CN101940242A - Grease composition of infant formula food - Google Patents
Grease composition of infant formula food Download PDFInfo
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- CN101940242A CN101940242A CN 201010225885 CN201010225885A CN101940242A CN 101940242 A CN101940242 A CN 101940242A CN 201010225885 CN201010225885 CN 201010225885 CN 201010225885 A CN201010225885 A CN 201010225885A CN 101940242 A CN101940242 A CN 101940242A
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Abstract
The invention discloses a grease composition of infant formula food. The grease composition comprises the following components in percentage by weight: 20 to 80 percent of fat of Pangasianodon gigas or liquid component fractionated therefrom, and 80 to 20 percent of animal/vegetable grease mixture. The grease composition is similar to breast milk fat in terms of fatty acid composition and triglyceride distribution and can be used as a grease ingredient of the infant formula food, and additional AA and DHA is not needed or only a small amount of AA or DHA is added.
Description
Technical field
The present invention relates to a kind of fat or oil composition that is used for infant formula.
Background technology
Breast milk is the most perfect food of baby.It offers required various physiologically active speciality of baby and enough nutrition comprehensively, also offer the necessary but essential fatty acid that can not synthesize again in the body etc. of baby, can grow up healthy and sound, avoid the invasion and attack of numerous disease etc. in birth in six months to guarantee the baby.When breast milk can not satisfy baby's needs fully, babies ' formula milk powder was best substitute.Best babies ' formula milk powder, be on nutritional labeling with the complete approaching formula milk of breast milk.Formula milk is to be matrix with milk, adjusts the product of nutrients such as protein, carbohydrate, fat, vitamin and mineral matter.Entered since 21 century; babies ' formula milk powder still is in the imitation breast milk stage; with the breast milk is standard, adds whey powder, protein hydrolysate, compound sugar, vegetable oil, vitamin, mineral matter, taurine, AA and DHA etc. in formula milk, and nutritional labeling is as far as possible near breast milk.The lipid that contains 3%-5% in the breast milk, 98% with lipid be glycerine trigalloyl ester, it is one of main nutrient matter in the breast milk, offers about 45% (0-6 month) and 30%-40% (7-12 month) of baby institute energy requirement, and extremely important for the growth of organs such as brain.
During breast milk fatty acids is formed, the oleic acid content maximum, unsaturated acids (mainly referring to C18:1, C18:2 and C18:3) mainly is distributed in Sn-1,3, but the most special with Sn-2 aliphatic acid, 40% saturated fatty acid is distributed in Sn-2, and the 60%-70% of palmitic acid is in the Sn-2 position.This characteristic distributions obviously is different from general vegetable oil (the Sn-2 position is mainly unsaturated acids).Just because of these characteristics are arranged, the sweet three ester types of fat are mainly Sn-USU type (U refers to unsaturated acids, and S refers to saturated acid) in the human milk, as Sn-OPO, and Sn-OPL (O refers to that oleic acid, P refer to that palmitic acid, L refer to linoleic acid) etc.
The characteristics of digesting and assimilating of human milk fat: characteristics that breast milk fatty acids is formed and baby's self absorption characteristics are closely related.Human milk fat passes through the hydrolysis of stomach lipolytic enzyme earlier in infants, this kind of enzyme is for Sn-1,3 have certain selectivity, sweet three esters are hydrolyzed into free fatty and Sn-2 monoglyceride, but not every aliphatic acid is the energy good absorption all, just is not so good as middle carbochain saturated acid (C8:0-C12:0) and unsaturated acids as long carbochain saturated ester (C14:0-C18:0) and easily digests and assimilates.This mainly is because long carbochain saturated acid forms stodgy soap in small intestine, has disturbed the absorption of baby to metal ion (as calcium ion) and aliphatic acid.Especially, in small intestine the absorption of free C16:0 very low, only 63%, and free C18:1 ω 9, C18:2 ω 9 can reach more than 90%.Because of free C16:0 easily and metal ion form insoluble calcium soap, thereby cause the loss of calcium ion and energy etc.The Sn-2 monoglyceride is to digest and assimilate with the monoglyceride form in small intestine, and C16:0 is in the Sn-2 position, and promptly the palmitic acid monoglyceride is beneficial to the absorption of baby to fat, also influences the metabolism of cholesterol simultaneously.This absorption pattern the sixth of the twelve Earthly Branches is through being confirmed, and the 1.2-1.4 that the absorption of being rich in the lard of C16:0 for the Sn-2 position as the baby is it after ester exchange at random doubly.
At present, adipose-derived in the infant formula has following several;
(1) directly use cow's milk fat:
Directly replace human milk fat with cow's milk fat, there are notable difference in the composition of sweet three ester aliphatic acid wherein and distribution and human milk fat.C16:0 accounts for 45% of its total amount in the Sn-2 position in the cow's milk fat, is lower than 70% in the human milk fat; Unsaturated fatty acid content in the cow's milk fat is starkly lower than human milk fat.
(2) directly be in harmonious proportion with vegetable oil:
Directly be in harmonious proportion with vegetable oil, aliphatic acid is formed and can be met the requirements well, but different with human milk fat on sweet three ester structures.
(3) carry out ester exchange at random with miscella:
Carry out ester exchange at random with miscella, it is similar that aliphatic acid is formed, and can accomplish that also the composition of Sn-2 position is similar, but structure is Sn-1 in this product, 3 unrighted acid Sn-2, and the content of saturated fatty acid (OPO or OPL) is less.
(4) to be rich in the grease of palmitic acid on the enzyme process ester exchange acquisition Sn-2 position:
Can produce the product that structure comparatively meets with this kind method, but complex process, production cost is very high.
(5) sweet three ester structures of lard fat are very near human milk fat, be rich in Sn-1, sweet three esters of 3 unrighted acid Sn-2 saturated fatty acids (mainly being palmitic acid) structure, wherein about 67% palmitic acid is distributed on the Sn-2 position, is a kind of very desirable human milk fat substituted raw material.Japan, Korea S have food company that the fraction leach-s/tive of lard is added in the babies ' formula milk powder as the grease batching.But there is religious taboo in lard as edible oil, can not be widely used as glyceride stock.
Summary of the invention
The objective of the invention is to the above problem, provide a kind of and human milk fat approaching fat or oil composition that is used for infant formula in aliphatic acid composition and the distribution of sweet three esters at the fat existence in the existing infant formula.
The fat or oil composition that is used for infant formula of the present invention, it consists of: in weight percentage,
Derive from fat of Mekong Delta catfish (Pangasianodon gigas) or the liquid component 20%-80% that its branch is carried,
Other vegetable and animals oils lipoprotein mixture 80%-20%.
Described Mekong Delta catfish (Pangasianodon gigas) is meant Ba Sha catfish (basa catfish), the short, bristly hair or beard catfish (tra catfish) that derives from Mekong Delta.Desirable wherein one or both.
The described fat that derives from Mekong Delta catfish (Pangasianodon gigas) is the catfish fat that extracts from the full fish of Mekong Delta catfish (Pangasianodon gigas) or extract from all the other later positions of removal fillet.
As preferred version, the extracting method of described catfish fat is: Mekong Delta catfish raw material is cleaned, full fish pulverized maybe will remove raw material remaining behind the fillet and pulverize, pass through continuously cooking then, press filtration is used Steam Heating 20-60 minute with filtrate, centrifugal then, the crude fat that obtains dewaters, and refining then promptly gets catfish fat.
As preferred version, the branch extracting method of the liquid component that the branch of described catfish fat is carried is: Mekong Delta catfish fat is heated to 55-60 ℃, after stablizing 20 minutes, be cooled to 30 ℃ with 10 ℃/hour speed, be cooled to 10-30 ℃ with 1.5-2.5 ℃/hour speed again, thermostatical crystallization 3-5 hour, aforementioned all processes add band and stir, after solid crystal to be separated out partly reaches the 10-50% of gross weight, under temperature 10-30 ℃, begin to carry out isolated by filtration, after filtering, obtain branch extract body component.
Described other vegetable and animals oils lipoprotein mixture is meant the whole or wherein several any mixture in soybean oil, Canola Oil, sunflower oil, corn oil, high oleic sunflower oil, coconut oil, palm-kernel oil, the butterfat.As preferred version, in the composition of described other vegetable and animals oils lipoprotein mixture, except that butterfat, at least a grease is through enzyme process or chemistry ester exchange at random, and making the content of palmitic acid on the Sn-2 position of other vegetable and animals oils lipoprotein mixture of gained is 30-33.3%.
The aliphatic acid of catfish fat of the present invention table 1 composed as follows:
Table 1
With catfish fat under 10-30 ℃ of condition through too carrying, shown in the aliphatic acid table 2 composed as follows of the branch extract body component that obtains:
Table 2
According to statistics, shown in the table 3 composed as follows of the aliphatic acid of typical human milk fat:
| Fatty acid type | The content of aliphatic acid (%) |
| C8:0 | 0.20±0.43 |
| C10:0 | 1.38±0.27 |
| C12:0 | 5.29±1.67 |
| C14:0 | 4.45±1.64 |
| C16:0 | 17.62±1.96 |
| C16:1 | 2.09±0.35 |
| C18:0 | 4.26±0.74 |
| C18:1 | 34.19±3.09 |
| C18:2 | 26.15±5.25 |
| C18:3 | 2.85±0.53 |
| C20:4 | 0.76±0.11 |
| C22:6 | 0.41±0.11 |
Table 3
Fat and human milk fat contrast with the Mekong Delta catfish, be all to lack C8:0 in catfish fat or the liquid component that after too carrying, obtains as can be seen, C10:0, SCFA and C18:2 such as C12:0, polyunsaturated fatty acids such as C18:3.For can replenishing coconut oil, palm-kernel oil and branch thereof in grease, additional SCFA puies forward component; And can be to wherein replenishing soybean oil, Canola Oil, sunflower oil, corn oil, rice bran oil, safflower seed oil, perilla herb oil and flax wet goods in order to increase polyunsaturated fatty acid.
For more being approached the fat or oil composition of human milk fat, the present invention can adopt following steps:
1. the fat of Mekong catfish is divided and carries, with minute extract body component as base-material.Divide the purpose of carrying to have two: the one, the content of palmitic acid on the raising Sn-2 position; The 2nd, reduce the content of total saturated fatty acid, thereby in subsequent handling, add the mixed plant grease that palmitic acid content is lower on the Sn-2 position less, to increase the content of the last palmitic acid of Sn-2 in the final fat or oil composition.
2. the mixture with vegetable fat carries out enzyme process or chemical ester exchange.The vegetable fat of self-sow, saturated fatty acid mainly are positioned at Sn-1, and on 3, and unrighted acid mainly is positioned on the Sn-2 position.If directly the mixture with vegetable oil mixes with the liquid component that fat or its branch of Mekong Delta catfish are carried, because the content lower (being no more than 33.3%) of the palmitic acid on the Sn-2 position in the mixed plant grease, the content of the palmitic acid in the resulting end-product on the total Sn-2 position has bigger reduction.The content of the palmitic acid on the Sn-2 position in the mixed vegetable oil after the ester exchange can reach 33.3%, the liquid component of carrying with catfish fat or its branch mixes the end-product that obtains mutually, with respect to the mixed plant grease of not ester exchange, the content of the palmitic acid on its Sn-2 position can increase to some extent.
Technique effect of the present invention is: the present invention adopts and derives from Mekong Delta catfish (basa ﹠amp; Tra catfish) as the main base-material of sweet three esters of USU type (unrighted acid-saturated fatty acid-unrighted acid), mix other animal and plant fat and contrast the aliphatic acid that is lacked with human milk fat to replenish catfish fat, thereby provide a kind of and human milk fat approaching human milk fat substituted thing in aliphatic acid composition and the distribution of sweet three esters, prepare burden as the grease in the infant formula.Fat or oil composition of the present invention can overcome the defective that the fat in above-mentioned cited four kinds of existing infant formulas exists, and does not need additionally to add AA and DHA or only need add a spot of AA or DHA.
The specific embodiment
Embodiment one:
A kind of preparation method of the fat or oil composition that is used for infant formula is as follows:
1, extract Mekong Delta catfish fat:
The Ba Sha catfish (basa catfish) that derives from Mekong Delta is cleaned, extract fillet then, remaining raw material after removing fillet is pulverized, through carry out continuously cooking in continuous cooking machine, Steam Heating 20-60 minute used in press filtration after the slagging-off then, then that the crude fat that obtains is centrifugal, through the dehydration of flash distillation program, final purification gets catfish fat finished product again.
Mature technology is adopted in refining described in the embodiment of the invention, and concrete steps comprise: come unstuck, depickling, decolouring and deodorization.The deodorization stage wherein is by carrying out under 240 ℃ of temperature, 65 minutes time of staying, the vacuum 2.3mbar condition.
2, the grease branch is carried:
The Mekong Delta catfish fat that previous step is obtained is heated to 55-60 ℃, after stablizing 20 minutes, be cooled to 30 ℃ with 10 ℃/hour speed, be cooled to 15 ℃ with 1.5-2.5 ℃/hour speed again, thermostatical crystallization 3-5 hour, aforementioned all processes added band and stir, after solid crystal to be separated out partly reaches the 10-50% of gross weight, begin to carry out isolated by filtration under 15 ℃ of temperature, initial filter pressure is 3bar, is forced into 12bar and stops.After filtering, obtain branch extract body component.
3, stearic exchange:
Coconut oil and soybean oil are mixed by 1: 2 weight ratio, heat to 100 ℃, stir simultaneously, keep 20min, dehydration.Add the sodium methoxide fine catalyst, catalyst concn 0.2%, 95 ℃ of reaction temperatures, time 45min.Reaction finish to add oil, and to weigh 12% concentration be 8% aqueous citric acid solution, continues to stir 20min.Soap is taken off in washing.Reactant is heated to 100 ℃ after taking off soap, keeps the carclazyte of 20min. adding 2%, keeps 20min down at 110 ℃.Filter, ester exchange is finished, and carries out refining again.
4, grease mixes:
As shown in the table, the branch extract body component of above-mentioned Mekong Delta catfish fat is mixed in proportion with other glyceride stock, the compound lard of making is a kind of aliphatic acid and forms and sweet three ester structures and the approaching fat or oil composition that is used for infant formula of human milk fat.The compound lard that carries out the ester exchange gained after coconut oil and soybean oil mix by 1: 2 weight ratio in the table is got the compound lard of above-mentioned the 3rd step gained.
| Fat type | Percentage composition (wt%) |
| The branch extract body component of Mekong catfish fat | 60 |
| Butterfat | 16 |
| After mixing by 1: 2 weight ratio, coconut oil and soybean oil carry out the compound lard of ester exchange gained | 24 |
Embodiment two:
A kind of preparation method of the fat or oil composition that is used for infant formula is as follows:
The extraction of catfish fat is with embodiment one.
Mekong Delta catfish fat is mixed in proportion with other several glyceride stocks shown in the following table, and the compound lard of making is a kind of aliphatic acid and forms and sweet three ester structures and the approaching fat or oil composition that is used for infant formula of human milk fat.
| Fat type | Percentage composition (wt%) |
| Mekong catfish fat | 70 |
| Coconut oil | 10 |
| Soybean oil | 20 |
Embodiment three:
A kind of preparation method of the fat or oil composition that is used for infant formula is as follows:
The step that the extraction of catfish fat, grease branch are carried, stearic exchanges is with embodiment one.
As shown in the table, Mekong Delta catfish fat resulting liquid component after too carrying is mixed through the compound lard that the stearic clearing house gets in proportion with other several glyceride stock mixtures, the compound lard of making is a kind of aliphatic acid and forms and sweet three ester structures and the approaching fat or oil composition that is used for infant formula of human milk fat.
Embodiment four:
A kind of preparation method of the fat or oil composition that is used for infant formula is as follows:
The extraction of catfish fat, grease branch are put forward step with embodiment one.
As shown in the table, Mekong Delta catfish fat resulting minute extract body component after too carrying mixed in proportion with other several glyceride stocks, the compound lard of making is a kind of aliphatic acid and forms and sweet three ester structures and the approaching fat or oil composition that is used for infant formula of human milk fat.
| Fat type | Percentage composition (wt%) |
| The branch extract body component of Mekong catfish fat | 80 |
| Palm-kernel oil | 10 |
| Soybean oil | 5 |
| Sunflower oil | 5 |
Claims (9)
1. fat or oil composition that is used for infant formula is characterized in that it consists of: in weight percentage,
Derive from fat of Mekong Delta catfish (Pangasianodon gigas) or the liquid component 20%-80% that its branch is carried,
Other vegetable and animals oils lipoprotein mixture 80%-20%.
2. the fat or oil composition that is used for infant formula according to claim 1 is characterized in that: described Mekong Delta catfish (Pangasianodon gigas) is meant Ba Sha catfish (basa catfish), the short, bristly hair or beard catfish (tra catfish) that derives from Mekong Delta.
3. the fat or oil composition that is used for infant formula according to claim 1 and 2 is characterized in that: the described fat that derives from Mekong Delta catfish (Pangasianodon gigas) is the catfish fat that extracts from the full fish of Mekong Delta catfish or extract from all the other later positions of removal fillet.
4. the fat or oil composition that is used for infant formula according to claim 3, it is characterized in that: the extracting method of described catfish fat is, Mekong Delta catfish raw material is cleaned, full fish is pulverized maybe will remove behind the fillet raw material of remainder and pulverize, pass through continuously cooking then, press filtration, filtrate is used Steam Heating 20-60 minute, and centrifugal then, the crude fat that obtains dewaters, refining then promptly gets catfish fat.
5. the fat or oil composition that is used for infant formula according to claim 1 and 2, it is characterized in that: the branch extracting method of the liquid component that described branch is carried is, Mekong Delta catfish fat is heated to 55-60 ℃, after stablizing 20 minutes, be cooled to 30 ℃ with 10 ℃/hour speed, be cooled to 10-30 ℃ with 1.5-2.5 ℃/hour speed again, thermostatical crystallization 3-5 hour, aforementioned all processes add band and stir, after solid crystal to be separated out partly reaches the 10-50% of gross weight, under 15 ℃ of temperature, begin to carry out isolated by filtration, after filtering, obtain branch extract body component.
6. the fat or oil composition that is used for infant formula according to claim 5 is characterized in that: described minute the preferred 15-25 of temperature raising degree ℃.
7. the fat or oil composition that is used for infant formula according to claim 1 and 2 is characterized in that: described other vegetable and animals oils lipoprotein mixture is meant the whole or wherein several any mixture in soybean oil, Canola Oil, sunflower oil, corn oil, high oleic sunflower oil, coconut oil, palm-kernel oil, the butterfat.
8. the fat or oil composition that is used for infant formula according to claim 7, it is characterized in that: in the composition of described other vegetable and animals oils lipoprotein mixture, except that butterfat, at least a grease is through enzyme process or chemistry ester exchange at random, and making the content of palmitic acid on the Sn-2 position of other vegetable and animals oils lipoprotein mixture of gained is 30-33.3%.
9. the fat or oil composition that is used for infant formula according to claim 7 is characterized in that: described butterfat exists with the form of whole milk powder, and the weight of butterfat is pressed 26% of whole milk powder and calculated.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103766506A (en) * | 2012-10-23 | 2014-05-07 | 丰益(上海)生物技术研发中心有限公司 | Grease composition |
| CN105028659A (en) * | 2015-05-14 | 2015-11-11 | 江南大学 | Human milk substitute fat composition |
| WO2016101891A1 (en) * | 2014-12-24 | 2016-06-30 | Wilmar (Shanghai) Biotechnology Research & Development Center Co., Ltd | An oil/fat composition and a preparation method for the same |
| CN105994652A (en) * | 2016-06-08 | 2016-10-12 | 华南理工大学 | Formula milk powder for infants and young children |
| CN107072279A (en) * | 2014-07-16 | 2017-08-18 | Mjn美国控股有限责任公司 | Alimentation composition containing oily blend and application thereof |
| CN107105739A (en) * | 2014-12-19 | 2017-08-29 | 雀巢产品技术援助有限公司 | Infant nutrition containing aminosal and palmitic acid |
| CN107549313A (en) * | 2017-10-12 | 2018-01-09 | 中国农业科学院农产品加工研究所 | Baby milk grease compound method based on triglycerides analysis mode human milk fat |
| JP2020162444A (en) * | 2019-03-28 | 2020-10-08 | 日油株式会社 | Fat for modified milk powder, fat composition for modified milk powder, and modified milk powder |
| CN112314710A (en) * | 2020-08-21 | 2021-02-05 | 南昌大学 | Preparation method and application of Chinese breast milk triglyceride substitute fat |
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| CN103766506A (en) * | 2012-10-23 | 2014-05-07 | 丰益(上海)生物技术研发中心有限公司 | Grease composition |
| CN107072279A (en) * | 2014-07-16 | 2017-08-18 | Mjn美国控股有限责任公司 | Alimentation composition containing oily blend and application thereof |
| CN107105739A (en) * | 2014-12-19 | 2017-08-29 | 雀巢产品技术援助有限公司 | Infant nutrition containing aminosal and palmitic acid |
| WO2016101891A1 (en) * | 2014-12-24 | 2016-06-30 | Wilmar (Shanghai) Biotechnology Research & Development Center Co., Ltd | An oil/fat composition and a preparation method for the same |
| CN105779141A (en) * | 2014-12-24 | 2016-07-20 | 丰益(上海)生物技术研发中心有限公司 | Grease composition and preparation method thereof |
| CN105028659A (en) * | 2015-05-14 | 2015-11-11 | 江南大学 | Human milk substitute fat composition |
| CN105028659B (en) * | 2015-05-14 | 2018-10-30 | 江南大学 | A kind of human milk replacement oil/fat composition |
| CN105994652A (en) * | 2016-06-08 | 2016-10-12 | 华南理工大学 | Formula milk powder for infants and young children |
| CN107549313A (en) * | 2017-10-12 | 2018-01-09 | 中国农业科学院农产品加工研究所 | Baby milk grease compound method based on triglycerides analysis mode human milk fat |
| JP2020162444A (en) * | 2019-03-28 | 2020-10-08 | 日油株式会社 | Fat for modified milk powder, fat composition for modified milk powder, and modified milk powder |
| JP7283176B2 (en) | 2019-03-28 | 2023-05-30 | 日油株式会社 | Oil and fat for infant formula, oil and fat composition for infant formula, and infant formula |
| CN112314710A (en) * | 2020-08-21 | 2021-02-05 | 南昌大学 | Preparation method and application of Chinese breast milk triglyceride substitute fat |
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