CN107287025A - A kind of peony seed oil reparation technology - Google Patents
A kind of peony seed oil reparation technology Download PDFInfo
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- CN107287025A CN107287025A CN201710656677.4A CN201710656677A CN107287025A CN 107287025 A CN107287025 A CN 107287025A CN 201710656677 A CN201710656677 A CN 201710656677A CN 107287025 A CN107287025 A CN 107287025A
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- peony seeds
- peony
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Pretreatment Of Seeds And Plants (AREA)
- Fats And Perfumes (AREA)
Abstract
A kind of peony seed oil reparation technology, including the fresh peony seeds of harvesting are subjected to corruption processing, dried after corruption, shelled after drying and obtain seed shell separating mixture, seed shell separating mixture is screened, classification is freeze-dried, squeezes fuel-displaced step.The inventive method processing time is short, energy consumption is low, save manpower, is conducive to the raising of peony seeds oil content and oil yield, realizes the industrialized production of peony seed oil, can be widely used in peony seeds planting base and peony seed oil manufacturing enterprise.
Description
Technical field
Field is produced the present invention relates to edible oil, and in particular to a kind of peony seed oil reparation technology.
Background technology
Peony seeds are the elite crystallizations of peony plant, and in addition to all characteristics that tree peony has in itself have been passed on, it more has certainly
The medicine and nutritional ingredient of oneself uniqueness, Paeonia suffruticosa seed are the nuts by shell and kind shell double shielding, with natural " longevity "
Gene.Original producton location is located at Heze City, Shandong Province, releases first peony seed oil in the world in 2009, and obtain Shandong Province it is provincial into
Fruit is identified.Table is tested through grease authoritative department Southern Yangtze University and grain and oil quality Supervision Test Center Deng Duojia professional institutions of China
Bright, peony seed oil unsaturated fatty acid content is up to more than 90%, and especially estimable is wherein polyunsaturated fatty acid ---
Leukotrienes (category ω -3 series) content, more than 40%, is 140 times of olive oil.The vegetable oil extracted by peony seeds is that China is peculiar
Woody macadamia nut oil, because its is nutritious and unique, there is medical care effect again, be referred to as by relevant expert " best in the world
Oil ", is the treasure in vegetable oil, new resource food approval is obtained on March 22nd, 2011 (oily and male on approval acer truncatum seed
Red seed oil is used as bulletin (2011 No. 9) People's Republic of China's national health of new resource food and family planning committee member
Meeting).
Current peony seed oil production operation is main after peasant household plucks, accumulated, sun suncrack, seed selection of manually peeling off,
Naturally dry seed, this processing method spends the time long, and labor intensity is big, and chance rainy weather easily goes rotten, and has a strong impact on male
Red seed oil yield and oil quality；Also a small number of processing enterprises carry out high temperature flash baking, this method using dryer to peony seeds
High energy consumption, considerably increases processing cost, and high temperature drying is easily caused the oil yield decline of peony seeds, oil peroxidation, acid number
Rise.Patent document such as Application No. 200910310142.7 is disclosed in a kind of preparation method of peony seed oil, the method
Peony seeds are roasted at a temperature of 80~130 DEG C 30~80 minutes, the oil content and oil yield that peony seeds are not only resulted in decline,
And expend mass energy.The unprocessed unsuitable directly Exposure to Sunlight of fresh peony seeds, it is not easy to crack to be easily caused part fruit, becomes normal
" the dead fruit iron seed " said is, it is necessary to which artificial hammering ability broken shell takes seed.In addition, peony seeds diameter grade size difference is larger, combination drying
Moisture content is extremely uneven afterwards, and the small peony seeds drying of diameter grade is too fast, and moisture content is relatively low, and the big peony seeds of diameter grade are dried slow, contain
Water rate is higher, while being not easy to drying operation, has a strong impact on peony seeds dry mass.
Due to evening utilization time of peony seed oil, existing peony seed oil production technology long preparation period is not suitable for scale
Metaplasia is produced.As peony seed oil produces the expansion of industrialization, the oily processing enterprise of many large edibles faces large quantities of fresh peony seeds
How process problem after centralized purchasing, particularly under the conditions of place and limited personnel, further shorten processing time, improves
Efficiency, it is ensured that peony seeds oil yield and oil quality, it appears very urgent.A kind of people's urgently peony seed oil of the modernization of industry
Reparation technology is processed, to meet the market requirement, the predicament that peony seeds are quickly in high volume processed in enterprise scale is solved.
The content of the invention
Process and above-mentioned defect of the prior art, carry it is an object of the invention to the scale for solving fresh peony seed oil
For a kind of reparation technology of peony seed oil, this method processing time is short, energy consumption is low, save manpower, is conducive to containing for peony seed oil
The raising of oil cut rate and oil yield.
The reparation technology of the peony seeds of the present invention, comprises the following steps：
(1) the fresh peony seeds of harvesting are subjected to corruption processing；
(2) peony seeds for handling corruption well are dried；
(3) dried peony seeds are subjected to processing of shelling, obtain seed, shell separating mixture；
(4) seed, shell separating mixture material are screened, obtains clean peony seeds；
(5) peony seeds for obtaining step (4) are classified；
(6) by the progress freeze-drying process simultaneously at the same level of the peony seeds after classification；
(7) it is placed in three kinds of particle diameter peony seeds after freeze-drying are well mixed magnetic separation refined filtration screw oil expeller and is squeezed
Oil.
Specifically, the process of the corruption processing of peony seeds described in step (1) is：Sprayed on the fresh peony seeds of harvesting rotten
Agent simultaneously stirs, and being fitted into after bamboo weaving large bamboo or wicker basket to be put into corruption room makes shell progressively soften；One basket of dress 30kg peony seeds, every 4
~6 baskets are a pile, and gap is left between heap and heap；It is 20~25 DEG C to degenerate room temperature control, and air humidity is 70~75%, when
Between be 24 hours to 36 hours, corruption be disposed after peony seeds shell soften and separated with fruit.
Specifically, drying uses heated-air drying described in step (2), preferably directly carried out in corruption room, control corruption
Room temperature is 40~45 DEG C, and air humidity is 20~30%, and the time is 12 hours to 24 hours, dries and terminates rear casing and fruit
In moisture removal and make it is case hardening, cracking.
Specifically, peony seeds described in step (3) shell, processing is, is divided peony seeds seed, shell using oscillatory type scourer
From.
Specifically, the progress screening of seed described in step (4), shell separating mixture material is, will be male using revolving drum type screening machine
Impurity in red seed is removed, and obtains clean peony seeds.
Specifically, the classification of peony seeds described in step (5) is divided into Three Estate, respectively one according to peony seeds particle size
Level peony seeds, two grades of peony seeds, three-level peony seeds, one-level peony seeds particle diameter is maximum, and two grades of peony seeds particle diameters take second place, three-level tree peony
Seed footpath is minimum.
Specifically, the freeze-drying process process of peony seeds is described in step (6)：Peony seeds are loaded into bamboo weaving large bamboo or wicker basket simultaneously
It is deposited in refrigerating chamber, one basket fills 10~20kg peony seeds, and every 3~4 baskets are superposed to a pile, and gap is left between heap and heap, cold
Freezer temperature is first down to subzero 5~10 DEG C when lyophilized dry, 10~20 after the hydrogenesis of tree peony seed surface is ice crystal
30~40 DEG C are warming up in minute, the directly distillation of the ice crystal of tree peony seed surface is removed for steam.
Beneficial effects of the present invention are：The present invention by fresh peony seeds carry out corruption processing, drying, shell, seed shell is screened,
And classification drying is carried out to the peony seeds obtained after screening, compared with prior art, principle of the invention and beneficial effect are such as
Under：
(1) implement corruption processing to adopting rear fresh peony seeds, reduce the consumption of the internal limited nutrition thing of fruit, effectively improve
Fruit protein active, prevents that fat content declines in fruit.Peony seeds fruit after harvesting, is still continuing the physiological activation phase,
Appropriate corruption processing can promote the organic matters such as starch and soluble sugar to be converted into grease, improve peony seeds oil yield.Implement this
The preparation technique of invention, peony seeds oil yield can improve more than 5%.
(2) without manually drying and peel off, the problem of both having solved drying place, again for enterprise saved a large amount of labourers into
This, is suitable for the large batch of processing of peony seeds.
(3) industrialized production preparation method of the invention, peony seeds treating capacity is big, is particularly suitable for peony seeds cultivated area big
Planting household or peony seed oil manufacturing enterprise.
(4) peony seeds classification freeze-drying so that moisture content is uniform after peony seeds of different sizes are dried, and drying efficiency is carried
It is high.Moreover, the less peony seeds of particle can save the crushing process after shelling.
(5) present invention process employs oscillatory type scourer and revolving drum type screening machine, and Cong Er Minus have lacked the breakage of peony seeds,
The seed shell efficiency of separation is improved, high-volume is realized and focuses on fresh peony seeds, screens the production line of peony seeds in time.
(6) present invention process method, which is preferably integrated with, adopts rear fresh peony seeds to fuel-displaced state-of-the-art technology is squeezed, and realizes
The industrialized production of peony seeds, can be widely used in peony seeds base and peony seed oil manufacturing enterprise, shorten peony seeds to male
The production cycle of red seed oil, the oil yield and quality of peony seeds are improved and keep, and treating capacity is big.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Embodiment is closed, the present invention is expanded on further.
Embodiment one
Fresh peony seeds 600kg is harvested, concentration the agent aqueous solution is degenerated into for 1% peony seeds, uniform stirring sprays tree peony
Seed, is fitted into bamboo weaving large bamboo or wicker basket, every basket of dress 30kg, and every 4 baskets are a pile, and gap is left between heap and heap；Put after loading bamboo weaving large bamboo or wicker basket
Entering to degenerate in room makes shell progressively soften；It is 20 DEG C to degenerate room temperature control, and air humidity is 70%, and the time is 24 hours, rotten
Peony seeds shell softens and separated with fruit after change is disposed.
And then heated-air drying is directly carried out in corruption room, it is 40 DEG C to control corruption room temperature, and air humidity is 20%,
Time is 12 hours, and heated-air drying terminates the moisture removal in rear casing and fruit and makes case hardening, cracking.
The bamboo weaving large bamboo or wicker basket that will be equipped with peony seeds is removed from corruption room, is divided peony seeds seed, shell using oscillatory type scourer
From.
The impurity in peony seeds is removed using revolving drum type screening machine, clean peony seeds are obtained.
Peony seeds particle size is divided into Three Estate, respectively one-level peony seeds, two grades of peony seeds, three-level peony seeds,
The one-level peony seeds particle diameter is maximum, and two grades of peony seeds particle diameters take second place, and the three-level peony seeds particle diameter is minimum.
Peony seeds after classification are loaded into bamboo weaving large bamboo or wicker basket, one basket fills 10kg peony seeds, and every 3 baskets are superposed to a pile, heap and heap
Between leave gap, be respectively placed in freeze drying chamber and be freeze-dried：It is placed with the freeze-drying room temperature of one-level peony seeds
Subzero 10 DEG C are down to, 40 DEG C were warming up in 10 minutes after the hydrogenesis of tree peony seed surface is ice crystal, by tree peony seed surface
Ice crystal directly distillation removed for steam；The freeze-drying room temperature for being placed with two grades of peony seeds is down to subzero 7 DEG C, treats peony seeds
The hydrogenesis on surface directly distils the ice crystal of tree peony seed surface as steam to be warming up to 35 DEG C in 15 minutes after ice crystal
Remove；The freeze-drying room temperature for being placed with three-level peony seeds is down to subzero 5 DEG C, after the hydrogenesis of tree peony seed surface is ice crystal
30 DEG C were warming up in 20 minutes, the directly distillation of the ice crystal of tree peony seed surface is removed for steam.
It is placed in three kinds of particle diameter peony seeds after freeze-drying is well mixed magnetic separation refined filtration screw oil expeller and is extracted oil.
Embodiment two
Fresh peony seeds 1200kg is harvested, concentration the agent aqueous solution is degenerated into for 1% peony seeds, uniform stirring sprays male
Red seed, is fitted into bamboo weaving large bamboo or wicker basket, every basket of dress 30kg, and every 6 baskets are a pile, and gap is left between heap and heap；Load after bamboo weaving large bamboo or wicker basket
Being put into corruption room makes shell progressively soften；It is 25 DEG C to degenerate room temperature control, and air humidity is 75%, and the time is 36 hours,
Peony seeds shell softens and separated with fruit after corruption is disposed.
And then heated-air drying is directly carried out in corruption room, it is 45 DEG C to control corruption room temperature, and air humidity is 30%,
Time is 24 hours, and heated-air drying terminates the moisture removal in rear casing and fruit and makes case hardening, cracking.
The bamboo weaving large bamboo or wicker basket that will be equipped with peony seeds is removed from corruption room, is divided peony seeds seed, shell using oscillatory type scourer
From.
The impurity in peony seeds is removed using revolving drum type screening machine, clean peony seeds are obtained.
Peony seeds particle size is divided into Three Estate, respectively one-level peony seeds, two grades of peony seeds, three-level peony seeds,
The one-level peony seeds particle diameter is maximum, and two grades of peony seeds particle diameters take second place, and the three-level peony seeds particle diameter is minimum.
Peony seeds after classification are loaded into bamboo weaving large bamboo or wicker basket, one basket fills 15kg peony seeds, and every 3 baskets are superposed to a pile, heap and heap
Between leave gap, be respectively placed in freeze drying chamber and be freeze-dried：It is placed with the freeze-drying room temperature of one-level peony seeds
Subzero 10 DEG C are down to, 40 DEG C were warming up in 10 minutes after the hydrogenesis of tree peony seed surface is ice crystal, by tree peony seed surface
Ice crystal directly distillation removed for steam；The freeze-drying room temperature for being placed with two grades of peony seeds is down to subzero 7 DEG C, treats peony seeds
The hydrogenesis on surface directly distils the ice crystal of tree peony seed surface as steam to be warming up to 35 DEG C in 15 minutes after ice crystal
Remove；The freeze-drying room temperature for being placed with three-level peony seeds is down to subzero 5 DEG C, after the hydrogenesis of tree peony seed surface is ice crystal
30 DEG C were warming up in 20 minutes, the directly distillation of the ice crystal of tree peony seed surface is removed for steam.
It is placed in three kinds of particle diameter peony seeds after freeze-drying is well mixed magnetic separation refined filtration screw oil expeller and is extracted oil.
Same each three parts of quality peony seeds 600kg, 1200kg is weighed respectively, using traditional handicraft (squeezing process), application number
200910310142.7 techniques, present invention process produce peony seed oil, are worked continuously, and record and detect parameters, right
Than data such as following table：
600kg experimental groups
1200kg experimental groups
Remarks：Oil content is surveyed at random by nuclear magnetic resonance oil-containing flowmeter (unit type CNMR-1000) in table
Measure and take obtained by average；
Oil yield calculation formula：Go out weight of oil/fuel-displaced preceding peony seeds gross weight；
Unsaturated fatty acid content is measured using gas chromatography；
Averagely produce the cycle be from raw material to fuel-displaced work continuously during spent total time；
Produce cost and consider the indexs such as time, manpower, energy consumption, equipment attrition and converted.
As a result show, peony seed oil produced using present invention process, oil content, oil yield, unsaturated fatty acid content,
The cycle is averagely produced, the indices such as cost is produced and is superior to control group.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and that described in above-described embodiment and specification is only the present invention
Preference, be not intended to limit the present invention, without departing from the spirit and scope of the present invention, the present invention also have it is various
Changes and improvements, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by institute
Attached claims and its equivalent thereof.
Claims (7)
1. a kind of peony seed oil reparation technology, it is characterised in that this comprises the following steps：
(1) the fresh peony seeds of harvesting are subjected to corruption processing；
(2) peony seeds for handling corruption well are dried；
(3) dried peony seeds are subjected to processing of shelling, obtain seed, shell separating mixture；
(4) seed, shell separating mixture material are screened, obtains clean peony seeds；
(5) peony seeds for obtaining step (4) are classified；
(6) by the progress freeze-drying process simultaneously at the same level of the peony seeds after classification；
(7) it is placed in three kinds of particle diameter peony seeds after freeze-drying are well mixed magnetic separation refined filtration screw oil expeller and is extracted oil.
2. peony seed oil reparation technology as claimed in claim 1, it is characterised in that described in step (1) at peony seeds corruption
The process of reason is：Sprinkling is degenerated agent and stirred on the fresh peony seeds of harvesting, loads and corruption room is put into after bamboo weaving large bamboo or wicker basket
In shell is progressively softened；One basket of dress 30kg peony seeds, every 4~6 baskets are a pile, and gap is left between heap and heap；Degenerate room temperature
Degree control is 20~25 DEG C, and air humidity is 70~75%, and the time is 24 hours to 36 hours, peony seeds after corruption is disposed
Shell softens and separated with fruit.
3. peony seed oil reparation technology as claimed in claim 1, it is characterised in that drying uses hot blast described in step (2)
Dry, directly carried out in corruption room, it is 40~45 DEG C to control corruption room temperature, and air humidity is 20~30%, and the time is 12
Hour, drying the moisture removal terminated in rear casing and fruit simultaneously made case hardening, cracking to 24 hours.
4. peony seed oil reparation technology as claimed in claim 1, it is characterised in that peony seeds described in step (3) shell place
Reason is separated peony seeds seed, shell using oscillatory type scourer.
5. peony seed oil reparation technology as claimed in claim 1, it is characterised in that seed described in step (4), shell separation mixing
Material is carried out screening and is removed the impurity in peony seeds using revolving drum type screening machine, obtains clean peony seeds.
6. peony seed oil reparation technology as claimed in claim 1, it is characterised in that the classification of peony seeds described in step (5) according to
It is divided into Three Estate, respectively one-level peony seeds, two grades of peony seeds, three-level peony seeds, the one-level according to peony seeds particle size
Peony seeds particle diameter is maximum, and two grades of peony seeds particle diameters take second place, and three-level peony seeds particle diameter is minimum.
7. peony seed oil reparation technology as claimed in claim 1, it is characterised in that the freezing of peony seeds described in step (6)
Drying process process is：Peony seeds are fitted into bamboo weaving large bamboo or wicker basket and are deposited in refrigerating chamber, one basket fills 10~20kg peony seeds, every 3
~4 baskets are superposed to a pile, and gap is left between heap and heap, and freezer temperature first is down into subzero 5~10 DEG C during freeze-drying, treated
The hydrogenesis of tree peony seed surface is straight by the ice crystal of tree peony seed surface to be warming up to 30~40 DEG C in 10~20 minutes after ice crystal
Distillation is connect to remove for steam.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710656677.4A CN107287025A (en) | 2017-08-03 | 2017-08-03 | A kind of peony seed oil reparation technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710656677.4A CN107287025A (en) | 2017-08-03 | 2017-08-03 | A kind of peony seed oil reparation technology |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102071095A (en) * | 2009-08-27 | 2011-05-25 | 海南省粮油科学研究所 | Cold pressing preparation process for calophyllum inophyllum linn seed oil |
| CN102433219A (en) * | 2011-10-28 | 2012-05-02 | 江南大学 | Method for graded drying of camellia seeds |
| CN104186649A (en) * | 2014-08-29 | 2014-12-10 | 湖南林之神林韵油茶科技发展有限公司 | Industrial production process method of camellia seeds |
| KR20150109232A (en) * | 2014-03-19 | 2015-10-01 | 초임계연구소 주식회사 | Process for Manufacturing Camellia seed Oil of High Oxidative Stability and Low Color with Supercritical Fluid |
-
2017
- 2017-08-03 CN CN201710656677.4A patent/CN107287025A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102071095A (en) * | 2009-08-27 | 2011-05-25 | 海南省粮油科学研究所 | Cold pressing preparation process for calophyllum inophyllum linn seed oil |
| CN102433219A (en) * | 2011-10-28 | 2012-05-02 | 江南大学 | Method for graded drying of camellia seeds |
| KR20150109232A (en) * | 2014-03-19 | 2015-10-01 | 초임계연구소 주식회사 | Process for Manufacturing Camellia seed Oil of High Oxidative Stability and Low Color with Supercritical Fluid |
| CN104186649A (en) * | 2014-08-29 | 2014-12-10 | 湖南林之神林韵油茶科技发展有限公司 | Industrial production process method of camellia seeds |
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| 王世全，等: "油用紫斑牡丹播种育苗技术", 《农业科技通讯》 * |
| 王宏飞: "牡丹籽榨油工艺研究", 《北京农业》 * |
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