellulose with NaOH solution, with CS
2Solution (content be not less than α-content of cellulose 45%) is made cellulose sulfonate, is dissolved in diluted alkaline (NaOH content should be lower than contained α-content of cellulose 62%).Spinning solution mixes with combustion fat compound essential oil microcapsules, obtains spun filament through spinning, cuts off falling into current (H after boundling, drawing-off, the heat treatment
2SO
4＜40g/L), carry out post processing again, promptly make finished product through detecting packing at last.Prepared finished product regenerated cellulose combustion fat fiber, obtaining wherein by the detection of chemical solvent dissolution method, the mass fraction of each component consists of: 81.88 parts of polynosic; Combustion fat compound essential oil microcapsules are for accounting for 7.12 parts; 10.8 parts of water accounts, finish account for 0.2 part.The finish that adopts that oils is that common viscose fiber is used.
Case study on implementation three
The solvent-borne type regenerated celulose fibre (Lyocell, tencel), the fiber degree of polymerization is greatly about 500 ~ 550, and degree of crystallinity is approximately about 50%; Hydroscopicity is 10% ~ 12%.Adopt the cellulosic material of high-quality---and pulp (α-content of cellulose〉95%, the degree of polymerization〉600), after tearing up it directly is dissolved in the spinning solution that makes in the organic solvent N-methyl morpholine-N-oxide (NMMO) that contains suitable quantity of water, after filtration, after the deaeration with after combustion fat compound essential oil microcapsules fully mix, deliver on the spinning machine, (the component pressure scope is to extrude 0.0103～0.0257Mpa) pore from spinning head, through one section air gap layer, enter coagulating bath Cheng Sihou, subsequently again through washing, oil, drying, manufacturing procedures such as cut-out make finished product.Prepared finished product regenerated cellulose combustion fat fiber, obtaining wherein by the detection of chemical solvent dissolution method, the mass fraction of each component consists of: 79.2 parts of solvent-borne type regenerated celulose fibres; Combustion fat compound essential oil microcapsules are for accounting for 8.8 parts; 11.8 parts of water accounts, finish account for 0.2 part.The finish that adopts that oils is that common viscose fiber is used.
Claims (4)
1. the production method of a regenerated cellulose combustion fat fiber is characterized in that, may further comprise the steps:
(1) native cellulose is carried out dissolution process, to prepare spinning A liquid; The compound essential oil that possesses combustion fat function is carried out microencapsulation handle, to prepare combustion fat compound essential oil microcapsules;
(2) will fire fat compound essential oil microcapsules and add in the spinning A liquid, and make combustion fat compound essential oil microcapsules and spinning A liquid mix, to make spinning B liquid; In spinning B liquid, the mass ratio of combustion fat compound essential oil microcapsules and spinning A liquid is 1 ~ 15:100; Spinning B liquid is carried out wet spinning, to prepare the regenerated cellulose combustion fat fiber that possesses combustion fat function.
2. according to the production method of the described regenerated cellulose of claim 1 combustion fat fiber, it is characterized in that, the compound essential oil that possesses combustion fat function in the described step (1) comprises Rosemary Oil, needle juniper essential oil, Salvia japonica essential oil, thyme essential oil and grape fruit essential oil, and the quality proportioning of Rosemary Oil, needle juniper essential oil, Salvia japonica essential oil, thyme essential oil and grape fruit essential oil is 1:1:1:1:1.
3. according to the production method of the described regenerated cellulose of claim 1 combustion fat fiber, it is characterized in that, the preparation process of spinning A liquid comprises described in the step (1): at first adopting concentration is the sodium hydroxide solution dipping pulp of 240g/L, with the native cellulose synthetic alkali cellulose in the pulp; Then add CS
2Solution is to make cellulose sulfonate with alkali cellulose; Cellulose sulfonate is dissolved in the sodium hydroxide solution that concentration is 6.4-6.6g/L at last, can makes spinning A liquid.
4. the prepared regenerated cellulose of production method of the described regenerated cellulose combustion of claim 1 a fat fiber fires the fat fiber, it is characterized in that, this regenerated cellulose combustion fat fiber comprises regenerated celulose fibre, combustion fat compound essential oil microcapsules, moisture and finish, described regenerated cellulose combustion fat fiber quality adds up to 100, and wherein the quality of regenerated celulose fibre, combustion fat compound essential oil microcapsules, moisture and finish respectively accounts for 79 ~ 87,5 ~ 12,7 ~ 13 and 0.1 ~ 0.3 respectively; In addition, dried fracture strength 〉=1.42cN/dtex, the wet breaking strength 〉=0.64cN/dtex of described regenerated cellulose combustion fat fiber.
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| CN102493208A (en) * | 2011-12-06 | 2012-06-13 | 东华大学 | Preparation method of polynosic fabric with skin caring and calming functions |
| CN103590239A (en) * | 2013-11-20 | 2014-02-19 | 浙江惠侬丝针织内衣有限公司 | Fat-burning essential oil underwear fabric finishing technique |
| CN104005110A (en) * | 2014-05-05 | 2014-08-27 | 江苏金太阳布业有限公司 | Regenerated cellulose fiber containing microencapsulated anti-mite medicine and preparation method thereof |
| CN109056093A (en) * | 2018-08-29 | 2018-12-21 | 中科纺织研究院（青岛）有限公司 | A kind of rosemary cellulose fibre and preparation method thereof |
| CN109518290A (en) * | 2018-10-17 | 2019-03-26 | 罗莱生活科技股份有限公司 | A kind of preparation method of rosemary modified cellulose fibre |
| CN113249964A (en) * | 2021-05-06 | 2021-08-13 | 江苏金太阳纺织科技股份有限公司 | Fat burning and slimming finishing agent for fabric and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102493208A (en) * | 2011-12-06 | 2012-06-13 | 东华大学 | Preparation method of polynosic fabric with skin caring and calming functions |
| CN103590239A (en) * | 2013-11-20 | 2014-02-19 | 浙江惠侬丝针织内衣有限公司 | Fat-burning essential oil underwear fabric finishing technique |
| CN104005110A (en) * | 2014-05-05 | 2014-08-27 | 江苏金太阳布业有限公司 | Regenerated cellulose fiber containing microencapsulated anti-mite medicine and preparation method thereof |
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| CN109056093A (en) * | 2018-08-29 | 2018-12-21 | 中科纺织研究院（青岛）有限公司 | A kind of rosemary cellulose fibre and preparation method thereof |
| CN109518290A (en) * | 2018-10-17 | 2019-03-26 | 罗莱生活科技股份有限公司 | A kind of preparation method of rosemary modified cellulose fibre |
| CN113249964A (en) * | 2021-05-06 | 2021-08-13 | 江苏金太阳纺织科技股份有限公司 | Fat burning and slimming finishing agent for fabric and preparation method thereof |
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