CN101978851B - Three-in-one multifunctional premixed liquid feed and preparation method thereof - Google Patents

Three-in-one multifunctional premixed liquid feed and preparation method thereof Download PDF

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Publication number
CN101978851B
CN101978851B CN2010102555815A CN201010255581A CN101978851B CN 101978851 B CN101978851 B CN 101978851B CN 2010102555815 A CN2010102555815 A CN 2010102555815A CN 201010255581 A CN201010255581 A CN 201010255581A CN 101978851 B CN101978851 B CN 101978851B
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multifunctional
premixed
vitamin
liquid feed
premixed liquid
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CN101978851A (en
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丛方地
苏永鹏
王洪杰
姜云鹏
黄健
刘志辉
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Great Biology Pharmaceutical Tianjin Co Ltd
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Great Biology Pharmaceutical Tianjin Co Ltd
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Abstract

The invention relates to a three-in-one multifunctional premixed liquid feed and a preparation method thereof. The feed is a stable liquid premixed feed which is prepared by organically matching three main functional components such as vitamins, amino acid and linoleic acid by utilizing an emulsifier and an auxiliary emulsifier. In the feed and the preparation method, fat- soluble vitamins and the linoleic acid can be dispersed effectively by mixing surfactants Tween 80, Tween 80 and the auxiliary emulsifier, and simultaneously alkaline amino acid solution also contributes to pre-dispersing vitamin B2; and uniform, stable and clarified three-in-one premixed liquid is obtained by mutual fusion.

Description

Three-in-one multifunctional premixed liquid feed and preparation method thereof
Technical field
The invention belongs to the multi-functional premixed feed of multicomponent field, especially a kind of three-in-one multifunctional premixed liquid feed and preparation method thereof.
Technical background
Along with the development of aquaculture, the cultivation scale continues to increase, and is prevention and treatment livestock and poultry, a large amount of veterinary drugs and additive are abused, had a strong impact on the quality of product, for adapting to sustainable expanding economy pattern, green safety medicine for animals and additive are the inexorable trends of veterinary drug development.Under these circumstances, some green bioactive materials become the important alternative of veterinary drug industry research and development new product, such as vitamin, amino acid, linoleic acid etc.They are the indispensable feed adding components of animal health growth.Above-mentioned three effective constituents are dispersed in the same system, obtain homogeneous, stable multifunctional liquid premixed feed and will be that aquaculture develops in a healthy way is necessary.
Vitamin, that animal is kept the organic compound that normal physiological function must be gone up, has important regulating action for the metabolic activity in the body, vitamin can be by regulating metabolism, promote growth, strengthen animal disease resistant and anti-emergency capability, although the needs to vitamin are micro-, but human body itself is difficult to synthesize the vitamin of capacity, and the content in the feed also is limited, can not satisfy aquaculture for institute's feeding animals fast, the needs of healthy growth, therefore, to contain multivitamin premixed feed imperative in preparation.Vitamin is by regulating the metabolic process of animal, strengthens animal physique, disease-resistant, anti-ly meets an urgent need, fattens, improves self quality etc.Vitamin A can be regulated the liver metabolism function, makes livestock and poultry energetic, honey stomach.Vitamin D can strengthen the animal products of animal products skeleton development, particularly Fast Growth, is very essential.Vitamin E can strengthen the anti-emergency capability of animal, improves the laying rate of laying hen; Vitamin K can be regulated blood circulation system, has the sterilization and anticorrosion function; Cobastab can anti-inflammatory, improves the exterior quality of bird.
Amino acid can replenish Animal nutrition, the balance protein metabolism.Lysine, methionine can improve the utilization rate of feed, promote growth of animal, improve the meat of livestock and poultry, and lysine can also promote small intestine for calcareous absorption, and less domestic animals diarrhoea strengthens renal function.Tryptophan can strengthen disease-resistant, the anti-emergency capability of livestock and poultry.Threonine grows, strengthens and fatten, stimulate the secretion of milk the fowl poultry, and laying eggs all has obvious facilitation.Must amino acid can supplement the nutrients, the balance metabolism, improve efficiency of feed utilization, growth promotion, anti-ly meet an urgent need, improve the effect such as nutritional quality, the aqueous solution ratio that is prepared into comparatively speaking homogeneous is easier to, but one is the premixed goods that only contain aminoacid ingredient.The linoleic acid element has the immunologic function that strengthens livestock and poultry, reduce fat content, improve meat, improve the effects such as the output of milk and the quality of laying eggs, can improve the immunocompetence of livestock and poultry animal, and can reduce fat content, improve meat, improve the output of milk of milk cow, the accumulation of linoleic acid in animal products, improve the nutritive value of product, be of value to healthy diet.But effective cooperation of three effective constituents also is prepared into the multifunctional liquid premixed feed of homogeneous, and it is desired to be that aquaculture develops in a healthy way.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art part, three-in-one multifunctional premixed liquid feed that provide a kind of homogeneous, stablize, accelerate rate of dispersion, easily absorbs and preparation method thereof.
The present invention realizes that the technical scheme of purpose is:
A kind of three-in-one multifunctional premixed liquid feed, its constituent and parts by weight are as follows:
Vitamin 6-15
Amino acid 8-20
Linoleic acid 6-12
Surfactant 20-30
Assistant for emulsifying agent 8-12
Stabilizing agent 4-5
Inorganic salts 2-3
Water 30-50.
And described vitamin comprises vitamin A. D. E, B 2In one or more mixture.
And described amino acid comprises one or more the mixture in methionine, lysine, tryptophan, the threonine.
And described surfactant is one or more mixture in Tween 80, department class 80, the sucrose fatty ester etc.
And described assistant for emulsifying agent is one or more the mixture in propane diols, ethylene glycol, glycerine, the propyl alcohol.
And described stabilizing agent is one or more the mixture among cyclodextrin, xanthans, the CMC.
And described inorganic salts are one or more the mixture in sodium chloride, the sodium pyrophosphate.
And also bag expands auxiliary reagent.
And described auxiliary reagent is sucrose.
A kind of preparation method of three-in-one multifunctional liquid premixed feed, preparation process is as follows:
(1) in part water, add inorganic salts, hold over night is also filtered, at dissolved in filtrate amino acid, water soluble vitamin, the solution 1 of hold over night;
(2) part water, part surface activating agent, assistant for emulsifying agent are mixed, then add liposoluble vitamin, cross colloid mill, get solution 2;
(3) in part water, add stabilizing agent, then mix with part surface activating agent, assistant for emulsifying agent, linoleic mixed liquor, get solution 3;
(4) above-mentioned molten 1,2,3 liquid are mixed, and cross the three-in-one multifunctional liquid premixed feed of colloid mill;
Described each composition and parts by weight are as follows:
Vitamin 6-15
Amino acid 8-20
Linoleic acid 6-12
Surfactant 20-30
Assistant for emulsifying agent 8-12
Stabilizing agent 4-5
Inorganic salts 2-3
Water 30-50.
Advantage of the present invention and good effect are:
1, the present invention mixes by surfactant Tween 80, Tween 80 and assistant for emulsifying agent and can effectively disperse liposoluble vitamin, linoleic acid, and basic amino acid solution also helps Cobastab simultaneously 2Pre-dispersed, by mutual fusion, namely obtain homogeneous, stable, clear and bright three-in-one multifunctional premix.
2, the present invention has added stabilizing agent dextrin, glue class and inorganic salts in constituent, and this three classes material can play static stabilization, makes the shelf-life of product reach 6 months.
3, comprised the step of crossing colloid mill among the preparation method of the present invention, this step makes the granularity of the emulsification micelle of fat-soluble composition in the dispersion reach nano-scale, and about 50nm not only is easy to absorb, also be beneficial to the quickening rate of dispersion, the product active ingredient total content that finally makes reaches 30%.
4, the nanoscale premix body feedstuff of the present invention's preparation can be miscible with arbitrary proportion with water, animal edible is convenient, amount is easy to regulate, can be effectively livestock and poultry animal be played health care, growth promotion, improves the quality of meat and bird product, do not add any antioxidant content in the premixed feed, the edible safety environmental protection.
5, the premix of the present invention's preparation can tolerate 0-40 ℃, and low temperature freezes shape in formation below-5 ℃, still returns to original state after the intensification, therefore all can use safely in the north and south of China.
Specific embodiment
The invention will be further described below by specific embodiment, and following examples are descriptive, is not determinate, can not limit protection scope of the present invention with this.
The multiplex raw material of following examples is commercially available.
Embodiment 1
A kind of three-in-one multifunctional premixed liquid feed, constituent and weight are as follows:
Water 35g, sodium chloride 1g, each 1g of pyrophosphoric acid, methionine 4g, lysine 5g, look three sour 4g, threonine 3g, Cobastab 20.01g, Tween 80 18g, vitamin A 3g, vitamin E 3g, vitamin D 2g, the dextrin 5g (mass fraction) that contains xanthans 1%, department class 802g, ethylene glycol 5g, propane diols 5g, linoleic acid 6g.
A kind of preparation method of three-in-one multifunctional premixed liquid feed, step is as follows:
(1) in 15g water, add sodium chloride, each 1g of pyrophosphoric acid, hold over night is also filtered, and dissolves respectively methionine 4g, lysine 5g, look three sour 4g, threonine 3g in filtrate, then adds Cobastab 20.01g, the solution 1 of hold over night.
(2) 10g water, 10g Tween 80,5g ethylene glycol mix, and then add 3g vitamin A, 3g vitamin E, 2g vitamin D, cross colloid mill, get solution 2.
(3) add the dextrin 5g that contains xanthans 1% in the 10g water, then mix with 8g Tween 80, class of 2g department 80,5g propane diols, the linoleic mixed liquor of 6g, get solution 3.
(4) above-mentioned three solution are mixed, and cross the three-in-one multifunctional liquid premixed feed of colloid mill.
This premix can mix use with feeding water according to the ratio of 100mL: 500L, is suitable for broiler chicken and uses.
Embodiment 2
A kind of three-in-one multifunctional premixed liquid feed, constituent and weight are as follows:
Water 35g, sodium chloride 1g, each 1g of pyrophosphoric acid, methionine 4g, lysine 6g, look three sour 5g, threonine 3g, Cobastab 20.01g, Tween 80 18g, vitamin A 3g, vitamin E 3g, vitamin D 2g, the dextrin 5g (mass fraction) that contains CMC1%, department class 802g, ethylene glycol 5g, mixed, the linoleic acid 6g of 5g glycerine.
A kind of preparation method of three-in-one multifunctional premixed liquid feed, step is as follows:
(1) in 15g water, add sodium chloride, each 1g of pyrophosphoric acid, hold over night is also filtered, and dissolves respectively methionine 4g, lysine 6g, look three sour 5g, threonine 3g in filtrate, then adds Cobastab 20.01g, the solution 1 of hold over night.
(2) 10g water, 10g Tween 80,5g glycerine mix, and then add 3g vitamin A, 3g vitamin E, cross colloid mill, get solution 2.
(3) add the dextrin 5g that contains CMC1% in the 10g water, then mix with 8g Tween 80, class of 2g department 80,5g ethylene glycol, the linoleic mixed liquor of 6g, get solution 3.
(4) above-mentioned three solution are mixed, and cross the three-in-one multifunctional liquid premixed feed of colloid mill.
This premix can mix use with feeding water according to the ratio of 100mL: 500L, is fit to pig, sheep, ox use.
Embodiment 3
A kind of three-in-one multifunctional premixed liquid feed, constituent and weight are as follows:
Water 35g, sodium chloride 1g, each 1g of pyrophosphoric acid, methionine 4g, lysine 5g, look three sour 4g, threonine 3g, Cobastab 20.01g, Tween 80 18g, vitamin A 4g, vitamin E 2g, the dextrin 4g (mass fraction) that contains xanthans 1%, department class 80 2g, propane diols 11g, linoleic acid 8g.
A kind of preparation method of three-in-one multifunctional premixed liquid feed, step is as follows:
(1) in 15g water, add sodium chloride, each 1g of pyrophosphoric acid, hold over night is also filtered, and dissolves respectively methionine 4g, lysine 5g, look three sour 4g, threonine 3g in filtrate, then adds Cobastab 20.01g, the solution 1 of hold over night.
(2) 10g water, 10g Tween 80,5g mixed with propylene glycol are even, then add 4g vitamin A, 2g vitamin E, cross colloid mill, get solution 2.
(3) add the dextrin 4g that contains xanthans 1% in the 10g water, then mix with 8g Tween 80, class of 2g department 80,6g propane diols, the linoleic mixed liquor of 8g, get solution 3.
(4) above-mentioned three solution are mixed, and cross the three-in-one multifunctional liquid premixed feed of colloid mill.
This premix can mix use with feeding water according to the ratio of 100mL: 500L, is fit to milk cow, laying hen use.

Claims (2)

1. a three-in-one multifunctional premixed liquid feed is characterized in that, its constituent and parts by weight are as follows:
Vitamin 6-15
Amino acid 8-20
Linoleic acid 6-12
Surfactant 20-30
Assistant for emulsifying agent 8-12
Stabilizing agent 4-5
Inorganic salts 2-3
Water 30-50;
This three-in-one multifunctional premixed liquid feed preparation process is as follows:
⑴ add inorganic salts in part water, hold over night is also filtered, and at dissolved in filtrate amino acid, water soluble vitamin, hold over night gets solution 1;
⑵ mix part water, part surface activating agent, part assistant for emulsifying agent, then adds liposoluble vitamin, crosses colloid mill, gets solution 2;
⑶ add stabilizing agent in part water, then mix with part surface activating agent, part assistant for emulsifying agent, linoleic mixed liquor, gets solution 3;
⑷ mix above-mentioned molten 1,2,3 liquid, and cross the three-in-one multifunctional liquid premixed feed of colloid mill.
2. three-in-one multifunctional premixed liquid feed according to claim 1, it is characterized in that: described vitamin comprises vitamin A. D. E, B 2In one or more mixture.
3, three-in-one multifunctional premixed liquid feed according to claim 1 is characterized in that: described amino acid comprises one or more the mixture in methionine, lysine, tryptophan, the threonine.
4, three-in-one multifunctional premixed liquid feed according to claim 1 is characterized in that: described surfactant is one or more mixture in Tween 80, department class 80, the sucrose fatty ester etc.
5, three-in-one multifunctional premixed liquid feed according to claim 1 is characterized in that: described assistant for emulsifying agent is one or more the mixture in propane diols, ethylene glycol, glycerine, the propyl alcohol.
6, three-in-one multifunctional premixed liquid feed according to claim 1 is characterized in that: described stabilizing agent is one or more the mixture among cyclodextrin, xanthans, the CMC.
7, three-in-one multifunctional premixed liquid feed according to claim 1 is characterized in that: described inorganic salts are one or more the mixture in sodium chloride, the sodium pyrophosphate.
8, three-in-one multifunctional liquid premixed feed according to claim 1 is characterized in that: also bag expands auxiliary reagent.
9, three-in-one multifunctional liquid premixed feed according to claim 8 is characterized in that: described auxiliary reagent is sucrose.
CN2010102555815A 2010-08-17 2010-08-17 Three-in-one multifunctional premixed liquid feed and preparation method thereof Expired - Fee Related CN101978851B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102669450B (en) * 2012-01-15 2013-12-18 河南科技大学 Milk cow energy extender and preparation method thereof
CN102726595A (en) * 2012-06-11 2012-10-17 施瑞客(天津)生物技术有限公司 Livestock and poultry liquid feedstuff, preparation method thereof, and application method thereof
CN102845646B (en) * 2012-09-20 2013-12-11 合肥基石生物工程有限公司 Method for preparing piglet syrup feed without fish meal and plasma proteins
CN103053807B (en) * 2013-01-24 2014-04-16 南京日升昌生物技术有限公司 Water-soluble composite vitamin preparation and preparation method thereof
CN103431253B (en) * 2013-09-24 2015-06-17 冯万松 Liquid feed for live pigs and preparation process thereof
CN113966793A (en) * 2021-10-29 2022-01-25 江苏福润德科技有限公司 Viscous liquid aquatic product compound premix and production process thereof
CN113966794A (en) * 2021-10-29 2022-01-25 江苏福润德科技有限公司 Viscous liquid premix and production process thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1561967A (en) * 2004-03-23 2005-01-12 毛一鹏 Nano grade vitamin micro emulsion and its preparing method
CN1620896A (en) * 2004-12-16 2005-06-01 国龙科技饲料(上海)有限公司 Homogeneous liquid feed stuff additive and its preparation method
CN101120741A (en) * 2007-08-27 2008-02-13 耿瑞 Maturative liquid feed for sucking piglet

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1561967A (en) * 2004-03-23 2005-01-12 毛一鹏 Nano grade vitamin micro emulsion and its preparing method
CN1620896A (en) * 2004-12-16 2005-06-01 国龙科技饲料(上海)有限公司 Homogeneous liquid feed stuff additive and its preparation method
CN101120741A (en) * 2007-08-27 2008-02-13 耿瑞 Maturative liquid feed for sucking piglet

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