CN101973742B - Blue attapulgite polymer clay powder - Google Patents
Blue attapulgite polymer clay powder Download PDFInfo
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- CN101973742B CN101973742B CN2010102404410A CN201010240441A CN101973742B CN 101973742 B CN101973742 B CN 101973742B CN 2010102404410 A CN2010102404410 A CN 2010102404410A CN 201010240441 A CN201010240441 A CN 201010240441A CN 101973742 B CN101973742 B CN 101973742B
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- blue
- attapulgite
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- blue attapulgite
- polymer clay
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- 229960000892 attapulgite Drugs 0.000 title claims abstract description 57
- 229910052625 palygorskite Inorganic materials 0.000 title claims abstract description 57
- 239000000843 powder Substances 0.000 title claims abstract description 45
- 239000004927 clay Substances 0.000 title claims abstract description 25
- 229920000642 polymer Polymers 0.000 title abstract 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 9
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims abstract description 7
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims abstract description 7
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 6
- 239000004113 Sepiolite Substances 0.000 claims abstract description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000001110 calcium chloride Substances 0.000 claims abstract description 6
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract description 6
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910052624 sepiolite Inorganic materials 0.000 claims abstract description 6
- 235000019355 sepiolite Nutrition 0.000 claims abstract description 6
- 238000010298 pulverizing process Methods 0.000 claims description 11
- 239000004575 stone Substances 0.000 claims description 10
- 239000000428 dust Substances 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- CODAYFPFZXWNLD-UHFFFAOYSA-N 2-hydroxypropanoyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC(=O)C(C)O CODAYFPFZXWNLD-UHFFFAOYSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 5
- 235000011194 food seasoning agent Nutrition 0.000 claims description 3
- 229910000831 Steel Inorganic materials 0.000 claims description 2
- 235000012745 brilliant blue FCF Nutrition 0.000 claims description 2
- 230000003301 hydrolyzing effect Effects 0.000 claims description 2
- 230000008676 import Effects 0.000 claims description 2
- 229910001220 stainless steel Inorganic materials 0.000 claims description 2
- 239000010935 stainless steel Substances 0.000 claims description 2
- 239000010959 steel Substances 0.000 claims description 2
- 230000007306 turnover Effects 0.000 claims description 2
- 206010011376 Crepitations Diseases 0.000 abstract 1
- 208000037656 Respiratory Sounds Diseases 0.000 abstract 1
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 abstract 1
- 239000000440 bentonite Substances 0.000 abstract 1
- 229910000278 bentonite Inorganic materials 0.000 abstract 1
- 239000001768 carboxy methyl cellulose Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 abstract 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 abstract 1
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 abstract 1
- 229940080352 sodium stearoyl lactylate Drugs 0.000 abstract 1
- ODFAPIRLUPAQCQ-UHFFFAOYSA-M sodium stearoyl lactylate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC(=O)OC(C)C(=O)OC(C)C([O-])=O ODFAPIRLUPAQCQ-UHFFFAOYSA-M 0.000 abstract 1
- 239000000919 ceramic Substances 0.000 description 15
- 239000011347 resin Substances 0.000 description 8
- 229920005989 resin Polymers 0.000 description 8
- 238000000034 method Methods 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 3
- 239000005977 Ethylene Substances 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 229920002472 Starch Polymers 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 3
- 239000002932 luster Substances 0.000 description 3
- 239000004800 polyvinyl chloride Substances 0.000 description 3
- 230000001737 promoting effect Effects 0.000 description 3
- 239000008107 starch Substances 0.000 description 3
- 235000019698 starch Nutrition 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000004945 emulsification Methods 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000009965 odorless effect Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229920002545 silicone oil Polymers 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 230000009967 tasteless effect Effects 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 231100000652 hormesis Toxicity 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000011022 opal Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 235000019633 pungent taste Nutrition 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
Landscapes
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)
Abstract
The invention discloses blue attapulgite polymer clay powder. The technical scheme is characterized in that the blue attapulgite polymer clay powder is prepared from purified blue attapulgite clay, white bentonite, sepiolite, anatase titanium dioxide, phthalocyanine blue, calcium chloride, sodium polyacrylate, sodium carboxymethylcellulose and sodium stearoyl lactylate by the following steps of: mixing the ingredients of the blue attapulgite polymer clay powder, feeding in a crusher to crush, feeding the crushed mixture into a pulverizer to be pulverized into powder and packaging into a finished product of the blue attapulgite polymer clay powder. Blue attapulgite polymer clay made by adding water and methyl silicone oil to the blue attapulgite polymer clay powder has the advantages of high viscosity, good flexible plasticity, small shrinkage, no corrosiveness and no greasy feeling, is hardened after natural drying without baking and is crackless. The invention has the characteristics of simple production process and low cost, is convenient to use and benefits popularization and use, and the blue attapulgite polymer clay powder is suitable for making blue attapulgite polymer clay on site.
Description
Technical field
The present invention relates to the mud of making pottery, be specifically related to the soft pottery powder of a kind of blue attapulgite.
Background technology
The soft ceramic mud of supplying on the market is through the block soft ceramic mud after the batching processing, the main raw material of soft ceramic mud is polyvinyl chloride and lime carbonate, binding property is bad under the normal temperature state, and prolonged preservation easily wears out and fades, and bubbles easily during the baking soft ceramic mud, when if temperature surpasses 200 ℃, finished product is burnt and melt, even may cause burning, generate chloride pungency toxic smog, the selling price of soft ceramic mud is higher, is unfavorable for promoting the use of.
The Chinese patent publication number is: CN 101186736, open day: on May 28th, 2008, name is called " a kind of soft ceramic mud and preparation method thereof ", disclose: " a kind of soft ceramic mud and preparation method; it is prepared from by following parts by weight of component: polyvinyl chloride (PVC) paste resin 15～40, bizinc resin 20～55, lime carbonate 15～35, softening agent 0.1～0.4, toner 0.5～0.15, all the other are micro-moisture and impurity ".
The weak point of above-mentioned patent is that the soft ceramic mud main raw material that this technology is produced is polyvinyl chloride (PVC) paste resin, bizinc resin and lime carbonate, and binding property is bad under the normal temperature state, is unfavorable for making moulding, and bizinc resin belongs to dangerous product.
The Chinese patent Granted publication number is: CN 1273531, Granted publication day: on September 6th, 2006, name is called " a kind of manufacture method of transparent texture resin clay ", disclose: " a kind of manufacture method of transparent texture resin clay; it is characterized in that: it is at first mixed together by ethylene powder-vinyl acetate copolymer, starch, glycerol, sanitas, spices and adds water purification again and stir into mud shape thing; and then add whiteruss and mix and stir, vacuum-packed finished product ".
The weak point of above-mentioned patent is that the transparent texture resin clay main raw material that this technology is produced is ethylene powder-vinyl acetate copolymer and starch, ethylene powder-vinyl acetate copolymer has hormesis to eyes and skin, be not suitable for being used to manufacture the raw material of handicraft, need a large amount of starch in this product, be unfavorable for promoting the use of.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, provide a kind of blue attapulgite soft pottery powder.
The soft pottery powder of blue attapulgite is made up of Concavo-convex stick after purifying stone clay, white wilkinite, sepiolite, anatase thpe white powder, phthalocyanine blue, calcium chloride, sodium polyacrylate, Xylo-Mucine and stearoyl lactate.After the batch mixes with the soft pottery powder of blue attapulgite, pulverize in the input pulverizer, carry out abrasive dust in the mixture input pulverizing mill after will pulverizing again, be packaged as the finished product of the soft pottery powder of blue attapulgite.
Use the wet beneficiation craft of Attapulgite, the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of Concavo-convex stick after purifying stone clay, Concavo-convex stick after purifying stone clay soil property exquisiteness, smooth surface, quality is lighter, be viscosity and plasticity-when moist, its viscosity can reach more than the 3000mPas, helps the bonding between the raw material, the dry post-shrinkage ratio of attapulgite clay is little, and does not produce be full of cracks.
The white wilkinite is the wilkinite of a kind of high whiteness and high brightness, has excellent plasticity, cohesiveness and oilness.
Sepiolite is a kind of rich fibrous magnesium silicate clay mineral, has fine and smooth soft, viscosity is strong, shrinking percentage is low and plasticity-the is good characteristics of satin luster, light weight, helps improving the gloss and the mouldability of the soft pottery powder of blue attapulgite.
Phthalocyanine blue is the mazarine powder, and is water insoluble, lovely luster, and the tinting strength height, dispersed strong, sun-proof and heat-resisting.
Calcium chloride is water-soluble, is a kind of siccative commonly used, has in the present invention to improve the soft pottery powder of blue attapulgite and add hardness after water is made into the blue attapulgite soft ceramic mud, and can increase the anti-ability of freezing of blue attapulgite soft ceramic mud.
Anatase thpe white powder has excellent water dispersible and remarkable optical property, form and aspect stability, and size-grade distribution is good, has the characteristics of high gloss, high reducing power, high covering power.
Sodium polyacrylate is a kind of white powder, odorless, tasteless and nontoxic can be slowly soluble in water, forms utmost point heavy-gravity transparent gel, have thickening, emulsification, figuration, multiple function such as expanded, stable, can improve the cohesiveness and the ductility of the soft pottery powder of blue attapulgite.
Xylo-Mucine is white fiber shape or particle powder, and odorless is tasteless, and water absorbability is arranged, and easily is scattered in to be swelled into colloidal solution in the water, has good emulsifying stablizer and thickening material.
Stearoyl lactate is a kind of off-white powder or chip solid, can be scattered in the hot water, has effects such as emulsification, anti-aging and increase plasticity in the present invention.
Selecting sodium polyacrylate, stearoyl lactate and Xylo-Mucine in the present invention simultaneously for use, is to add water and make cohesiveness, flexibility, the ductility behind the blue attapulgite soft ceramic mud and prevent that the blue attapulgite soft ceramic mud is aging in order further to increase the soft pottery powder of blue attapulgite.
The present invention is achieved by following technical proposals:
1, the batching of the soft pottery powder of blue attapulgite is made up of following component by weight percentage: Concavo-convex stick after purifying stone clay 30～55%, white wilkinite 15～30%, sepiolite 5～20%, phthalocyanine blue 1～8%, calcium chloride 1～5%, anatase thpe white powder 0.1～5%, sodium polyacrylate 0.1～5%, Xylo-Mucine 0.1～5% and stearoyl lactate 0.1～5%.
2, the production method of the soft pottery powder of blue attapulgite: after the batch mixes with the soft pottery powder of blue attapulgite, pulverize in the input pulverizer, compound particles fineness after the pulverizing is less than 0.250 millimeter, carry out abrasive dust in the mixture input pulverizing mill after will pulverizing again, compound particles fineness behind the abrasive dust is packaged as the finished product of the soft pottery powder of blue attapulgite less than 0.045 millimeter.
Described Concavo-convex stick after purifying stone clay, it is the Attapulgite ore deposit mixture that will contain earth impurity, import in the hydrolytic tank after crushed, soak after 24 hours, dash with high-pressure pump and to turn over, and the sieve of the drum by making with stainless steel steel wire sieve removes the impurity more than 1 millimeter, send in the acclive settling tank, continuation is dashed with high-pressure pump and is turned over, after 12 hours, because the proportion in Attapulgite ore deposit is lighter, its the superiors in whole throw out draws this part Attapulgite ore deposit with slush pump and sends in the flat settling tank, emits unnecessary water after 15 hours, through 2-3 days seasoning, take out this part Attapulgite ore deposit and be Concavo-convex stick after purifying stone clay;
This technology is to adopt " the Attapulgite wet beneficiation craft " in application on September 18th, 2003 by the inventor, and the Chinese patent Granted publication number is: CN1224463, Granted publication day: on October 26th, 2005.
The using method of the soft pottery powder of blue attapulgite: 1. the soft pottery powder of blue attapulgite is placed in the container, slowly in the soft pottery powder of blue attapulgite, added 50～60 ℃ hot water, and in time mix and crumple blue into strips clod thoroughly, left standstill subsequently 30～60 minutes; 2. methyl-silicone oil is spread upon the blue clod outside surface of strip and crumple once more, be pressed into softish blue attapulgite soft ceramic mud, promptly can be used for moulding clear patterns, lovely luster, the artwork that effect is true to nature.
The separate case application of above-mentioned using method patent of invention, number of patent application is 201010240164.3.
Use the soft pottery powder of blue attapulgite to add the blue attapulgite soft ceramic mud viscosity height of water and methyl-silicone oil making, soft plasticity-is good, have that shrinking percentage is little, indeformable, hardening after seasoning, do not need to toast, do not produce be full of cracks, not mouldy, never degenerate, not skin irritation, nontoxic, non-corrosiveness and do not have the characteristics of greasy feeling.
Production technique of the present invention is simple, and is with low cost, easy to use, helps promoting the use of.
The soft pottery powder of blue attapulgite is applicable to the Attapulgite soft ceramic mud of field fabrication blueness.
Embodiment
The invention will be further described below in conjunction with embodiment:
1, the batching of the soft pottery powder of blue attapulgite is made up of following component by weight percentage: Concavo-convex stick after purifying stone clay 40%, white wilkinite 28%, sepiolite 18%, phthalocyanine blue 4%, calcium chloride 3%, anatase thpe white powder 3%, sodium polyacrylate 2%, Xylo-Mucine 1.5% and stearoyl lactate 0.5%.
2, the production method of the soft pottery powder of blue attapulgite: after the batch mixes with the soft pottery powder of blue attapulgite, pulverize in the input pulverizer, compound particles fineness after the pulverizing is less than 0.250 millimeter, carry out abrasive dust in the mixture input pulverizing mill after will pulverizing again, compound particles fineness behind the abrasive dust is packaged as the finished product of the soft pottery powder of blue attapulgite less than 0.045 millimeter.
Claims (1)
1. soft pottery powder of blue attapulgite, it is characterized in that the batching of the soft pottery powder of blue attapulgite is made up of following component by weight percentage: Concavo-convex stick after purifying stone clay 30～55%, white wilkinite 15～30%, sepiolite 5～20%, phthalocyanine blue 1～8%, calcium chloride 1～5%, anatase thpe white powder 0.1～5%, sodium polyacrylate 0.1～5%, Xylo-Mucine 0.1～5% and stearoyl lactate 0.1～5%;
The production method of the soft pottery powder of described blue attapulgite: after the batch mixes with the soft pottery powder of blue attapulgite, pulverize in the input pulverizer, compound particles fineness after the pulverizing is less than 0.250 millimeter, carry out abrasive dust in the mixture input pulverizing mill after will pulverizing again, compound particles fineness behind the abrasive dust is packaged as the finished product of the soft pottery powder of blue attapulgite less than 0.045 millimeter;
Described Concavo-convex stick after purifying stone clay, it is the Attapulgite ore deposit mixture that will contain earth impurity, import in the hydrolytic tank after crushed, soak after 24 hours, dash with high-pressure pump and to turn over, and the sieve of the drum by making with stainless steel steel wire sieve removes the impurity more than 1 millimeter, send in the acclive settling tank, continuation is dashed with high-pressure pump and is turned over, after 12 hours, because the proportion in Attapulgite ore deposit is lighter, its the superiors in whole throw out draws this part Attapulgite ore deposit with slush pump and sends in the flat settling tank, emits unnecessary water after 15 hours, through 2-3 days seasoning, take out this part Attapulgite ore deposit and be Concavo-convex stick after purifying stone clay.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102404410A CN101973742B (en) | 2010-07-30 | 2010-07-30 | Blue attapulgite polymer clay powder |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102404410A CN101973742B (en) | 2010-07-30 | 2010-07-30 | Blue attapulgite polymer clay powder |
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| Publication Number | Publication Date |
|---|---|
| CN101973742A CN101973742A (en) | 2011-02-16 |
| CN101973742B true CN101973742B (en) | 2011-10-26 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2010102404410A Expired - Fee Related CN101973742B (en) | 2010-07-30 | 2010-07-30 | Blue attapulgite polymer clay powder |
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| CA2841149C (en) | 2011-07-08 | 2019-11-05 | Purac Biochem Bv | Active formulation for use in feed products |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5008226A (en) * | 1989-05-16 | 1991-04-16 | Engelhard Corporation | Process for making acid activated bleaching earth using high susceptibility source clay and novel bleaching earth product |
| CN1167478A (en) * | 1995-08-04 | 1997-12-10 | 総合粘土窯业株式会社 | Synthetic clay for ceramics and process for preparing the same |
| US6130179A (en) * | 1998-11-12 | 2000-10-10 | Itc, Inc. | Purified attapulgite clay |
-
2010
- 2010-07-30 CN CN2010102404410A patent/CN101973742B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5008226A (en) * | 1989-05-16 | 1991-04-16 | Engelhard Corporation | Process for making acid activated bleaching earth using high susceptibility source clay and novel bleaching earth product |
| CN1167478A (en) * | 1995-08-04 | 1997-12-10 | 総合粘土窯业株式会社 | Synthetic clay for ceramics and process for preparing the same |
| US6130179A (en) * | 1998-11-12 | 2000-10-10 | Itc, Inc. | Purified attapulgite clay |
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| CN101973742A (en) | 2011-02-16 |
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