CN101961304B - Shell talcum powder - Google Patents

Shell talcum powder Download PDF

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Publication number
CN101961304B
CN101961304B CN2010102951592A CN201010295159A CN101961304B CN 101961304 B CN101961304 B CN 101961304B CN 2010102951592 A CN2010102951592 A CN 2010102951592A CN 201010295159 A CN201010295159 A CN 201010295159A CN 101961304 B CN101961304 B CN 101961304B
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China
Prior art keywords
shell
talcum powder
parts
conch meal
conch
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Expired - Fee Related
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CN2010102951592A
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Chinese (zh)
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CN101961304A (en
Inventor
李�泳
张兆霞
洪鹏志
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Guangdong Ocean University
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Guangdong Ocean University
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Abstract

The invention discloses shell talcum powder and a preparation method thereof, relating to the field of sterilization skin care. The talcum powder consists of the following components in part by weight: 70 to 90 parts of shell powder, 5 to 10 parts of zinc oxide, 2 to 8 parts of boric acid, 5 to 10 parts of zinc stearate, 1 to 3 parts of urea, 0.05 to 0.5 part of menthol, 0.1 to 0.15 part of Nipagin ester, and 0.1 to 0.5 part of essence. The talcum powder is dry and smooth, has the functions of absorbing moisture, dispelling itch, breathing, sterilizing and disinfecting, and smoothing skin, can reduce discomfort caused by secretion and sweat, and is a perfect product for skin care in daily life of people.

Description

A kind of shell talcum powder
Technical field
The invention belongs to the sterilizing skin-protective field, concrete, relate to a kind of shell talcum powder and preparation method thereof.
Background technology
Human body skin is because perspire under damp and hot stuffy condition, causes various dermatosiss easily; Serious especially like miliaria, eczema etc., particularly summer, for this type of phenomenon takes place in prevention; People generally use talcum powder and are coated on the skin, make the skin surface smooth state that keeps dry.Along with China's constant development of economy, living standards of the people improve constantly, and talcum powder progresses into average family as requisite cleaning supplies in the modern life, for people's lives bring great convenience.Now, the talcum powder that is used to clean, though a multitude of names, its product is many to adopt Pulvis Talci as base material with traditional handicraft production mostly, though it has the hygroscopic desiccation effect, does not have sterilizing function.Pulvis Talci is a kind of mineral relevant with asbestos, sees the fiber of sharp type asbestiform at microscopically, and research worker is through obtaining multiple disease research, and human body should avoid contacting Pulvis Talci as far as possible, to reduce ill probability.1973, U.S. food Surveillance Authority one draft clearly limited the content of the similar asbestos fibre material of used for cosmetic Pulvis Talci, and cosmetic field has reduced the consumption of this type of material at present.1993, Research in China mechanism carried out a zoopery and has found, even use the Pulvis Talci that does not contain the asbestiform fiber, also can cause sucking this talcous mouse and suffer from pain, thereby the explanation Pulvis Talci is deleterious to health.Present talcum powder on the market generally all contains Pulvis Talci, and content must produce adverse consequences to human body up to 60~95 in the prescription.Natural botanical toilet powder is at the early-stage in China, like patent CN91100730.X, but just with starch in replace the part Pulvis Talci, and technology complicacy.
Summary of the invention
The object of the present invention is to provide a kind of shell talcum powder, concrete to have provided a kind of be the sterilizing type talcum powder of base material with the conch meal.A kind of method for preparing of shell talcum powder is provided simultaneously.Complex process, no disinfection function or the disinfection sanitizer cost that the present invention mainly solves existing talcum powder existence is high, side effect is big, cost is high and the shortcoming of absorption transparent performance difference.
For realizing the foregoing invention purpose, the technical scheme that the present invention adopts is that this shell talcum powder is to be processed by the raw material of following parts by weight: 70~90 parts of conch meals; 5~10 parts of zinc oxide, 2~8 parts of boric acid, 5~10 parts of zinc stearates; 1~3 part in carbamide; 0.05~0.5 part of Mentholum, 0.1~0.15 part of Nipagin ester, 0.1~0.5 part in essence;
It is subsequent use to be ground into 150~400 purpose conch meals to pretreated shell on request; After in proportion conch meal, zinc oxide, boric acid, zinc stearate, carbamide, Mentholum, Nipagin ester, the various raw materials of essence being prepared, join in the dry powder blender and stirred 10~30 minutes, discharging is a product.Wherein, described washing and alkali cleaning or pickling are meant earlier and wash with NaOH or the HCl aqueous solution soaking with 0.01% concentration behind the clear water, with dirt and the residual slough of removing shell surface; Described washing again is exactly the shell washing by soaking after cleaning, with alkali or the sour material of removing shell absorption with clear water; The described conch meal that is meant after the washing that grinds is broken into 150~400 purpose conch meals; Described drying is meant that ground conch meal is dry under 40~100 ℃ of temperature, to remove the entrained water of crystallization of conch meal; Described shell talcum powder is characterized in that used zinc oxide, boric acid, zinc stearate, carbamide are the 150 purpose powders that are not less than through obtaining after the pulverization process separately; Described Nipagin ester comprises one or more in methyl hydroxybenzoate, ethyl hydroxybenzoate, propylparaben, butoben, nipalgin monooctyl ester and the compound Nipagin ester.Described Mentholum, Nipagin ester and essence are after being formulated into alcoholic solution, join with the vaporific method that sprays in the mixture of other component of talcum powder.
The method for preparing of shell talcum powder is characterized in that, the shell talcum powder is to be processed by the raw material of following weight portion: 70~90 parts of conch meals; 5~10 parts of zinc oxide, 2~8 parts of boric acid, 5~10 parts of zinc stearates; 1~3 part in carbamide; 0.05~0.5 part of Mentholum, 0.1~0.15 part of Nipagin ester, 0.1~0.5 part in essence;
Method for preparing:
(1) shell cleans with clear water earlier, and the NaOH of reuse 0.01% concentration or the washing of HCl aqueous solution soaking are with dirt and the residual slough of removing shell surface; At last the shell after alkali cleaning or the pickling is ground into 150~400 purpose conch meals with pulverizer
(2) conch meal of pulverizing is dry under 40~100 ℃ of temperature, to remove the entrained water of crystallization of conch meal;
(3) be not less than 150 purpose powders with what zinc oxide, boric acid, zinc stearate, carbamide obtained after the pulverization process separately; After Mentholum, Nipagin ester, essence is mixed with alcoholic solution, join with the vaporific method that sprays in the mixture of other component of talcum powder.
(4) in proportion conch meal, zinc oxide, boric acid, zinc stearate, carbamide, Mentholum, Nipagin ester, the various raw materials of essence are joined and stir 10~30 minutes in the dry powder blender, discharging is a product.
The present invention utilizes conch meal to be primary raw material, it it be not only adsorbent, antibacterial, detergent and nutrient among the present invention, and have adsorbing separation and ion exchange.Contain mass crystallization inorganic matter and natural polymer in the shell, inorganic matter such as calcium carbonate and calcium phosphate, natural polymer such as protein and polysaccharide organically couple together the natural inorganic thing through natural polymer.Since the inorganic phase in the shell and the characteristic size of organic facies at submicron to nanoscale; Be a kind of natural organic---inorganic hybrid material; Guaranteed that shellfish material has inside and formed uniform duct, many apertures and the very big advantage of internal surface area; Cause conch meal to have very strong absorbability, have adsorbing separation and ion exchange, can adsorb perspiration and dirt expeditiously; Shell contains abundant natural chitin class binding agent and active substance; Totally nontoxic not only; And having good adhesive property, chitin itself possesses anticorrosion and prevents the microbial attack function, is natural antibacterial bacteriostatic material; Can reduce the use amount of poisonous antisepsis and sterilization component, even not use; The advantage of these natural structures just is the natural material that serves as talcum powder or talcum powder base material.Simultaneously, shell is a kind of natural resources of cheapness, and is inexhaustible.At present, Comprehensive Utilization of Shells is limited in one's ability, and pile up like a mountain by the sea often can to see shell, rots, and when environment is caused very big pollution, also wastes valuable resource.
Main Ingredients and Appearance Mentholum topical application can be controlled headache, neuralgia, pruritus etc.Be applied to skin, cool sense is at first arranged, the sense of burning of slight thorn is arranged later on, the cool sense of this kind is not that skin temperature reduces, and is that the excite nerve Cold receptor of tip causes.In vitro tests Herba Menthae decoct has inhibitory action to herpes simplex virus, forest virus, mumps virus, and staphylococcus aureus, Staphylococcus albus, alpha streptococcus, group B streptococcus, micrococcus catarrhalis, enteritis coccus, shigella flexneri, anthrax bacillus, diphtheria corynebacterium, Bacillus typhi, bacillus pyocyaneus, escherichia coli etc. are had bacteriostasis; The Oleum menthae external, the cold receptor of the tip that can excite nerve and produce creeping chill, and reflexive cause the variation of deep tissue blood vessel and play antiinflammatory, pain relieving, itching-relieving action.
The Main Ingredients and Appearance zinc oxide in medical and health and food industry, have draw out pus by applying a plaster to the affected part, the function of hemostasis, promoting tissue regeneration by astringents.Boric acid is white powder crystallization or three clinopinacoid flakey gloss crystallizations; Satiny feel is arranged; Be used to produce the aching and limp cream of alkali, disinfectant, astringent, antiseptic etc.; These article are external antibacterial, disinfectant, astringent and antiseptic, and it all has inhibitory action to various bacteria, mycete, and action principle is that it can combine with the amino in the bacterioprotein and play a role; Can be used for irrigation and disinfections such as skin, mucosa, wound, oral cavity, vagina, bladder, also can be used for otitis, burn, scald, eczema etc.Simultaneously, zinc oxide and boric acid generation " synergism " has broad-spectrum skin care effect.Zinc stearate is made lubricant, and nontoxic, pollution-free, the no hazard property of these article has adsorptivity, and skin is had good adhesiveness.
Main Ingredients and Appearance carbamide (urea) is colourless or white needles or bar-shaped crystalline solid; Water-soluble, pure; Be insoluble to ether, chloroform, be alkalescence, carbamide has epiderm skin horny layer and the effect that keeps skin moisturizing of removing; Effectively antibiotic skin-care, anti-chap, anti-chilblain and can suppress staphylococcus aureus, Candida albicans, and almost be free from side effects.Carbamide is for hardware, and advantage is a corroding metal not.Thereby carbamide is skin protectant, antiseptic, antifreezing agent, the antibacterial among the present invention.Main Ingredients and Appearance Nipagin ester, toxicity are extremely low, and be non-stimulated to human body, is good sterilization antiseptic.Parabens is typical growth inhibitor, and it can suppress the transfer of nutrient substance to bacterial cell.Through one of following several means, as permease is quit work, destroy how empty passage, change the pH value gradient of film or the charge potential of film both sides etc., the para hydroxybenzene esters of gallic acid has obviously suppressed the absorption of bacterial cell to nutrient substance.The change of transmembrane potential can prevent the transfer of enzyme substrate and the generation of ATP.The antibacterial mechanism of Nipagin ester: the cell membrane of destroy microorganisms makes intracellular protein denaturation, and can suppress the activity of respiratory enzyme system with the electron transport enzyme system of microbial cell.The bacteriostatic activity of Nipagin ester mainly is that molecular state works, and its intramolecular hydroxyl esterification, and no longer ionization is so it all has good fungistatic effect in the scope of pH 3~8.Nipagin ester is the disinfection sanitizer among the present invention.Nipagin ester and carbamide the two " synergism " have efficient, broad-spectrum, quick, safe sterilization effect.
The specific embodiment
Be broken into the conch meal after handling that to be ground into 150~400 purpose conch meals subsequent use on request; On request used zinc oxide, boric acid, zinc stearate, carbamide be through obtain after the pulverization process separately to be not less than 150 purpose powders subsequent use; After being mixed with alcoholic solution to used Mentholum, Nipagin ester, essence on request, join with the vaporific method that sprays in the mixture of other component of talcum powder.
Embodiment 1
Take by weighing 150 order conch meal 75g, zinc oxide 5g, boric acid 4g, zinc stearate 8g, carbamide 2g, Mentholum 0.08g, pool tortoise beetle ester 0.1g, essence 0.2g adds respectively and mixes, and stirs at normal temperatures 20 minutes, and discharging is a product.
Embodiment 2
Take by weighing 300 order conch meal 90g, zinc oxide 6g, boric acid 4g, zinc stearate 10g, carbamide 2g, Mentholum 0.1g, pool tortoise beetle ester 0.11g, essence 0.2g adds respectively and mixes, and stirs at normal temperatures 15 minutes, and discharging is a product.
Embodiment 3
Take by weighing 200 order conch meal 80g, zinc oxide 5g, boric acid 3g, zinc stearate 10g, carbamide 2g, Mentholum 0.06g, ethyl hydroxybenzoate 0.12g, essence 0.3g adds respectively and mixes, and stirs at normal temperatures 30 minutes, and discharging is a product.
Embodiment 4
Take by weighing 400 order conch meal 85g, zinc oxide 7g, boric acid 4g, zinc stearate 9g, carbamide 1g, Mentholum 0.05g, ethyl hydroxybenzoate 0.1g, essence 0.2g adds respectively and mixes, and stirs at normal temperatures 25 minutes, and discharging is a product.
Embodiment 5
Take by weighing 220 order conch meal 100g, zinc oxide 8g, boric acid 5g, zinc stearate 15g, carbamide 3g, Mentholum 0.1g, butoben 0.15g, essence 0.4g adds respectively and mixes, and stirs at normal temperatures 18 minutes, and discharging is a product.
Embodiment 6
Take by weighing 260 order conch meal 180g, zinc oxide 11g, boric acid 6g, zinc stearate 20g, carbamide 4g, Mentholum 0.15g, butoben 0.2g, essence 0.8g adds respectively and mixes, and stirs at normal temperatures 26 minutes, and discharging is a product.
Embodiment 7
Take by weighing 320 order conch meal 190g, zinc oxide 10g, boric acid 7g, zinc stearate 24g, carbamide 2g, Mentholum 0.12g, propylparaben 0.2g, essence 0.5g adds respectively and mixes, and stirs at normal temperatures 26 minutes, and discharging is a product.
Embodiment 8
Take by weighing 380 order conch meal 200g, zinc oxide 12g, boric acid 10g, zinc stearate 31g, carbamide 5g, Mentholum 0.2g, propylparaben 0.32g, essence 1g adds respectively and mixes, and stirs at normal temperatures 30 minutes, and discharging is a product.
Embodiment 9
Take by weighing 290 order conch meal 190g, zinc oxide 8g, boric acid 6g, zinc stearate 20g, carbamide 3g, Mentholum 0.1g, nipalgin monooctyl ester 0.3g, essence 0.4g adds respectively and mixes, and stirs at normal temperatures 20 minutes, and discharging is a product.
Embodiment 10
Take by weighing 350 order conch meal 300g, zinc oxide 17g, boric acid 15g, zinc stearate 35g, carbamide 5g, Mentholum 0.15g, compound Nipagin ester 0.4g, essence 1g adds respectively and mixes, and stirs at normal temperatures 22 minutes, and discharging is a product.

Claims (4)

1. a shell talcum powder is characterized in that being processed by the raw material of following weight portion: 70~90 parts of conch meals, 5~10 parts of zinc oxide; 2~8 parts of boric acid, 5~10 parts of zinc stearates, 1~3 part in carbamide; 0.05~0.5 part of Mentholum, 0.1~0.15 part of Nipagin ester, 0.1~0.5 part in essence;
It is subsequent use to be ground into 150~400 purpose conch meals to pretreated shell on request; After in proportion conch meal, zinc oxide, boric acid, zinc stearate, carbamide, Mentholum, Nipagin ester, the various raw materials of essence being prepared, join in the dry powder blender and stirred 10~30 minutes, discharging is a product;
Used conch meal is through washing, alkali cleaning or pickling, washes, grinds and dry pretreated conch meal;
Described washing and alkali cleaning or pickling are to wash with NaOH or the HCl aqueous solution soaking with 0.01% concentration behind the clear water earlier, with dirt and the residual slough of removing shell surface;
Described washing again is exactly the shell washing by soaking after cleaning, with alkali or the sour material of removing shell absorption with clear water;
The described conch meal that is meant after the washing that grinds is broken into 150~400 purpose conch meals;
Described drying is meant that ground conch meal is dry under 40~100 ℃ of temperature, to remove the entrained water of crystallization of conch meal.
2. shell talcum powder according to claim 1 is characterized in that used zinc oxide, boric acid, zinc stearate, carbamide are the 150 purpose powders that are not less than through obtaining after the pulverization process separately.
3. shell talcum powder according to claim 1 is characterized in that used Nipagin ester is selected from one or more in methyl hydroxybenzoate, ethyl hydroxybenzoate, propylparaben, butoben or the nipalgin monooctyl ester.
4. shell talcum powder according to claim 1 is characterized in that used Mentholum, Nipagin ester and essence are after being formulated into alcoholic solution, joins with the vaporific method that sprays in the mixture of other component of talcum powder.
CN2010102951592A 2010-09-28 2010-09-28 Shell talcum powder Expired - Fee Related CN101961304B (en)

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Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102773140A (en) * 2011-05-09 2012-11-14 王志平 Manufacturing method for ultrafine shell powder
CN102240256B (en) * 2011-07-07 2012-10-31 赵君雄 Natural acorn talcum powder and preparation technology thereof
CN103284930A (en) * 2013-05-10 2013-09-11 周卫忠 Preparation method of pure natural talcum powder
CN105411875A (en) * 2015-12-14 2016-03-23 安徽丰乐香料有限责任公司 Preparation method of high-content menthol talcum powder
CN106361614A (en) * 2016-11-28 2017-02-01 无比滴(广东)药业有限公司 Baby talcum powder
CN106727130A (en) * 2016-12-22 2017-05-31 江西宜信堂医疗科技有限公司 A kind of mosquito-expelling talcum powder and preparation method thereof
CN107898738A (en) * 2017-11-30 2018-04-13 浙江海洋大学 One kind is based on modified mussel shell framework material suncream and its preparation
CN108210435A (en) * 2018-03-02 2018-06-29 合肥仙之峰农业科技有限公司 It is a kind of to sterilize the acne green spot eliminating skin care suncream and preparation method thereof that disappears
CN109044858A (en) * 2018-09-18 2018-12-21 广东山石微量元素研究院(普通合伙) A kind of Khotan jade talcum powder
CN109652835B (en) * 2018-12-28 2020-09-25 重庆新久融科技有限公司 Easy-demoulding aluminum alloy template and preparation method thereof

Family Cites Families (3)

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Publication number Priority date Publication date Assignee Title
CN1058713A (en) * 1990-08-07 1992-02-19 中国有色金属工业总公司矿产地质研究院 A kind of talcum powder
CN1454587A (en) * 2002-04-30 2003-11-12 胡世珍 Talcum powder with disinfecting effect
JP2008105947A (en) * 2005-02-10 2008-05-08 Asada Shokai:Kk Cream containing burned powder of shell or the like, and method of producing the same

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