CN101880599A - Waxberry leaf extract and application thereof as tobacco product additives - Google Patents
Waxberry leaf extract and application thereof as tobacco product additives Download PDFInfo
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- CN101880599A CN101880599A CN2009100619970A CN200910061997A CN101880599A CN 101880599 A CN101880599 A CN 101880599A CN 2009100619970 A CN2009100619970 A CN 2009100619970A CN 200910061997 A CN200910061997 A CN 200910061997A CN 101880599 A CN101880599 A CN 101880599A
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- leaf extract
- waxberry leaf
- waxberry
- tobacco
- extraction agent
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- 239000000284 extract Substances 0.000 title claims abstract description 61
- 235000007270 Gaultheria hispida Nutrition 0.000 title claims abstract description 48
- 235000009134 Myrica cerifera Nutrition 0.000 title claims abstract description 48
- 235000012851 Myrica pensylvanica Nutrition 0.000 title claims abstract description 48
- 235000019505 tobacco product Nutrition 0.000 title claims abstract description 25
- 239000000654 additive Substances 0.000 title claims abstract description 18
- 244000024215 Myrica gale Species 0.000 title claims description 43
- 241000208125 Nicotiana Species 0.000 claims abstract description 28
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 28
- 238000000605 extraction Methods 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims abstract description 24
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 19
- 238000000926 separation method Methods 0.000 claims abstract description 16
- 238000001914 filtration Methods 0.000 claims abstract description 15
- 239000002253 acid Substances 0.000 claims abstract description 13
- 238000001556 precipitation Methods 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000003205 fragrance Substances 0.000 claims abstract description 7
- 150000007524 organic acids Chemical class 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims abstract description 3
- 239000002798 polar solvent Substances 0.000 claims abstract description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 235000019504 cigarettes Nutrition 0.000 claims description 28
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 230000000996 additive effect Effects 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 230000001105 regulatory effect Effects 0.000 claims description 12
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 5
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 5
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 5
- 239000000920 calcium hydroxide Substances 0.000 claims description 5
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 5
- 239000003546 flue gas Substances 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 235000017550 sodium carbonate Nutrition 0.000 claims description 5
- 239000003513 alkali Substances 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 230000002378 acidificating effect Effects 0.000 claims description 2
- 238000004090 dissolution Methods 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 6
- 239000000779 smoke Substances 0.000 abstract description 4
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 244000269152 Myrica pensylvanica Species 0.000 abstract 5
- 239000000463 material Substances 0.000 abstract 2
- 239000002198 insoluble material Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 23
- 238000012360 testing method Methods 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 3
- -1 flavonoid compounds Chemical class 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- KJXSIXMJHKAJOD-LSDHHAIUSA-N (+)-dihydromyricetin Chemical compound C1([C@@H]2[C@H](C(C3=C(O)C=C(O)C=C3O2)=O)O)=CC(O)=C(O)C(O)=C1 KJXSIXMJHKAJOD-LSDHHAIUSA-N 0.000 description 2
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
- HVQAJTFOCKOKIN-UHFFFAOYSA-N flavonol Natural products O1C2=CC=CC=C2C(=O)C(O)=C1C1=CC=CC=C1 HVQAJTFOCKOKIN-UHFFFAOYSA-N 0.000 description 2
- 235000011957 flavonols Nutrition 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000013355 food flavoring agent Nutrition 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 1
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- KQILIWXGGKGKNX-UHFFFAOYSA-N dihydromyricetin Natural products OC1C(=C(Oc2cc(O)cc(O)c12)c3cc(O)c(O)c(O)c3)O KQILIWXGGKGKNX-UHFFFAOYSA-N 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 150000007946 flavonol Chemical class 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 235000019633 pungent taste Nutrition 0.000 description 1
- 235000005875 quercetin Nutrition 0.000 description 1
- 229960001285 quercetin Drugs 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Abstract
The invention relates to a waxberry leaf extract and application thereof as tobacco product additives. The waxberry leaf extract is obtained according to the following steps: adopting waxberry leaves as extraction raw materials; adopting polar solvents as extraction agents; carrying out extraction reaction in an alkaline medium; carrying out filtering separation after the extraction is completed to obtain material liquid; carrying out precipitation separation on the material liquid by organic acid under the acid condition and collecting precipitation products; dissolving the precipitation products by the extraction agents again; and then, separating insoluble materials to obtain the waxberry leaf extract of the invention. The extract of the invention can be used as tobacco product additives to be added into shredded tobacco of tobacco, can effectively enhance the fragrance during the tobacco product smoking, has rich fragrance, and improves the intense effect of the smoke. In addition, the waxberry leaf extract can also give unique odor nuance and odor note to the tobacco products.
Description
Technical field
The present invention relates to the application of a kind of natural plant extracts in tobacco product, specifically a kind of Waxberry leaf extract and as the purposes of additive of tobacco product.
Background technology
" Chinese style cigarette " core competitiveness is to form the selling point style, embodies personalization and differentiation, adapts to sucking of Chinese consumers in general and is accustomed to and consumer need.Chinese style cigarette essence and flavoring agent is Chinese style cigarette product " soul ", is the secret place that " Chinese style cigarette " style characteristic forms.Flavoring and casing scientifically in cigarette, the important means of the personalized style of outstanding cigarette product just.Simultaneously, in order to improve the security of smoking, lowering harm and decreasing coking becomes an important component part of " Chinese style cigarette ".When reducing coke tar in cigarette, promote and raising flue gas concentration and fragrance, also only by means of the flavoring and casing technology.Along with going deep into of Chinese style cigarette lowering harm and decreasing coking work, reinforced its importance that demonstrates further of tobacco flavoring.Extracting essence and flavoring agent from the natural herbal plant, succession herbal medicine in thousand is used for cigarette, allow healthy theory along with the refined perfume (or spice) of cigarette, move towards the human consumer together, is one of fundamental research of development " Chinese style cigarette ".
Contain multiple flavonoid compounds such as ampelopsin, Quercetin in the Folium Myricae rubrae, have prospect as essence spice for cigarette.And isolating 4 kinds of flavonol glucosides and a kind of these 5 kinds of flavonoid compound of flavonol all have significant antioxidant role from Folium Myricae rubrae, can remove peroxy radical, can be used for the work of cigarette harm reduction.But the achievement in research that sees report at present has only Folium Myricae rubrae to be used in Chinese medicine and correlated product, the wine brewing, and not seeing has the bibliographical information that is used to cigaret additive.And in our research process, discovery is simple to have bigger negative effect by the resulting Waxberry leaf extract of conventional extraction process, can't satisfy the service requirements as cigaret additive.
Summary of the invention
Purpose of the present invention is exactly the defective at prior art, provides a kind of Waxberry leaf extract and as the purposes of additive of tobacco product.
Technical scheme of the present invention is achieved in that it is to adopt Folium Myricae rubrae to extract raw material, with the polar solvent is extraction agent, in alkaline medium, carry out abstraction reaction, extract the after-filtration separation and obtained feed liquid, feed liquid is carried out precipitate and separate and collecting precipitation thing with organic acid under acidic conditions, throw out once more with the extraction agent dissolving, is separated insolubles then, promptly obtain Waxberry leaf extract of the present invention.
Wherein said extraction agent is 40～70% aqueous ethanolic solution; Described alkali is sodium hydroxide, calcium hydroxide, ammoniacal liquor or yellow soda ash; Described acid is toluylic acid, citric acid, oxysuccinic acid or Citric Acid.
Extracting method of the present invention is to adopt Folium Myricae rubrae for extracting raw material, specifically may further comprise the steps: earlier alkali is joined in the extraction agent, regulating extraction agent pH value is 8.0～12.0, extraction agent is 10～20: 1 with the weight ratio of extracting raw material, extracted 1～5 hour at 50～90 ℃, after isolating feed liquid, feed liquid is concentrated into 1/3 of original volume, add organic acid in concentrated solution, regulating the pH value is 3.5～5.5, filtering separation gained precipitation, with 5～10 times of extraction agent dissolvings, the filtering separation insolubles is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains Waxberry leaf extract of the present invention.
Extracting method of the present invention technical scheme preferably is: described extraction agent is 40～70% aqueous ethanolic solution; Described alkali is sodium hydroxide, calcium hydroxide, ammoniacal liquor or yellow soda ash; Described acid is toluylic acid, citric acid, oxysuccinic acid or Citric Acid.
The present invention is the purposes of additive of tobacco product, it is that Waxberry leaf extract is added in the pipe tobacco of cigarette, and the Waxberry leaf extract that is added in the pipe tobacco accounts for 0.01%～0.05% of pipe tobacco weight, flavouring effectively when tobacco product aspirates, and fragrance is abundant, increases the solid sense of flue gas.The Waxberry leaf extract that wherein is added in the pipe tobacco preferably accounts for 0.02%～0.04% of pipe tobacco weight.
The present invention is during as the purposes of additive of tobacco product, preferably Waxberry leaf extract is dissolved in 70% the ethanol, the alcohol solvent that is dissolved with Waxberry leaf extract rolled at the pipe tobacco of production of cigarettes be sprayed in the process on the pipe tobacco, subsequently evaporating solvent.
A series of experimental study results that smoke panel test of patent applicant show, the Waxberry leaf extract of adding flavouring effectively when tobacco product aspirates, and fragrance is abundant, increases the solid sense of flue gas; And Waxberry leaf extract can also be given the aromatic and the note of tobacco product uniqueness.And when improving the tobacco product mouthfeel, can avoid introducing negative impacts such as assorted gas, increase pungency.
The present invention has opened up a new Application Areas for Waxberry leaf extract, has increased new effect and the effect of Folium Myricae rubrae.Waxberry leaf extract is as additive of tobacco product, and effect is obvious, and " Chinese style cigarette " goods of developing characteristic style are had good application prospects.
Embodiment
The present invention is described further below by embodiment.
The extraction of embodiment 1 Folium Myricae rubrae
Earlier sodium hydroxide is joined in 50% aqueous ethanolic solution, regulating aqueous ethanolic solution pH value is 12.0, the weight ratio of aqueous ethanolic solution and Folium Myricae rubrae is 15: 1, extracted 3 hours at 80 ℃, after isolating feed liquid, feed liquid is concentrated into 1/3 of original volume, in concentrated solution, add toluylic acid, regulating the pH value is 4.5, and filtering separation gained throw out is with 50% aqueous ethanolic solution dissolution precipitation thing of 5 times of weight ratios, filtering separation insolubles once more, feed liquid is concentrated into the medicinal extract shape, and density is 1.1, promptly obtains Waxberry leaf extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 2
Earlier ammoniacal liquor is joined in 60% aqueous ethanolic solution, regulating aqueous ethanolic solution pH value is 8.0, and aqueous ethanolic solution and Folium Myricae rubrae weight ratio are 12: 1, extracted 4 hours at 70 ℃, isolate feed liquid after, feed liquid is concentrated into 1/3 of original volume, in concentrated solution, add citric acid, regulating the pH value is 5.5, and filtering separation gained throw out is with the aqueous ethanolic solution dissolving of 8 times of weight ratios, filtering separation insolubles once more, feed liquid is concentrated into the medicinal extract shape, and density is 1.2, promptly obtains Waxberry leaf extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 3
Earlier calcium hydroxide is joined in 40% aqueous ethanolic solution, regulating aqueous ethanolic solution pH value is 10.0, aqueous ethanolic solution and Folium Myricae rubrae weight ratio are 20: 1, extracted 2 hours at 90 ℃, after isolating feed liquid, feed liquid is concentrated into 1/3 of original volume, in concentrated solution, add Citric Acid, regulating the pH value is 3.5, and filtering separation gained throw out is with the aqueous ethanolic solution dissolving of 10 times of weight ratios, filtering separation insolubles once more, feed liquid is concentrated into the medicinal extract shape, and density is 1.2, promptly obtains Waxberry leaf extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 4
Earlier yellow soda ash is joined in 70% aqueous ethanolic solution, regulating aqueous ethanolic solution pH value is 9.0, aqueous ethanolic solution and Folium Myricae rubrae weight ratio are 18: 1, extracted 5 hours at 60 ℃, after isolating feed liquid, feed liquid is concentrated into 1/3 of original volume, in concentrated solution, add oxysuccinic acid, regulating the pH value is 4.0, and filtering separation gained throw out is with the aqueous ethanolic solution dissolving of 10 times of weight ratios, filtering separation insolubles once more, feed liquid is concentrated into the medicinal extract shape, and density is 1.1, promptly obtains Waxberry leaf extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 5 adds the extract that is obtained in the pipe tobacco of cigarette
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.Be added into the Waxberry leaf extract in the pipe tobacco, account for 0.03% of pipe tobacco weight.Concrete grammar is earlier Waxberry leaf extract to be dissolved in the ethanol, and the Diluted Alcohol that is dissolved with Waxberry leaf extract evenly is sprayed on the pipe tobacco, and ethanol evaporation is fallen subsequently.Pipe tobacco rolls into test sample cigarette through cigarette machine.
Effect experiment in embodiment 6 cigarette smokes
Be taken at two parts of the good finished cut tobacco of 22 ℃ ± 1 ℃ of temperature and 60% ± 2% time balance of relative humidity (RH) 40 grams, take by weighing Waxberry leaf extract by 0.04% of its quality, behind 70% alcohol dilution, be sprayed on the pipe tobacco equably with the larynx jet pipe, perfuming and not the aromatic tobacco sample be placed in the climatic chamber of 22 ℃ ± 1 ℃ of temperature and RH60% ± 2% balance 48 hours, with fill out the cigarette device respectively with perfuming and not the pipe tobacco of perfuming make cigarette and prop up, 22 ℃ ± 1 ℃ and RH60% ± 2% time balance 48 hours, please cigarette sensory evaluating smoking group smoke panel test again.
The personnel that smoke panel test are consistent to think the Waxberry leaf extract that adds flavouring effectively when tobacco product aspirate, and fragrance is abundant, the solid sense of increase flue gas; And Waxberry leaf extract can also be given the aromatic and the note of cigarette uniqueness.
Claims (10)
1. Waxberry leaf extract, it is to adopt Folium Myricae rubrae to extract raw material, with the polar solvent is extraction agent, in alkaline medium, carry out abstraction reaction, extracted the after-filtration separation and obtained feed liquid, feed liquid has been carried out precipitate and separate and collecting precipitation thing with organic acid under acidic conditions, throw out has been dissolved with extraction agent once more, separate insolubles then, promptly obtain Waxberry leaf extract of the present invention.
2. Waxberry leaf extract according to claim 1, wherein said extraction agent are 40～70% aqueous ethanolic solution.
3. Waxberry leaf extract according to claim 1, wherein extraction agent is 10～20: 1 with the weight ratio of extracting raw material
4. Waxberry leaf extract according to claim 1, wherein said alkaline medium are sodium hydroxide, calcium hydroxide, ammoniacal liquor or yellow soda ash; Described organic acid is toluylic acid, citric acid, oxysuccinic acid or Citric Acid.
5. the extracting method of a Waxberry leaf extract, it adopts Folium Myricae rubrae for extracting raw material, specifically may further comprise the steps: earlier alkali is joined in the extraction agent, regulating extraction agent pH value is 8.0～12.0, extraction agent is 10～20: 1 with the weight ratio of extracting raw material, extracted 1～5 hour at 50～90 ℃, after isolating feed liquid, feed liquid is concentrated into 1/3 of original volume, in concentrated solution, adds organic acid, regulating the pH value is 3.5～5.5, filtering separation collecting precipitation thing is with 5～10 times of extraction agent dissolution precipitation things, filtering separation insolubless once more, feed liquid is concentrated into the medicinal extract shape, promptly obtains Waxberry leaf extract of the present invention.
6. the extracting method of Waxberry leaf extract according to claim 5, wherein said extraction agent is 40～70% aqueous ethanolic solution.
7. the extracting method of Waxberry leaf extract according to claim 5, wherein said alkaline medium is sodium hydroxide, calcium hydroxide, ammoniacal liquor or yellow soda ash; Described organic acid is toluylic acid, citric acid, oxysuccinic acid or Citric Acid.
8. a Waxberry leaf extract is as the purposes of additive of tobacco product, it is that Waxberry leaf extract is added in the pipe tobacco of cigarette, the Waxberry leaf extract that is added in the pipe tobacco accounts for 0.01%～0.05% of pipe tobacco weight, flavouring effectively when tobacco product aspirates, and fragrance is abundant, increases the solid sense of flue gas.
9. Waxberry leaf extract according to claim 8 is as the purposes of additive of tobacco product, and the Waxberry leaf extract that wherein is added in the pipe tobacco accounts for 0.02%～0.04% of pipe tobacco weight.
10. Waxberry leaf extract according to claim 8 is as the purposes of additive of tobacco product, wherein Waxberry leaf extract is dissolved in 70% the ethanol, the alcohol solvent that is dissolved with Waxberry leaf extract is rolled in the process at the pipe tobacco of production of cigarettes is sprayed on the pipe tobacco.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100619970A CN101880599B (en) | 2009-05-05 | 2009-05-05 | Waxberry leaf extract and application thereof as tobacco product additives |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100619970A CN101880599B (en) | 2009-05-05 | 2009-05-05 | Waxberry leaf extract and application thereof as tobacco product additives |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101880599A true CN101880599A (en) | 2010-11-10 |
| CN101880599B CN101880599B (en) | 2012-07-25 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009100619970A Expired - Fee Related CN101880599B (en) | 2009-05-05 | 2009-05-05 | Waxberry leaf extract and application thereof as tobacco product additives |
Country Status (1)
| Country | Link |
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| CN (1) | CN101880599B (en) |
Cited By (11)
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| CN102161935A (en) * | 2010-12-31 | 2011-08-24 | 广东中烟工业有限责任公司 | Endogenous perfume from tobacco as well as preparation method and application thereof |
| CN102499459A (en) * | 2011-10-28 | 2012-06-20 | 浙江中烟工业有限责任公司 | Natural plant essential oil, preparation method thereof and application of natural plant essential oil to cigarettes |
| CN102499468A (en) * | 2011-11-17 | 2012-06-20 | 云南中烟昆船瑞升科技有限公司 | Method capable of remarkably increasing softness and absorptivity of papermaking-method reconstituted tobaccos |
| CN102499433A (en) * | 2011-10-19 | 2012-06-20 | 江苏中烟工业有限责任公司 | Application of suberenol extract in cigarette flavoring additive |
| CN102727540A (en) * | 2012-06-25 | 2012-10-17 | 陆建益 | Method for preparing red bayberry leaf extract |
| CN103271429A (en) * | 2013-05-02 | 2013-09-04 | 广东中烟工业有限责任公司 | Application of moringa oleifera leaf extractive to cigarette and cigarette comprising moringa oleifera leaf extractive |
| CN103330282A (en) * | 2013-05-02 | 2013-10-02 | 广东中烟工业有限责任公司 | Application of moringa oil in cigarette and cigarette containing moringa oil |
| CN103349355A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Black pepper and dark plum compound extract, preparation method thereof and application of compound extract taken as tobacco product additive |
| CN103740465A (en) * | 2013-12-13 | 2014-04-23 | 浙江中烟工业有限责任公司 | Waxberry extract used for cigarettes, preparation method thereof and use by being taken as tobacco additive |
| CN103865654A (en) * | 2014-01-26 | 2014-06-18 | 广西中烟工业有限责任公司 | Novel method for obtaining waxberry volatile aroma components |
| CN106235392A (en) * | 2016-09-09 | 2016-12-21 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of Polianthes tuberosa L. cigarette extract |
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| RU2352211C1 (en) * | 2008-05-15 | 2009-04-20 | Олег Иванович Квасенков | Method of production reconstituted tobacco |
| CN101298449A (en) * | 2008-06-27 | 2008-11-05 | 赵全成 | Novel preparation of myricetin |
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| CN102499433B (en) * | 2011-10-19 | 2014-06-04 | 江苏中烟工业有限责任公司 | Application of suberenol extract in cigarette flavoring additive |
| CN102499433A (en) * | 2011-10-19 | 2012-06-20 | 江苏中烟工业有限责任公司 | Application of suberenol extract in cigarette flavoring additive |
| CN102499459A (en) * | 2011-10-28 | 2012-06-20 | 浙江中烟工业有限责任公司 | Natural plant essential oil, preparation method thereof and application of natural plant essential oil to cigarettes |
| CN102499468A (en) * | 2011-11-17 | 2012-06-20 | 云南中烟昆船瑞升科技有限公司 | Method capable of remarkably increasing softness and absorptivity of papermaking-method reconstituted tobaccos |
| CN102727540A (en) * | 2012-06-25 | 2012-10-17 | 陆建益 | Method for preparing red bayberry leaf extract |
| CN103330282B (en) * | 2013-05-02 | 2015-12-09 | 广东中烟工业有限责任公司 | The application of oil ben in cigarette and the cigarette containing oil ben |
| CN103330282A (en) * | 2013-05-02 | 2013-10-02 | 广东中烟工业有限责任公司 | Application of moringa oil in cigarette and cigarette containing moringa oil |
| CN103271429A (en) * | 2013-05-02 | 2013-09-04 | 广东中烟工业有限责任公司 | Application of moringa oleifera leaf extractive to cigarette and cigarette comprising moringa oleifera leaf extractive |
| CN103271429B (en) * | 2013-05-02 | 2015-12-23 | 广东中烟工业有限责任公司 | The application of moringa oleifera leaf extractive in cigarette and the cigarette containing moringa oleifera leaf extractive |
| CN103349355A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Black pepper and dark plum compound extract, preparation method thereof and application of compound extract taken as tobacco product additive |
| CN103349355B (en) * | 2013-06-28 | 2016-03-09 | 湖北中烟工业有限责任公司 | Black pepper dark plum composite extract and preparation method thereof and the purposes as additive of tobacco product |
| CN103740465A (en) * | 2013-12-13 | 2014-04-23 | 浙江中烟工业有限责任公司 | Waxberry extract used for cigarettes, preparation method thereof and use by being taken as tobacco additive |
| CN103865654A (en) * | 2014-01-26 | 2014-06-18 | 广西中烟工业有限责任公司 | Novel method for obtaining waxberry volatile aroma components |
| CN103865654B (en) * | 2014-01-26 | 2015-07-29 | 广西中烟工业有限责任公司 | A kind of novel method obtaining red bayberry aroma volatile |
| CN106235392A (en) * | 2016-09-09 | 2016-12-21 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of Polianthes tuberosa L. cigarette extract |
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