CN102028774A - Antiallergic raspberry composite product and preparation method thereof - Google Patents
Antiallergic raspberry composite product and preparation method thereof Download PDFInfo
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- CN102028774A CN102028774A CN2010105702572A CN201010570257A CN102028774A CN 102028774 A CN102028774 A CN 102028774A CN 2010105702572 A CN2010105702572 A CN 2010105702572A CN 201010570257 A CN201010570257 A CN 201010570257A CN 102028774 A CN102028774 A CN 102028774A
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Abstract
The invention discloses an antiallergic raspberry composite product and a preparation method thereof. A raspberry composite comprises the following original medicament components in part by weight: 20 to 160 parts of raspberry, 10 to 100 parts of fiveleaf gynostemma herb, 10 to 100 parts of champignon and 0.1 to 1 part of ganoderma lucidum spore powder. The preparation method comprises the following steps of: respectively extracting active ingredients of the raspberry, the fiveleaf gynostemma herb and the champignon, and mixing the active ingredients and the ganoderma lucidum spore powder uniformly to obtain the antiallergic raspberry composite; and then adding accessory starch and dextrin auxiliary materials, mixing uniformly by the conventional pharmaceutical method, granulating and preparing into various formulations such as granules, tablets, tea bags, oral liquid and capsules, or preparing into additives of other medicines and foods. The antiallergic raspberry composite product is an antiallergic composite product which has quick response to antianaphylaxis and has better effect.
Description
Technical field:
The invention belongs to Chinese medicine and food technology field, relate to a kind of antiallergic product Fructus Rubi corchorifolii Immaturus complex and preparation method thereof.
Background technology:
Fructus Rubi corchorifolii Immaturus (Rubus Suavissimus S.Lee) is commonly called as Folium hydrangeae strigosae, is Rosaceae rubus perennial plant, is Dayao Mountain, Guangxi district endemic plant, and Yin Qiye has high sweet ingredient and by extensive use among the people, it is cool in nature, nontoxic.Modern pharmacology proves that the polyphenols in the Fructus Rubi corchorifolii Immaturus---ellagitannic acid has the antiallergic effect, safety non-toxic, thereby Fructus Rubi corchorifolii Immaturus becomes the product of the most effective natural anti-pollen hypersensitivity on the Japanese market.
Though Fructus Rubi corchorifolii Immaturus has been applied to antiallergic, but result of use is slow separately, general patient will shift to an earlier date 1～2 month and takes just and produces effect, anaphylactic disease and body immunity are closely bound up, we are through making great efforts for many years, utilize Chinese medicine compound recipe guideline, with the Fructus Rubi corchorifolii Immaturus is primary raw material, be equipped with the Herb Gynostemmae Pentaphylli, Lentinus Edodes, the Ganoderma spore powder that improve body immunity, extract through science composite, develop have rapid-action, the significant complex antiallergic of antiallergic effect product, and prove that through pharmacology pharmacodynamic its antiallergic effect is suitable with the dexamethasone acetate effect.
Summary of the invention:
The objective of the invention is: provide a kind of antiallergic rapid-action, the significant antiallergic product of effect Fructus Rubi corchorifolii Immaturus complex and preparation method thereof.
Technical scheme of the present invention is:
The Fructus Rubi corchorifolii Immaturus complex comprises that Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder are mixed in proportion the antiallergic product that obtains.
Described Fructus Rubi corchorifolii Immaturus extract is to adopt water extracting method to obtain extract from the Fructus Rubi corchorifolii Immaturus cured leaf, and by macroporous resin adsorption, ethanol elution is isolated Fructus Rubi corchorifolii Immaturus elladitannin acids polyphenol substance.
Described Herb Gynostemmae Pentaphylli extract is to adopt decoction and alcohol sedimentation technique to obtain to contain gypenoside class material from Herb Gynostemmae Pentaphylli.
Described Lentinus Edodes extract adopts decoction and alcohol sedimentation technique to obtain to contain lentinan class material from Lentinus Edodes.
Described Ganoderma spore powder is market purchasing.
Product of the present invention is Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder to be mixed in proportion obtain antiallergic tcm product Fructus Rubi corchorifolii Immaturus complex, adds that supplementary product starch, dextrin etc. are made into various dosage forms such as dissolved granule, capsule, tablet or as the additive of other medicines and food.
The former medicine and the property of medicine that the Fructus Rubi corchorifolii Immaturus complex adopts are respectively:
Fructus Rubi corchorifolii Immaturus (Rubus Suavissimus S.Lee) is commonly called as Folium hydrangeae strigosae, is Rosaceae rubus perennial plant, is Dayao Mountain, Guangxi district endemic plant, and Yin Qiye has high sweet ingredient and by extensive use among the people, it is cool in nature, nontoxic.Modern pharmacology proves that the polyphenols ellagitannic acid in the Fructus Rubi corchorifolii Immaturus has the antiallergic effect, safety non-toxic,
Herb Gynostemmae Pentaphylli: soap was sweet during Herb Gynostemmae Pentaphylli contained more than 80, comprised Radix Ginseng soap former times Rg3, the acid of hydrogen base, 23 kinds of inorganic elementss, sweet in the mouth, property is flat, heat-clearing and toxic substances removing is arranged, eliminating phlegm and stopping cough, supplementing QI and nourishing YIN, anticancer, anti-old, the function of blood fat reducing, it is vexed to be used for the treatment of the chest painful abdominal mass, stagnation of phlegm blood ripple, shortness of breath and palpitation, dizziness and headache, forgetful ear toot, unconsciously sweat and tire, hyperlipidemia, Simple Obesity, old cough.
Lentinus Edodes: the fragrant letter of Lentinus Edodes another name, Lentinus Edodes contains lentinan, and property is sweet, flat, stomach reinforcing gas, and the holder varioliform exanthema is controlled the wind removing blood stasis, and phlegm-eliminiating and qi-regulating is the vitamin compensation.Be used for the treatment of toxic plant poisoning, treating measles, hypertension, edema, headache, dizziness, the weak and avitaminosis of health.
Ganoderma spore: Ganoderma spore contains several amino acids, calms the nerves, and protects god, goes into the heart being responsible for production of blood, help the heart to fill arteries and veins, the liver benefiting, lung, spleen, anti-cancer antitumor, anti-radiation, prevent hepatitis, heart tonifying, coordinate the human body metabolism, life lengthening prevents old age that ' dementia disease has certain curative effect.
The present invention is achieved in that
Antiallergic product Fructus Rubi corchorifolii Immaturus complex, be Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder to be mixed in proportion obtain antiallergic product Fructus Rubi corchorifolii Immaturus complex, add perhaps that supplementary product starch, dextrin etc. are made into various dosage form tcm products such as dissolved granule, capsule, tablet or as the additive of other medicines and food, the former medicine component and the parts by weight thereof of Fructus Rubi corchorifolii Immaturus complex are: 0.1～1 part of 20～160 parts of Fructus Rubi corchorifolii Immaturuss, 10～100 parts of Herb Gynostemmae Pentaphylli, 10～100 parts on Lentinus Edodes and Ganoderma spore powder.
The former medicine component and the parts by weight thereof of above-described Fructus Rubi corchorifolii Immaturus complex are: 0.25 part of 50 parts of Fructus Rubi corchorifolii Immaturuss, 25 parts of Herb Gynostemmae Pentaphylli, 20 parts on Lentinus Edodes and Ganoderma spore powder.
The preparation method of above-described antiallergic product Fructus Rubi corchorifolii Immaturus complex is:
1, in reaction pot, adds the Fructus Rubi corchorifolii Immaturus that takes by weighing by former medicine component and parts by weight thereof, add the water extraction secondary, each amount of water is 10～13 times of Fructus Rubi corchorifolii Immaturus parts by weight, be incubated 0.5～1.5 hour behind the water boil, filter, filtrate is by DM101 absorption with macroporous adsorbent resin and washing, and mother solution and water lotion are 500～30000 daltonian organic membrane ultrafiltration and concentration by twice molecular weight, and trapped fluid is standby after concentrated, drying and pulverizing obtain elladitannin acids polyphenol substance.
2, in reaction pot, add the Herb Gynostemmae Pentaphylli that takes by weighing by former medicine component and parts by weight thereof, the extracting in water secondary, add water at every turn and be 10～13 times of Herb Gynostemmae Pentaphylli parts by weight, be incubated 1～2 hour behind the water boil, filter, filtrate is condensed into the thick paste that filtrate is condensed into proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, reach 50～60% until the solution concentration of alcohol, staticly settled 24～48 hours, filter, filtrate recycling ethanol, it is standby that concentrated, dry and pulverizing obtains to contain gypenoside class material.
3, add the Lentinus Edodes that takes by weighing by former medicine component and parts by weight thereof in reaction pot, the extracting in water secondary adds water at every turn and is 18～22 times of Herb Gynostemmae Pentaphylli parts by weight, be incubated 1～2 hour behind the water boil, filter, filtrate is condensed into thick paste, proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 50～60% until the solution concentration of alcohol, staticly settles 24～48 hours, filter and take out precipitate, it is standby that concentrated, dry and pulverizing obtains to contain lentinan class material.
4, take by weighing Ganoderma spore powder by former medicine component and parts by weight thereof, standby.
5,, get antiallergic tcm product Fructus Rubi corchorifolii Immaturus complex with Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder mix homogeneously.Add 0.6 part of adjuvant water soluble starch, 0.6 part of maltodextrin adopts conventional pharmaceutical methods mix homogeneously, granulates, and makes antiallergic product such as dissolved granule, capsule, tablet, oral liquid or as the additive of other medicines and food.
Above-described reaction pot comprises rustless steel or enamelled reactor or retort.
Advantage of the present invention and good effect:
Modern pharmacology proves, polyphenols ellagitannic acid in the Fructus Rubi corchorifolii Immaturus has the antiallergic effect, safety non-toxic, thereby Fructus Rubi corchorifolii Immaturus becomes the product of the most effective natural anti-pollen hypersensitivity on the Japanese market, but separately result of use is slow, and general patient will shift to an earlier date 1～2 month and takes just and produces effect.The present invention utilizes Chinese medicine compound recipe guideline, with the Fructus Rubi corchorifolii Immaturus is primary raw material, be equipped with the Herb Gynostemmae Pentaphylli, Lentinus Edodes, the Ganoderma spore powder that improve body immunity, extract composite through science, make the various dosage forms of dissolved granule, tablet, teabag, oral liquid and capsule or as the additive of other medicines and food, it is rapid-action to have antiallergic, is antiallergic effect composite product preferably.Prove that through pharmacology pharmacodynamic its antiallergic effect is suitable with the dexamethasone acetate effect.
Description of drawings:
Fig. 1 is a process chart of the present invention.
The specific embodiment:
Embodiment 1:
Former medicine component and parts by weight thereof are:
0.25 part of 50 parts of Fructus Rubi corchorifolii Immaturuss, 25 parts of Herb Gynostemmae Pentaphylli, 20 parts on Lentinus Edodes and Ganoderma spore powder.
Preparation method is:
1, in enamel reaction still, adds Fructus Rubi corchorifolii Immaturus, add the water extraction secondary, add water is 600 parts at every turn, be incubated 0.5～1 hour behind the water boil, filter, filtrate is by DM101 absorption with macroporous adsorbent resin and washing, and liquid mother solution and water lotion are by twice organic membrane ultrafiltration and concentration, and trapped fluid is standby after concentrated, dry and pulverizing.
2, in enamel reaction still, add Herb Gynostemmae Pentaphylli, the extracting in water secondary, add water is 300 parts at every turn, be incubated 1.5～2 hours behind the water boil, filter, filtrate is condensed into thick paste, proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 55% until the solution concentration of alcohol, staticly settled 48 hours, filter, filtrate recycling ethanol concentrates, dry and pulverize standby.
3, in enamel reaction still, add Lentinus Edodes, the extracting in water secondary, add water is 400 parts at every turn, be incubated 1～1.5 hour behind the water boil, filter, filtrate is condensed into thick paste, proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 50% until the solution concentration of alcohol, staticly settles 48 hours, filter to take out precipitate, concentrate, dry and pulverize standby.
4, take by weighing Ganoderma spore powder by former medicine component and parts by weight thereof, standby.
5,, get antiallergic tcm product Fructus Rubi corchorifolii Immaturus complex with Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder mix homogeneously.Add 0.6 part of adjuvant water soluble starch then, 0.6 part of maltodextrin adopts conventional pharmaceutical methods mix homogeneously, granulates, and makes dissolved granule antiallergic tcm product.
Embodiment 2:
Former medicine component and parts by weight thereof are:
0.5 part of 80 parts of Fructus Rubi corchorifolii Immaturuss, 50 parts of Herb Gynostemmae Pentaphylli, 50 parts on Lentinus Edodes and Ganoderma spore powder.
Preparation method is:
1, in stainless steel cauldron, adds Fructus Rubi corchorifolii Immaturus, add the water extraction secondary, add water is 1000 parts at every turn, insulation is 1 hour behind the water boil, filter, filtrate is by DM101 absorption with macroporous adsorbent resin and washing, and liquid mother solution and water lotion are by twice organic membrane ultrafiltration and concentration, and trapped fluid is standby after concentrated, dry and pulverizing.
2, in stainless steel cauldron, add Herb Gynostemmae Pentaphylli, the extracting in water secondary, add water is 600 parts at every turn, insulation is 1.5 hours behind the water boil, filters, and filtrate is condensed into thick paste, proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 50% until the solution concentration of alcohol, staticly settled 48 hours, filter, filtrate recycling ethanol concentrates, dry and pulverize standby.
3, in stainless steel cauldron, add Lentinus Edodes, the extracting in water secondary, add water is 700 parts at every turn, insulation is 1 hour behind the water boil, filter, filtrate is condensed into thick paste, proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 60% until the solution concentration of alcohol, staticly settles 48 hours, filter to take out precipitate, concentrate, dry and pulverize standby.
4, take by weighing Ganoderma spore powder by former medicine component and parts by weight thereof, standby.
5,, get antiallergic tcm product Fructus Rubi corchorifolii Immaturus complex with Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder mix homogeneously.Add 0.6 part of adjuvant water soluble starch then, 0.6 part of maltodextrin adopts conventional pharmaceutical methods mix homogeneously, and tabletting is made tablet antiallergic tcm product.
Embodiment 3:
Former medicine component and parts by weight thereof are:
0.8 part of 30 parts of Fructus Rubi corchorifolii Immaturuss, 40 parts of Herb Gynostemmae Pentaphylli, 60 parts on Lentinus Edodes and Ganoderma spore powder.
Preparation method is:
1, in the stainless steel reaction jar, adds Fructus Rubi corchorifolii Immaturus, add the water extraction secondary, add water is 800 parts at every turn, be incubated 1～1.5 hour behind the water boil, filter, filtrate is by DM101 absorption with macroporous adsorbent resin and washing, and liquid mother solution and water lotion are by twice organic membrane ultrafiltration and concentration, and trapped fluid is standby after concentrated, dry and pulverizing.
2, in the stainless steel reaction jar, add Herb Gynostemmae Pentaphylli, the extracting in water secondary, add water is 400 parts at every turn, insulation is 1.5 hours behind the water boil, filters, and filtrate is condensed into thick paste, proportion 1.10～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 60% until the solution concentration of alcohol, staticly settled 48 hours, filter, filtrate recycling ethanol concentrates, dry and pulverize standby.
3, in the stainless steel reaction jar, add Lentinus Edodes, the extracting in water secondary, add water is 500 parts at every turn, be incubated 1～1.5 hour behind the water boil, filter, filtrate is condensed into thick paste, proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 60% until the solution concentration of alcohol, staticly settles 48 hours, filter to take out precipitate, concentrate, dry and pulverize standby.
4, take by weighing Ganoderma spore powder by former medicine component and parts by weight thereof, standby.
5, with Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder mix homogeneously, get antiallergic tcm product Fructus Rubi corchorifolii Immaturus complex, adopt conventional pharmaceutical methods then, make capsule antiallergic tcm product.
Claims (4)
1. antiallergic product Fructus Rubi corchorifolii Immaturus complex, it is characterized in that: Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract and Ganoderma spore powder are mixed in proportion obtain antiallergic tcm product Fructus Rubi corchorifolii Immaturus complex, add perhaps that supplementary product starch, dextrin adjuvant are made into dissolved granule, capsule, the various dosage form tcm products of tablet or as the additive of other medicines and food, the former medicine component and the parts by weight thereof of Fructus Rubi corchorifolii Immaturus complex are: 0.1～1 part of 20～160 parts of Fructus Rubi corchorifolii Immaturuss, 10～100 parts of Herb Gynostemmae Pentaphylli, 10～100 parts on Lentinus Edodes and Ganoderma spore powder.
2. antiallergic product Fructus Rubi corchorifolii Immaturus complex according to claim 1 is characterized in that: the former medicine component and the parts by weight thereof of described Fructus Rubi corchorifolii Immaturus complex are: 0.25 part of 50 parts of Fructus Rubi corchorifolii Immaturuss, 25 parts of Herb Gynostemmae Pentaphylli, 20 parts on Lentinus Edodes and Ganoderma spore powder.
3. the preparation method of antiallergic product Fructus Rubi corchorifolii Immaturus complex according to claim 1, it is characterized in that: preparation technology is operating as:
(1) in reaction pot, adds the Fructus Rubi corchorifolii Immaturus that takes by weighing by former medicine component and parts by weight thereof, add the water extraction secondary, each amount of water is 10～13 times of Fructus Rubi corchorifolii Immaturus parts by weight, be incubated 0.5～1.5 hour behind the water boil, filter, filtrate is by DM101 absorption with macroporous adsorbent resin and washing, and mother solution and water lotion are by twice organic membrane ultrafiltration and concentration, and trapped fluid obtains elladitannin acids polyphenol substance after concentrated, dry and pulverizing standby;
(2) add the Herb Gynostemmae Pentaphylli that takes by weighing by former medicine component and parts by weight thereof in reaction pot, the extracting in water secondary adds water at every turn and is 10～13 times of Herb Gynostemmae Pentaphylli parts by weight, be incubated 1～2 hour behind the water boil, filter, filtrate is condensed into the thick paste of proportion 1.1～1.15, slowly adds 95% ethanol, the limit edged stirs, reach 50～60% until the solution concentration of alcohol, staticly settled 24～48 hours, filter, filtrate recycling ethanol, it is standby that concentrated, dry and pulverizing obtains to contain gypenoside class material;
(3) add the Lentinus Edodes that takes by weighing by former medicine component and parts by weight thereof in reaction pot, the extracting in water secondary adds water at every turn and is 18～22 times of Herb Gynostemmae Pentaphylli parts by weight, be incubated 1～2 hour behind the water boil, filter, filtrate is condensed into thick paste, proportion 1.1～1.15, slowly add 95% ethanol, the limit edged stirs, and reaches 50～60% until the solution concentration of alcohol, staticly settles 24～48 hours, filter and take out precipitate, it is standby that concentrated, dry and pulverizing obtains to contain lentinan class material;
(4) take by weighing Ganoderma spore powder by former medicine component and parts by weight thereof, standby;
(5) with Fructus Rubi corchorifolii Immaturus extract, Herb Gynostemmae Pentaphylli extract, Lentinus Edodes extract, Ganoderma spore powder mix homogeneously, get antiallergic tcm product Fructus Rubi corchorifolii Immaturus complex, perhaps add 0.6 part of adjuvant water soluble starch, 0.6 part of maltodextrin, adopt conventional pharmaceutical methods mix homogeneously, granulate, make antiallergic tcm product such as dissolved granule, capsule, tablet, oral liquid or as the additive of other medicines and food.
4. the preparation method of antiallergic product Fructus Rubi corchorifolii Immaturus complex according to claim 3 is characterized in that: the reaction pot that is adopted comprises rustless steel or enamelled reactor or retort.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103948705A (en) * | 2014-03-18 | 2014-07-30 | 广西俊宁百康生物科技有限公司 | Antiallergy composition and its preparation method |
| US20140343135A1 (en) * | 2011-05-12 | 2014-11-20 | Universidad De Costa Rica | Method for obtaining an extract rich in ellagic acid tannins from fruits that contain these compounds, and resulting extract |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1296779A (en) * | 2000-11-27 | 2001-05-30 | 湖南省凤凰绿色食品有限公司 | Health-care sobering-up carambola juice beverage |
| CN101120706A (en) * | 2007-08-02 | 2008-02-13 | 史涛涛 | Tea for morning-getting-up health-preserving |
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- 2010-12-02 CN CN2010105702572A patent/CN102028774A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1296779A (en) * | 2000-11-27 | 2001-05-30 | 湖南省凤凰绿色食品有限公司 | Health-care sobering-up carambola juice beverage |
| CN101120706A (en) * | 2007-08-02 | 2008-02-13 | 史涛涛 | Tea for morning-getting-up health-preserving |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20140343135A1 (en) * | 2011-05-12 | 2014-11-20 | Universidad De Costa Rica | Method for obtaining an extract rich in ellagic acid tannins from fruits that contain these compounds, and resulting extract |
| US10278949B2 (en) * | 2011-05-12 | 2019-05-07 | Universidad De Costa Rica | Method for obtaining an extract rich in ellagic acid tannins from fruits that contain these compounds, and resulting extract |
| CN103948705A (en) * | 2014-03-18 | 2014-07-30 | 广西俊宁百康生物科技有限公司 | Antiallergy composition and its preparation method |
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Application publication date: 20110427 |