CN102071095A - Cold pressing preparation process for calophyllum inophyllum linn seed oil - Google Patents

Cold pressing preparation process for calophyllum inophyllum linn seed oil Download PDF

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CN102071095A
CN102071095A CN2009101668743A CN200910166874A CN102071095A CN 102071095 A CN102071095 A CN 102071095A CN 2009101668743 A CN2009101668743 A CN 2009101668743A CN 200910166874 A CN200910166874 A CN 200910166874A CN 102071095 A CN102071095 A CN 102071095A
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oil
seed
fine jade
malus spectabilis
drying
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CN102071095B (en
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郑联合
赵阔
王涛
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Hainan Province Gain & Oil Research Institute
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Abstract

The invention relates to a new physical low-temperature cold pressing process for calophyllum inophyllum linn seed oil. The process comprises the steps of airing, peeling, husking, grading, cleaning, removing impurity, slicing kernels, drying at a low temperature, proportioning kernels and husks, crushing, pressing, settling oil, filtering, degumming, and dehydrating to prepare the calophyllum inophyllum linn seed oil serving as a finished product. The process has high oil yield, and is simple, convenient and feasible; the pressing process does not lose nutritional components and active substances in the oil and special fragrance of the calophyllum inophyllum linn seed oil; the refining process does not produce secondary pollution; and the finished product is clear and transparent, and is yellow green to dark green.

Description

一种琼崖海棠籽油的冷榨制备工艺 A kind of cold-pressing preparation process of Tamanya seed oil

一、技术领域1. Technical field

本发明属于植物油脂加工技术领域,适用于琼崖海棠籽的加工。 The invention belongs to the technical field of vegetable oil processing and is suitable for the processing of tamanu seeds. the

二、背景技术2. Background technology

琼崖海棠(Calophyllum inophyllum Linn),又名海棠果、红厚壳、胡桐、海桐、君子树、海棠木,是一种高产的木本油料植物,在我国主要分布于海南、广东、广西、台湾等省区,东南亚、南亚、非洲等热带地区均有。在我国民间,琼崖海棠果被用来治疗眼病、外伤出血、风湿骨痛、跌打损伤等。研究试验表明琼崖海棠籽油中富含呫吨酮类、香豆素衍生物、黄酮类、三萜类及海棠果酸等活性物质,具有促进组织再生、抗神经痛、抗菌、消炎、抗细胞毒素、抗溃疡、抗肝毒素、祛风湿、抗衰老、抗肿瘤、抗白血病、抗艾滋病毒、抑制HIV21逆转录酶、抑制HIV212KT复制等活性。目前,国内关于琼崖海棠籽油活性成分及其作用的研究较多,但是如何制备富含活性成分的琼崖海棠籽油却鲜见报道。琼崖海棠果肉果实的含油率很高,其中果实部分含油25-30%,种仁部分含油48-55%。琼崖海棠籽油中不饱和脂肪酸含量很高,占总脂肪酸的60-75%,其中油酸、亚油酸含量很高。 Qiongya crabapple (Calophyllum inophyllum Linn), also known as crabapple fruit, red thick shell, oregano, Pittosporum, gentleman tree, crabapple wood, is a high-yield woody oil plant, mainly distributed in Hainan, Guangdong, Guangxi in my country , Taiwan and other provinces and regions, Southeast Asia, South Asia, Africa and other tropical regions. In our country, Qiongya crabapple fruit is used to treat eye diseases, traumatic bleeding, rheumatic bone pain, bruises and so on. Research tests have shown that tamanu seed oil is rich in active substances such as xanthones, coumarin derivatives, flavonoids, triterpenoids, and begonia fruit acid, which have the functions of promoting tissue regeneration, anti-neuralgia, antibacterial, anti-inflammatory, and anti-inflammatory. Cytotoxin, anti-ulcer, anti-hepatotoxin, anti-rheumatism, anti-aging, anti-tumor, anti-leukemia, anti-HIV, inhibition of HIV21 reverse transcriptase, inhibition of HIV212KT replication and other activities. At present, there are many domestic studies on the active components of tamanu seed oil and their functions, but there are few reports on how to prepare tamanu seed oil rich in active components. The oil content of Tamanu chinensis pulp is very high, wherein the fruit part contains 25-30% oil, and the kernel part contains 48-55% oil. The content of unsaturated fatty acids in tamanu seed oil is very high, accounting for 60-75% of the total fatty acids, of which oleic acid and linoleic acid are very high. the

三、发明内容3. Contents of the invention

本发明的目的就在于提供一种工艺简单,能耗低,所用加工设备少,成品油中富含天然活性成分,无溶剂残留的琼崖海棠籽油的制备方法。本发明的目的可以通过下述技术措施来实现: The object of the present invention is to provide a method for preparing tamanu seed oil with simple process, low energy consumption, less processing equipment, rich in natural active ingredients in the finished oil, and no solvent residue. The purpose of the present invention can be achieved through the following technical measures:

(1)将收集到的琼崖海棠果晒干,脱皮; (1) the collected Tamanya fruit is dried and peeled off;

(2)将琼崖海棠籽用剥壳机剥壳,将籽仁、籽壳分离; (2) Peel the tamanthus seeds with a sheller, and separate the kernels and shells;

(3)精选优质的琼崖海棠籽仁、籽壳,分别用自来水冲洗,去除黏附在表面的杂质; (3) Select the high-quality Qiong Tay Begonia seed kernels and seed shells, and wash them with tap water to remove impurities adhering to the surface;

(4)将琼崖海棠籽仁切片,与籽壳一并放入烘箱中干燥,干燥温度30℃~60℃,干燥时间8h~25h; (4) Slice the kernels of Tamanya seeds, put them together with the shells in an oven for drying, the drying temperature is 30°C-60°C, and the drying time is 8h-25h;

(5)将干燥后的琼崖海棠籽仁与琼崖海棠籽壳以一定的比例混合,用粉碎机粉碎; (5) Mix the dried Tamanu seed kernels with the Tamanu seed shell in a certain ratio, and pulverize with a pulverizer;

(6)将粉碎后的琼崖海棠籽仁籽壳在常温下直接压榨,用板框过滤机过滤; (6) The crushed Tamanya seeds kernel seed husk is directly squeezed at normal temperature, and is filtered with a plate-and-frame filter;

(7)将毛油加热到30℃~50℃,并将略高于油温的水加入其中,加水量为毛油的1%~25%, 快速搅拌,离心分离,脱去其中胶质; (7) Heat the crude oil to 30°C to 50°C, add water slightly higher than the oil temperature, the amount of water added is 1% to 25% of the crude oil, stir rapidly, and centrifuge to remove the colloid;

(8)将脱胶后的油脂进行真空干燥,脱去其中水分,得到成品琼崖海棠籽油。 (8) Vacuum drying the degummed oil to remove water therein to obtain the finished product Tamanuja seed oil. the

本发明的剥壳工艺使用刀笼剥壳机剥壳,分离工艺采用振动筛与风选机结合分离。The shelling process of the present invention uses a cutter cage shelling machine for shelling, and the separation process adopts a vibrating screen combined with an air separator for separation.

本发明的切片工艺使用切片机切片,使切片厚度控制在0.5mm~5.0mm之间。 The slicing process of the present invention uses a slicer to slice, so that the slice thickness is controlled between 0.5 mm and 5.0 mm. the

本发明的干燥工艺指干燥琼崖海棠籽至含水率0.1%~5%。 The drying process of the invention refers to drying the tamanu seeds to a moisture content of 0.1% to 5%. the

本发明的压榨工艺使用静压式榨油机,压榨压力50~100MPa,压榨时间1h~5h。 The pressing process of the present invention uses a static pressure oil press, the pressing pressure is 50-100 MPa, and the pressing time is 1h-5h. the

本发明的真空干燥工艺,是在真空度为70KPa~110KPa,温度40℃~50℃条件下,真空干燥0.5h~3h。 The vacuum drying process of the present invention is to vacuum dry for 0.5h to 3h under the conditions of a vacuum degree of 70KPa-110KPa and a temperature of 40°C-50°C. the

本发明具有以下特点: The present invention has the following characteristics:

(1)精选优质的琼崖海棠籽,仁壳清洗、除杂,保证了原料质量良好,没有污染,提高榨油品质。 (1) Select high-quality Tamanu seeds, wash the shells and remove impurities to ensure good quality of raw materials without pollution and improve the quality of oil extraction. the

(2)将籽仁切片干燥,确保籽仁干燥均匀,同时缩短了干燥时间,提高工作效率。 (2) Slice and dry the kernels to ensure uniform drying of the kernels, shorten the drying time and improve work efficiency. the

(3)将籽仁与籽壳以一定比例混合压榨,疏通了油的通道,提高了出油率。 (3) The seed kernel and seed shell are mixed and pressed in a certain proportion, which dredges the passage of oil and improves the oil yield. the

(4)采用低温冷榨工艺,整个工艺过程无高温介入,保护了琼崖海棠籽油中的活性成分不被高温破坏。 (4) The low-temperature cold-pressing process is adopted, and there is no high temperature intervention in the whole process, which protects the active ingredients in the tamanu seed oil from being damaged by high temperature. the

(5)工艺过程没有使用任何试剂,保证了琼崖海棠籽油中的活性成分不破坏,不损失,保证了成品油中没有试剂残留。 (5) No reagent is used in the process, which ensures that the active ingredients in the tamanu seed oil are not destroyed or lost, and that no reagent remains in the finished oil. the

(6)精炼工艺简单,成品琼崖海棠籽油呈特有的墨绿色,油脂澄清透明,脱胶和脱水工艺有效提高了油脂品质,延长了琼崖海棠籽油保质期。 (6) The refining process is simple, the finished tamanu seed oil has a unique dark green color, and the oil is clear and transparent. The degumming and dehydration process effectively improves the quality of the oil and prolongs the shelf life of the tamanu seed oil. the

四、具体实施方式4. Specific implementation

为了更加详细地说明本发明,下面用具体的实施例详细说明本发明: In order to illustrate the present invention in more detail, describe the present invention in detail below with specific embodiment:

具体实施方式: Detailed ways:

收集琼崖海棠果,将其晒干,脱皮。将脱皮后的琼崖海棠果送入刀笼剥壳机剥壳,用振动筛与风选机结合将琼崖海棠籽仁与琼崖海棠籽壳分离。将剥壳分离后的琼崖海棠籽仁及琼崖海棠籽壳进行分级,精选优质的琼崖海棠籽仁、籽壳,分别用自来水冲洗,去除黏附在表面的杂质。将挑选好的琼崖海棠籽仁用切片机切片,切片厚度控制在0.5mm~5.0mm之间。将切片好的籽仁与籽壳一并放入烘箱中干燥,干燥温度30℃~60℃,干燥时间8h~25h,干燥至 琼崖海棠籽仁含水率在0.1%~5%之间。将干燥后的琼崖海棠籽仁与琼崖海棠籽壳以一定的比例混合,用粉碎机粉碎。粉碎后送入静压式榨油机在常温下冷榨,压榨压力50~100MPa,压榨时间1h~5h。用板框过滤机过滤毛油,然后将毛油加热到30℃~50℃,并将略高于油温的水加入其中,加水量为毛油的1%~25%,快速搅拌,离心分离,脱去其中胶质。将脱胶后的油脂进行真空干燥,真空度70KPa~110KPa,温度40℃~50℃,干燥时间0.5h~3h,脱去其中水分,得到澄清的墨绿色成品琼崖海棠籽油。附图为冷榨制备工艺的工艺流程图。Tamana fruits are collected, dried and peeled. The peeled tamanu fruit is sent to the cutter cage peeling machine for shelling, and the tamanu seed kernel and the tamanu seed shell are separated by a vibrating screen and a winnowing machine. The peeled and separated tamanu seed kernels and tamanu seed shells are graded, and high-quality tamanu seed kernels and seed shells are selected and washed with tap water to remove impurities adhering to the surface. Slice the selected tamanu seeds with a slicer, and the thickness of the slices is controlled between 0.5 mm and 5.0 mm. Put the sliced kernels and shells into an oven to dry at a drying temperature of 30°C to 60°C and a drying time of 8h to 25h until the moisture content of the tamanu seed kernels is between 0.1% and 5%. The dried tamanu seed kernels are mixed with the tamanu seed shells in a certain ratio, and pulverized by a pulverizer. After being crushed, it is sent to a static pressure oil press for cold pressing at room temperature, with a pressing pressure of 50-100 MPa and a pressing time of 1h-5h. Filter the crude oil with a plate and frame filter, then heat the crude oil to 30°C to 50°C, and add water slightly higher than the oil temperature, the amount of water added is 1% to 25% of the crude oil, stir quickly, and centrifuge , to remove the colloid. The degummed oil is vacuum-dried at a vacuum degree of 70KPa to 110KPa, at a temperature of 40°C to 50°C, and for a drying time of 0.5h to 3h, to remove the water in it, and obtain a clear dark green finished tamanu seed oil. The accompanying drawing is a process flow chart of the cold pressing preparation process.

Claims (7)

1. the cold press preparation technology of a fine jade precipice Malus spectabilis seed oil is characterized in that adopting the low-temperature cold pressing legal system to be equipped with fine jade precipice Malus spectabilis seed oil.
2. the cold press preparation technology of a kind of fine jade according to claim 1 precipice Malus spectabilis seed oil is characterized in that this technology comprises following operation steps:
(1) the fine jade precipice calophyllum inophyllum of collecting is dried decortication;
(2) fine jade precipice Malus spectabilis seed is peeled off with decorticator, seed benevolence, seed shell are separated;
(3) selected fine fine jade precipice Malus spectabilis seed benevolence, seed shell with the tap water flushing, are removed the impurity that is attached on the surface respectively;
(4) with fine jade precipice Malus spectabilis seed benevolence section, to put into baking oven in the lump dry with the seed shell, 30 ℃~60 ℃ of drying temperatures, time of drying 8h~25h;
(5) dried fine jade precipice Malus spectabilis seed benevolence is mixed in certain proportion with fine jade precipice Malus spectabilis seed shell, pulverize with pulverizer;
(6) the directly squeezing at normal temperatures of the fine jade precipice Malus spectabilis seed benevolence seed shell after will pulverizing is filtered with flame filter press;
(7) crude oil is heated to 30 ℃~50 ℃, and will adds wherein a little more than the water of oil temperature, amount of water is 1%~25% of a crude oil, stirs fast, and wherein colloid is sloughed in centrifugation;
(8) grease after will coming unstuck carries out vacuum-drying, sloughs wherein moisture, obtains finished product fine jade precipice Malus spectabilis seed oil.
3. technology according to claim 2 is characterized in that the described technology of peeling off uses bar-cage decorticator to peel off, and separating technology adopts vibratory screening apparatus and winnowing machine in conjunction with separating.
4. technology according to claim 2 is characterized in that described slice process uses the slicing machine section, is controlled between 0.5mm~5.0mm slice thickness.
5. technology according to claim 2 is characterized in that described drying process refers to that dry fine jade precipice Malus spectabilis seed is to water ratio 0.1%~5%.
6. technology according to claim 2 is characterized in that described squeezing process uses the static pressure type oil press zhai, squeeze pressure 50~100MPa, squeezing time 1h~5h.
7. technology according to claim 2 is characterized in that described vacuum drying process, is to be 70KPa~110KPa in vacuum tightness, under 40 ℃~50 ℃ conditions of temperature, and vacuum-drying 0.5h~3h.
CN200910166874A 2009-08-27 2009-08-27 Cold pressing preparation process for calophyllum inophyllum linn seed oil Expired - Fee Related CN102071095B (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107287025A (en) * 2017-08-03 2017-10-24 安徽省雷氏农业科技有限公司 A kind of peony seed oil reparation technology
CN110760383A (en) * 2019-12-10 2020-02-07 海南省粮油科学研究所 A kind of deacidification, decolorization and debittering method of crabapple seed crude oil
CN112210432A (en) * 2019-07-11 2021-01-12 海南省粮油科学研究所 A kind of squeezing method of green kumquat seed oil
CN114874847A (en) * 2022-05-07 2022-08-09 广西壮族自治区林业科学研究院 A kind of original anise seed oil preparation process
CN118064206A (en) * 2023-09-19 2024-05-24 湖南大三湘茶油股份有限公司 A method for rapidly preparing camellia oil
CN119709311A (en) * 2024-12-25 2025-03-28 科奕美(广州)健康产业有限公司 Preparation method and application of cliff begonia seed oil
WO2025105094A1 (en) * 2023-11-13 2025-05-22 株式会社J-オイルミルズ Method for expressing tamanu oil

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CN101225344B (en) * 2007-12-21 2014-06-04 全万平 Vegetable oil low-temperature cold-pressing technique and pressing equipment thereof
CN101497846A (en) * 2008-01-31 2009-08-05 中国热带农业科学院分析测试中心 Method for extracting Calophyllum essential oil constituent

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107287025A (en) * 2017-08-03 2017-10-24 安徽省雷氏农业科技有限公司 A kind of peony seed oil reparation technology
CN112210432A (en) * 2019-07-11 2021-01-12 海南省粮油科学研究所 A kind of squeezing method of green kumquat seed oil
CN110760383A (en) * 2019-12-10 2020-02-07 海南省粮油科学研究所 A kind of deacidification, decolorization and debittering method of crabapple seed crude oil
CN114874847A (en) * 2022-05-07 2022-08-09 广西壮族自治区林业科学研究院 A kind of original anise seed oil preparation process
CN118064206A (en) * 2023-09-19 2024-05-24 湖南大三湘茶油股份有限公司 A method for rapidly preparing camellia oil
WO2025105094A1 (en) * 2023-11-13 2025-05-22 株式会社J-オイルミルズ Method for expressing tamanu oil
CN119709311A (en) * 2024-12-25 2025-03-28 科奕美(广州)健康产业有限公司 Preparation method and application of cliff begonia seed oil

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