CN101961305A - Skin-protecting cosmetic host material and preparation method thereof - Google Patents
Skin-protecting cosmetic host material and preparation method thereof Download PDFInfo
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- CN101961305A CN101961305A CN 201010295333 CN201010295333A CN101961305A CN 101961305 A CN101961305 A CN 101961305A CN 201010295333 CN201010295333 CN 201010295333 CN 201010295333 A CN201010295333 A CN 201010295333A CN 101961305 A CN101961305 A CN 101961305A
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Abstract
The invention provides a skin-protecting cosmetic host material. An oil and fat product is extracted from ratite birds such as ostriches, emus and the like by an organic solvent extraction method or a supercritical extraction method. The skin-protecting cosmetic host material is rich in important active ingredients such as unsaturated fatty acid and the like and the active ingredients comprise oleic acid, linoleic acid, linolenic acid and the like, wherein the oleic acid content is highest and accounts for 32 to 45 percent of the weight of the total fatty acid ingredients. The skin-protecting cosmetic host material has good effect of promoting percutaneous absorption, capacity of reducing the resistance of other functional components penetrating the skin, no toxicity and nonirritant to human skin, effects of repairing skin injury, diminishing inflammation and stopping pain, contributing to regeneration and moistening the skin and obvious skin-protecting effect, so the host material is a safe and ideal skin-protecting cosmetic host material.
Description
Technical field
The present invention relates to a kind of cosmetic base material and preparation method thereof, especially a kind of protection type cosmetic base material that is used for skin protection and preparation method thereof belongs to the cosmetic material technical field.
Background technology
The substrate that is used for cosmetics can be divided into aqueous matrix and oleaginous base.Aqueous matrix is representative with glycerol, propylene glycol, Polyethylene Glycol, and main purpose is to give moist feeling; Oleaginous base is representative with triglyceride and silicone oil then, and main purpose is that skin is not clamminess, and gives smooth feeling etc.But because these two kinds of substrate intersolubilities are relatively low, the cosmetics of Xiao Shouing all can add the physicochemical property that additives such as a large amount of surfactants, thickening agent, emulsifying agent are regulated cosmetics in substrate in the market, produce the characteristic of smooth feeling and moist feeling two aspects.Yet these additives are when increasing cosmetics smooth feeling and moist feeling, can produce bigger side effect also, the additive that for example remains on the skin can produce certain zest to skin, and then damage normal skin, especially to allergic skin, even can produce symptoms such as erythema, pruritus.Now, also be devoted in the industry to address the above problem always, wherein just be included in the research above the cosmetic base.Patent CN 1561193A discloses a kind of new medium, but it mainly acts in order to improve usability, is unprofitable to improve the additive side effect.Patent CN 1416804A then discloses a kind of cosmetics new medium that is used for skin-nourishing, does not but relate to the effect of resisting various additive damages.Therefore, for alleviate additive in the cosmetics to the damage of skin, safeguard the health of skin, the developmental research of protection type cosmetic base is imperative.
The oils and fats of ratite such as Ostriches, Dromaius novaehollandiae class mostly derives from its body fat, also can obtain from bird meat, generally comprises fatty acid composition and non-saponification compositions such as Squalene, vitamin E such as Palmic acid, stearic acid, oleic acid, linoleic acid, linolenic acid.Owing to belong to same catalogue, the composition of various ratite quasi-greases and character is very approaching all, causes the similar of its physiological function then.Because the unique chemical composition, the ratite oils and fats has advantages of good skin permeability, the lubricated and emulsification property of water holding capacity, height efficiently, is a kind of natural superior cosmetics desirable feedstock.As substrate, then can reduce the addition of additives such as emulsifying agent, reduce the various side effect that additive brought.A long time ago, just used the ratite oil that comprises ostrich oil, fat of Oromaius norvaehollandeae the different local aborigines of Australia with Asia, Africa, South America etc.It is found that, smear health, can treat dermatosis, myalgia, arthritis, scratch, burn etc. with ostrich oil or oriole emu oil.Modern study shows that the ratite oils and fats is relaxed muscle rapidly, fatigue alleviating, repair damaging cells fast, promote tissue regeneration, significantly increase the comprehensive density of skin, the chafe hair follicle growth, smooth away wrinkles, opposing aging and anti-inflammatory analgetic reduce cutaneous sensibility, alleviate the symptom (Wu Xiaoying etc. of neurodermatitis or dry eczema, the China poultry, 2005 the 27th the 5th phases of volume).Greasy these obvious effect of ratite make it possess the potentiality that are developed to the protection type cosmetic base fully.(Jiang Nianqiong etc., economic animal journal, 2006 the 10th the 2nd phases of volume; Yang Xiufang etc., grain and oils and fats, 2009 the 12nd phases).
The oils and fats of ratite such as Ostriches, Dromaius novaehollandiae class can obtain by several different methods, for example traditional smelting process, organic solvent extraction method and supercritical extraction etc.Tradition smelting process and organic solvent method all are through the long-term practice checking, reach the mature technology of suitability for industrialized production level already, are used widely in actual oils and fats extracts.But its shortcoming is pyroprocess and causes in the oils and fats important active component such as unsaturated fatty acid to be destroyed easily, and then changes or slacken some physicochemical property and the protective capacities of extract.By contrast, supercritical extraction occurs later, is but developing rapidly always, the existing now suitability for industrialized production level that much enters.Because of advantages such as its low-temperature extraction, high efficiency, high selectivity and no solvent residues, supercritical extraction technique can keep the original effective ingredient in the extract to greatest extent, guaranteed the good characteristic and the remarkable efficacy of product, this also is that it is equipped with the concerned by the industry reason.
Summary of the invention
The present invention is intended to remedy the blank of above-mentioned present situation, a kind of skin protection type cosmetic base material is provided, and is a kind ofly to develop natural the have damage of reparation, anti-inflammatory analgetic from ratite apoplexy due to endogenous wind such as Ostriches, Dromaius novaehollandiaes, promote regeneration, the protection type cosmetic base material of effects such as skin care.This host material is rich in important active component such as unsaturated fatty acid, comprises oleic acid, linoleic acid, linolenic acid etc., and is wherein the highest with oleic acid content, accounts for the 32-45% of total fatty acids composition.Proved already that oleic acid, linoleic acid belonged to transdermal absorption accelerator, and can other functional components penetrate into skin.
The invention provides a kind of skin protection type cosmetic base material obtains by following preparation method:
1. after the fatty tissue of ratite classes such as Ostriches, Dromaius novaehollandiae being cleaned, with rubbing in the meat grinder, it is standby to place refrigerator and cooled to freeze;
2. take by weighing a certain amount of frozen fat, be cut into small pieces, adopt organic solvent extraction method or supercritical extraction to extract, extract obtained process is further purified, the product that obtains promptly can be used as natural protection type cosmetic base material, be a kind of oils product, be light yellow or white semisolid under the room temperature, cool off the solid that is white in color.
The used extraction solvent of organic solvent extraction method is a petroleum ether, its outward appearance and character are: colourless transparent liquid has the kerosene abnormal smells from the patient, boiling range: 30-60 ℃, serve as better wherein with 40-60 ℃, in 40-65 ℃ of reflux, extract, 1-2 time, extraction time 1-3h is with extracting solution sucking filtration, merging, then, is under the condition of 70-95kPa at 40-45 ℃ with vacuum, and the extraction solvent is removed in distillation, obtains target product.
Supercritical extraction is with CO
2For extractant carries out cycling extraction.Process conditions are as follows: extraction kettle pressure is 15-25MPa, wherein is better with 15-20MPa; Extraction temperature is 35-60 ℃, serves as better with 35-45 ℃ wherein; The pressure of separator 1 is 7-9MPa, and temperature is 50-60 ℃; The pressure of separator 2 is 4-5MPa, and temperature is 40-55 ℃.The extract that the course of processing is often collected from separating still.Extract is the white solid paste, and room temperature is placed the semisolid that is white in color, and cools off the solid that is white in color.Extract need not to handle, just can be directly as protection type cosmetic base of the present invention.
Usefulness of the present invention is: adopt organic solvent extraction method or supercritical extraction to extract a kind of oils host material from ratite apoplexy due to endogenous wind such as Ostriches, Dromaius novaehollandiaes, this host material is rich in important active component such as unsaturated fatty acid, comprises oleic acid, linoleic acid, linolenic acid etc.Host material of the present invention has good percutaneous and absorbs facilitation; can reduce the percutaneous resistance of other functional components; nontoxic to human body skin simultaneously, nonirritant; has the damage of reparation; anti-inflammatory analgetic promotes regeneration, effects such as skin care; for skin significant protective effect being arranged, is the ideal protection type cosmetic base of a kind of safety material.
The specific embodiment
The present invention is described in further detail below in conjunction with specific embodiment.
Embodiment 1---and conventional organic solvent method extracts the Ostriches oils and fats
Take by weighing Ostriches fat 200g, place the 2000mL round-bottomed flask, add the petroleum ether (30-60) that is equivalent to 5 times of Ostriches fat weights, reflux, extract, 2 times, each 2h.Merge extractive liquid,, sucking filtration, filtrate does not steam liquid in 40 ℃ of rotary evaporations to having, to go out petroleum ether solvent.The extract that obtains is yellow fluid, and room temperature is placed and engendered cotton-shaped solid, and color shoals gradually, finally forms faint yellow semi-solid, cools off the solid that is white in color.Extraction ratio is up to 78%.
Embodiment 2---supercritical fluid extraction Ostriches oils and fats
Take by weighing 200g Ostriches fat, place the 1L extraction kettle of HA-220-50-06 supercritical extraction equipment (Huaan supercritical extraction company limited), regulate supercritical equipment and reach following condition: extracting pressure: 20MPa, extraction temperature: 45 ℃, CO
2Flow: 15L/h separates I pressure: 8MPa, separates the I temperature: 35 ℃, separate II pressure: 4-6MPa (deciding) according to gas tank pressure, and separate the II temperature: 35 ℃, the extraction time: 5h.After extraction finished, the extract of collecting from separate I was the white solid paste, and room temperature is placed the semisolid that is white in color, and cooled off the solid that is white in color.Extract need not to handle, just can be directly as protection type cosmetic base of the present invention.Extraction yield reaches 71.6%.
Embodiment 3---supercritical fluid extraction Dromaius novaehollandiae oils and fats
Take by weighing 250g Dromaius novaehollandiae fat, place the 1L extraction kettle, regulate supercritical equipment and reach following condition: extracting pressure: 25MPa, extraction temperature: 50 ℃, CO
2Flow: 35L/h separates I pressure: 8MPa, separates the I temperature: 40 ℃, separate II pressure: 4-6MPa (deciding) according to gas tank pressure, and separate the II temperature: 40 ℃, the extraction time: 5h.After extraction finished, the extract of collecting from separate I was the white solid paste, and room temperature is placed the semisolid that is white in color, and cooled off the solid that is white in color.Extract need not to handle, just can be directly as protection type cosmetic base of the present invention.Extraction yield is 20.6%.
Embodiment 4---the preparation of Ostriches bloom
Develop a kind of skin protection type Ostriches bloom with the ostrich oil extract that embodiment 2 prepares.Its punishment is: 0.4 part of stearic acid, 3.5 parts of 16-18 alcohol, 2 parts of glyceryl monostearates, 1 part of tween 80, Si Pan-800.4 part, 2 parts in vaseline, 10 parts of ostrich oil extracts, 2 parts of cera alba, 0.5 part of polymethyl siloxane, 0.1 part of methyl hydroxybenzoate, 5 parts of glycerol, 1,13 parts of 3-butanediols, 1 part of polyethylene glycol 1500,0.1 part of Vitamin E acetate, octyldimethyl is to 0.01 part in ammonium benzoic acid, and 0.5 part of triethanolamine adds 20 parts of Purified Waters and makes water in oil latex A at the emulsifying still.Then, other gets 10 parts of 1% polyacrylic acid solution, 5 parts of 1% hyaluronic acid solutions, and 0.1 part of Aloe extract, 0.1 part of Radix Glycyrrhizae Saponin acid dipotassium, 0.25 part of 21.5 parts of Purified Waters and spice are made solution B.Then A and B are mixed, carry out second emulsifying, the gained unguentum is novel Ostriches bloom.Through preliminary test, this product has skin moisture-keeping, smoothes away wrinkles and resists old and feeble effect.
Embodiment 5---the preparation of Dromaius novaehollandiae bloom
The punishment of Dromaius novaehollandiae bloom is: 0.4 part of stearic acid, 2 parts of glyceryl monostearates, 1 part of tween 80, Si Pan-80 0.4 part, 2 parts in vaseline, 6 parts of fat of Oromaius norvaehollandeae extracts, 2 parts of cera alba, 0.5 part of polymethyl siloxane, 0.1 part of methyl hydroxybenzoate, 4 parts of glycerol, 15 parts of 1,3 butylene glycols, 1 part of polyethylene glycol 1500,0.1 part of Vitamin E acetate, octyldimethyl is to 0.01 part in ammonium benzoic acid, 0.5 part of triethanolamine adds 15 parts of Purified Waters and makes water in oil latex A at the emulsifying still.Then, other gets 10 parts of 1% polyacrylic acid solution, 5 parts of 1% hyaluronic acid solutions, and 0.1 part of Aloe extract, 0.1 part of Radix Glycyrrhizae Saponin acid dipotassium, 0.25 part of 20 parts of Purified Waters and spice are made solution B.Then A and B are mixed, carry out second emulsifying, the gained unguentum is novel Dromaius novaehollandiae bloom.
Claims (4)
1. skin protection type cosmetic base material, this host material contains unsaturated fatty acid, comprises oleic acid, linoleic acid or linolenic acid, and wherein oleic acid content accounts for the 32-45% of total fatty acids composition, and described host material obtains by the following method:
(1) fatty tissue of ratite classes such as Ostriches, Dromaius novaehollandiae is cleaned after, with rubbing in the meat grinder, it is standby to place refrigerator and cooled to freeze;
(2) take by weighing a certain amount of frozen fat, be cut into small pieces, adopt organic solvent extraction method or supercritical extraction to extract, extract obtained process is further purified, the product that obtains is natural protection type cosmetic base material, be a kind of oils product, be light yellow or white semisolid under the room temperature, cool off the solid that is white in color.
2. a kind of skin protection type cosmetic base material according to claim 1, it is characterized in that the organic solvent extraction method is described in the preparation method (2): used extractant is the solvent petroleum ether, boiling range: 30-60 ℃, wherein preferred 40-60 ℃, 40-65 ℃ of reflux, extract, temperature extracted 1-2 time, extraction time 1-3 hour, with extracting solution sucking filtration, merging, then, be under the condition of 70-95kPa with vacuum at 40-45 ℃, extractant is removed in distillation, obtains target product.
3. a kind of skin protection type cosmetic base material according to claim 1 is characterized in that supercritical extraction described in the preparation method (2): with CO
2For extractant carries out cycling extraction, extraction kettle pressure is 15-25MPa, preferred 15-20Mpa, and extraction temperature is 35-60 ℃, and preferred 35-45 ℃, the pressure of separator 1 is 7-9MPa, and temperature is 50-60 ℃; The pressure of separator 2 is 4-5MPa, and temperature is 40-55 ℃, and the course of processing is often collected extract from separating still, obtain target product.
4. a kind of skin protection type cosmetic base material according to claim 1 is characterized in that, the extraction kettle pressure of supercritical extraction is 15-20Mpa in the preparation method (2), and extraction temperature is 35-45 ℃.
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Cited By (8)
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| CN102389378A (en) * | 2011-11-23 | 2012-03-28 | 天津郁美净集团有限公司 | Compound grease microemulsion used in cosmetics and preparation method thereof |
| CN102614099A (en) * | 2012-04-10 | 2012-08-01 | 张仕英 | Method for preparing rose extract for supercritical CO2 extraction cosmetics |
| RU2614720C1 (en) * | 2016-02-18 | 2017-03-28 | Мария Владимировна Горбачева | Cosmetic |
| CN109381353A (en) * | 2018-11-26 | 2019-02-26 | 深圳市景光生物科技有限公司 | A kind of cream reaching repairing effect of releiving with fat of Oromaius norvaehollandeae |
| RU2691130C1 (en) * | 2018-12-13 | 2019-06-11 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Московская государственная академия ветеринарной медицины и биотехнологии - МВА имени К.И. Скрябина" (ФГБОУ ВО МГАВМиБ - МВА им. К.И. Скрябина) | Cosmetic night cream |
| RU2692057C1 (en) * | 2018-12-13 | 2019-06-20 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Московская государственная академия ветеринарной медицины и биотехнологии - МВА имени К.И. Скрябина" (ФГБОУ ВО МГАВМиБ - МВА им. К.И. Скрябина) | Cosmetic day cream |
| CN113440618A (en) * | 2021-07-06 | 2021-09-28 | 朱景平 | Transdermal matrix and preparation method thereof |
| CN114732803A (en) * | 2022-04-26 | 2022-07-12 | 长江大学 | Vaseline containing ostrich oil and fat and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102389378A (en) * | 2011-11-23 | 2012-03-28 | 天津郁美净集团有限公司 | Compound grease microemulsion used in cosmetics and preparation method thereof |
| CN102614099A (en) * | 2012-04-10 | 2012-08-01 | 张仕英 | Method for preparing rose extract for supercritical CO2 extraction cosmetics |
| CN102614099B (en) * | 2012-04-10 | 2013-03-20 | 张仕英 | Method for preparing rose extract for supercritical CO2 extraction cosmetics |
| RU2614720C1 (en) * | 2016-02-18 | 2017-03-28 | Мария Владимировна Горбачева | Cosmetic |
| CN109381353A (en) * | 2018-11-26 | 2019-02-26 | 深圳市景光生物科技有限公司 | A kind of cream reaching repairing effect of releiving with fat of Oromaius norvaehollandeae |
| RU2691130C1 (en) * | 2018-12-13 | 2019-06-11 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Московская государственная академия ветеринарной медицины и биотехнологии - МВА имени К.И. Скрябина" (ФГБОУ ВО МГАВМиБ - МВА им. К.И. Скрябина) | Cosmetic night cream |
| RU2692057C1 (en) * | 2018-12-13 | 2019-06-20 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Московская государственная академия ветеринарной медицины и биотехнологии - МВА имени К.И. Скрябина" (ФГБОУ ВО МГАВМиБ - МВА им. К.И. Скрябина) | Cosmetic day cream |
| CN113440618A (en) * | 2021-07-06 | 2021-09-28 | 朱景平 | Transdermal matrix and preparation method thereof |
| CN114732803A (en) * | 2022-04-26 | 2022-07-12 | 长江大学 | Vaseline containing ostrich oil and fat and preparation method thereof |
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Application publication date: 20110202 |