CN102058102B - Industrial production method for efficiently and continuously eluting capsaicin in chilli seed - Google Patents
Industrial production method for efficiently and continuously eluting capsaicin in chilli seed Download PDFInfo
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- CN102058102B CN102058102B CN201010557445.1A CN201010557445A CN102058102B CN 102058102 B CN102058102 B CN 102058102B CN 201010557445 A CN201010557445 A CN 201010557445A CN 102058102 B CN102058102 B CN 102058102B
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Abstract
The invention relates to a method for extracting an active ingredient from a natural product, in particular to an industrial production method for efficiently and continuously eluting capsaicin in chilli seed. The method comprises the following steps of: (1) putting the chilli seed into a closed extractor; (2) continuously adding a polar organic solvent into the extractor to elute the capsaicin in the chilli seed; (3) conveying the chilli seed in which the capsaicin is eluted to a desolvation dryer to remove the solvent so as to obtain the chilli seed without pungency; and (4) concentrating eluent and recovering the solvent to obtain chilli oil resin. By the method, a pungent ingredient contained in the chilli seed can be thoroughly eluted, and the eluted capsaicin can be totally recovered.
Description
Technical field
The present invention relates to the method that effective components from natural materials is extracted, the industrialized preparing process of the wash-out Capsaicin that more specifically says a kind of high-efficiency and continuous from chilli seed.
Background technology
There is abundant pepper resource in China, the production forward development in pluralism of capsicum product.Capsicum processing not only has traditional production of condiments, also comprises the exploitation of capsicum red pigment and the capsaicine with higher economic benefit and social benefit; And the exploitation aspect research of chilli seed that accounts for the about 40-50% of pepper fruit dry weight is fewer.In chilli seed, except containing oil, protein, crude fibre, ash content, also contain a certain amount of Capsaicin; Unrighted acid in chilli seed (being mainly oleic acid and linoleic acid) is playing a very important role aspect body metabolism regulation and control, and the lipid material in adjusting blood, antithrombotic, minimizing cholesterol etc. are had to remarkable result; In chilli seed, also contain several kinds of mineral elements and vitamin, particularly VE content is higher, can cure the disease, diseases prevention and anti-ageing; In chilli seed, also contain the active principles such as phosphatide, polymerization chromolipid, sterol, hydrocarbon and liposoluble vitamin.The chilli seed using in the raw material of luxury food raw material and special use at present cannot get a desired effect because containing Capsaicin, in seed, the existence of Capsaicin has reduced the quality of chilli seed, to client, cause inconvenience, therefore the existence of the pungency component in chilli seed has limited its range of application; The Capsaicin (capsicum oleoresin) extracting from chilli seed both can be widely used in the various seasonings containing peppery food simultaneously, also can be used as the standing seasoning matter of restaurant, dining room, family, can be directly used in the styles of cooking such as culinary art river, Hubei Province, Hunan, especially in pot-stewed meat or fowl and other requirement, can not see raw material and have better effect on food that can be tasty, also having improved the value of chilli seed itself simultaneously.
The patent application that application number is 200910075604.1, name is called a kind of method of capsaicinoids elimination of chilli seeds, discloses the method for a capsaicinoids elimination of chilli seeds, and it adopts heat water-spraying to capsaicinoids elimination of chilli seeds.Although method is simple, poor effect; Pungent, with hot water emission, is not only wasted, and contaminated environment.
Summary of the invention:
In order to overcome the shortcoming of prior art, the industrialized preparing process of the wash-out Capsaicin that the invention provides a kind of high-efficiency and continuous from chilli seed, the pungency component that it not only thoroughly contains in wash-out chilli seed, and can also all reclaim the Capsaicin eluting.
The present invention solves the technical scheme that its technical problem takes: comprise the following steps: 1, the industrialized preparing process of Capsaicin in a kind of high-efficiency and continuous wash-out chilli seed, it is characterized in that: (1), chilli seed is put into continuously in the large-scale airtight continuous extractor of running, temperature is 20-40 ℃; (2) in extractor, add continuously polar organic solvent to elute Capsaicin in chilli seed, organic solvent is methyl alcohol, ethanol or the aqueous acetone solution of concentration 10-60%, simultaneously, and solid-to-liquid ratio is 1: 2-1: 3; (3), elute chilli seed after Capsaicin and be delivered to precipitation drying machine and slough solvent, obtain the chilli seed without pungent; (4), containing Capsaicin polar organic solvent eluent, after concentrated, obtain capsicum oleoresin.
The inventive method has following advantages: 1, technological process is simple, easy operating is controlled, production cost is low; 2, can large-scale continuous production, efficiency is high, and day production capacity can reach more than 100 tons; ; 3, the pungency component thoroughly containing in wash-out chilli seed, and can also all reclaim the Capsaicin eluting; 4, the chilli seed cleanliness factor of producing is high, does not destroy the intrinsic smell of chilli seed.
The specific embodiment
The present invention includes the following step: (1), chilli seed is put into continuously in the large-scale airtight continuous extractor of running, temperature is 20-40 ℃; (2) in extractor, add continuously polar organic solvent to elute Capsaicin in chilli seed, solid-to-liquid ratio is 1: 2-1: 3, simultaneously; (3), elute chilli seed after Capsaicin and be delivered to precipitation drying machine and slough solvent, obtain the chilli seed without pungent; (4), containing Capsaicin polar organic solvent eluent, after concentrated, obtain capsicum oleoresin.Capsicum oleoresin pungent is pure, can meet foodstuff flavouring aspect and use.
Claims (2)
1. an industrialized preparing process for Capsaicin in continuous wash-out chilli seed, is characterized in that: (1), chilli seed is put into continuously in the airtight continuous extractor of running, and temperature is 20-40 ℃; (2) in extractor, add continuously polar organic solvent to elute Capsaicin in chilli seed, solid-to-liquid ratio is 1: 2-1: 3, simultaneously; (3), elute chilli seed after Capsaicin and be delivered to precipitation drying machine and slough solvent, obtain the chilli seed without pungent; (4), containing Capsaicin polar organic solvent eluent, after concentrated, obtain capsicum oleoresin; Described polar organic solvent, refers to that concentration is 10-60% methyl alcohol, ethanol or aqueous acetone solution.
2. a kind of industrialized preparing process of wash-out Capsaicin from chilli seed continuously according to claim 1, is characterized in that: described extractor and precipitation drying machine are pipelining equipment, can produce continuously.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010557445.1A CN102058102B (en) | 2010-11-22 | 2010-11-22 | Industrial production method for efficiently and continuously eluting capsaicin in chilli seed |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010557445.1A CN102058102B (en) | 2010-11-22 | 2010-11-22 | Industrial production method for efficiently and continuously eluting capsaicin in chilli seed |
Publications (2)
| Publication Number | Publication Date |
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| CN102058102A CN102058102A (en) | 2011-05-18 |
| CN102058102B true CN102058102B (en) | 2014-05-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201010557445.1A Active CN102058102B (en) | 2010-11-22 | 2010-11-22 | Industrial production method for efficiently and continuously eluting capsaicin in chilli seed |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104366332B (en) * | 2014-11-17 | 2018-06-15 | 晨光生物科技集团股份有限公司 | A kind of deep working method of chilli seed |
| CN111676091B (en) * | 2020-07-06 | 2023-03-24 | 遵义师范学院 | Chilli seed processing equipment and processing method thereof |
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2010
- 2010-11-22 CN CN201010557445.1A patent/CN102058102B/en active Active
Non-Patent Citations (11)
| Title |
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| 刘蓉等.辣椒红色素提取方法研究进展.《中外食品》.2006,(第06期), |
| 戎志梅.食品色素与香料.《生物化工新产品与新技术开发指南》.化学工业出版社,2004, * |
| 杨博智等.辣椒红色素的提取方法和应用.《辣椒杂志》.2007,(第02期), |
| 牛古丹等.辣椒红色素的提取及稳定性的研究.《化学工程师》.2006,(第05期), |
| 辣椒红色素提取方法研究进展;刘蓉等;《中外食品》;20060615(第06期);55-57 * |
| 辣椒红色素的提取;陈咏梅;《科技信息(科学教研)》;20070920(第25期);321，337 * |
| 辣椒红色素的提取及稳定性的研究;牛古丹等;《化学工程师》;20060528(第05期);60-61 * |
| 辣椒红色素的提取方法和应用;杨博智等;《辣椒杂志》;20070620(第02期);26-29 * |
| 辣椒红色素的研究进展;陶莎等;《食品工业科技》;20080825(第08期);308-309 * |
| 陈咏梅.辣椒红色素的提取.《科技信息(科学教研)》.2007,(第25期), |
| 陶莎等.辣椒红色素的研究进展.《食品工业科技》.2008,(第08期), |
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| CN102058102A (en) | 2011-05-18 |
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