CN101986076A - 带浆料喷射系统的球磨回转炉及其应用 - Google Patents
带浆料喷射系统的球磨回转炉及其应用 Download PDFInfo
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- CN101986076A CN101986076A CN 201010569548 CN201010569548A CN101986076A CN 101986076 A CN101986076 A CN 101986076A CN 201010569548 CN201010569548 CN 201010569548 CN 201010569548 A CN201010569548 A CN 201010569548A CN 101986076 A CN101986076 A CN 101986076A
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- ball milling
- rotary furnace
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- pulp jets
- milling rotary
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- 239000002002 slurry Substances 0.000 title claims abstract description 64
- 238000000498 ball milling Methods 0.000 title claims abstract description 63
- 239000000843 powder Substances 0.000 claims abstract description 20
- 238000007669 thermal treatment Methods 0.000 claims description 13
- 238000001816 cooling Methods 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 8
- 230000001681 protective effect Effects 0.000 claims description 5
- 238000002347 injection Methods 0.000 claims description 4
- 239000007924 injection Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 15
- 238000007599 discharging Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 description 15
- 238000000034 method Methods 0.000 description 11
- 239000002245 particle Substances 0.000 description 11
- 238000001035 drying Methods 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- 238000003801 milling Methods 0.000 description 4
- 229910010707 LiFePO 4 Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000001354 calcination Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 230000001360 synchronised effect Effects 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000002389 environmental scanning electron microscopy Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229940116007 ferrous phosphate Drugs 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910000155 iron(II) phosphate Inorganic materials 0.000 description 1
- SDEKDNPYZOERBP-UHFFFAOYSA-H iron(ii) phosphate Chemical compound [Fe+2].[Fe+2].[Fe+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O SDEKDNPYZOERBP-UHFFFAOYSA-H 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910001386 lithium phosphate Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- TWQULNDIKKJZPH-UHFFFAOYSA-K trilithium;phosphate Chemical compound [Li+].[Li+].[Li+].[O-]P([O-])([O-])=O TWQULNDIKKJZPH-UHFFFAOYSA-K 0.000 description 1
- 239000012498 ultrapure water Substances 0.000 description 1
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Abstract
Description
批号 | D97(μm) | 放电(mAh/g) | 容量损失(%) |
本方法 | 5 | 152.5 | 3.25 |
常规方法 | 30 | 139.0 | 7.39 |
喷雾干燥/球磨回转炉 | 使用带喷射系统的球磨回转炉 | |
能源消耗 | 350KW | 150KW |
管理成本 | 3000元/天 | 1500元/天 |
效 率 | 2 吨/天 | 4 吨/天 |
降本节支 | / | 比上法节约5000元/吨成本 |
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201010569548A CN101986076B (zh) | 2010-12-02 | 2010-12-02 | 带浆料喷射系统的球磨回转炉及其应用 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201010569548A CN101986076B (zh) | 2010-12-02 | 2010-12-02 | 带浆料喷射系统的球磨回转炉及其应用 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101986076A true CN101986076A (zh) | 2011-03-16 |
CN101986076B CN101986076B (zh) | 2012-10-10 |
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CN201010569548A Expired - Fee Related CN101986076B (zh) | 2010-12-02 | 2010-12-02 | 带浆料喷射系统的球磨回转炉及其应用 |
Country Status (1)
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CN (1) | CN101986076B (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103464082A (zh) * | 2013-01-31 | 2013-12-25 | 宜昌市三峡天润纳米材料工程技术研究中心有限公司 | 一种纳米粉体材料制备系统 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2098054A (en) * | 1935-11-23 | 1937-11-02 | Du Pont | Ball mill attack of titaniferous ores |
JPH01167580A (ja) * | 1987-12-22 | 1989-07-03 | Toshiba Corp | マイクロ波加熱処理装置 |
CN101186289A (zh) * | 2006-11-17 | 2008-05-28 | 喻维杰 | 一种真空回转窑生产磷酸铁锂材料的工艺方法 |
CN201407891Y (zh) * | 2009-05-19 | 2010-02-17 | 恒正科技(苏州)有限公司 | 球磨回转炉 |
CN101671012A (zh) * | 2009-10-13 | 2010-03-17 | 恒正科技(苏州)有限公司 | 电化学活性材料的制造方法 |
CN201876104U (zh) * | 2010-12-02 | 2011-06-22 | 恒正科技(苏州)有限公司 | 带浆料喷射系统的球磨回转炉 |
-
2010
- 2010-12-02 CN CN201010569548A patent/CN101986076B/zh not_active Expired - Fee Related
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2098054A (en) * | 1935-11-23 | 1937-11-02 | Du Pont | Ball mill attack of titaniferous ores |
JPH01167580A (ja) * | 1987-12-22 | 1989-07-03 | Toshiba Corp | マイクロ波加熱処理装置 |
CN101186289A (zh) * | 2006-11-17 | 2008-05-28 | 喻维杰 | 一种真空回转窑生产磷酸铁锂材料的工艺方法 |
CN201407891Y (zh) * | 2009-05-19 | 2010-02-17 | 恒正科技(苏州)有限公司 | 球磨回转炉 |
CN101671012A (zh) * | 2009-10-13 | 2010-03-17 | 恒正科技(苏州)有限公司 | 电化学活性材料的制造方法 |
CN201876104U (zh) * | 2010-12-02 | 2011-06-22 | 恒正科技(苏州)有限公司 | 带浆料喷射系统的球磨回转炉 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103464082A (zh) * | 2013-01-31 | 2013-12-25 | 宜昌市三峡天润纳米材料工程技术研究中心有限公司 | 一种纳米粉体材料制备系统 |
CN103464082B (zh) * | 2013-01-31 | 2015-09-09 | 宜昌市三峡天润纳米材料工程技术研究中心有限公司 | 一种纳米粉体材料制备系统 |
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CN101986076B (zh) | 2012-10-10 |
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