CN101875543B - Attapulgite finely-carved oil sludge and production method thereof - Google Patents
Attapulgite finely-carved oil sludge and production method thereof Download PDFInfo
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- CN101875543B CN101875543B CN2010101326950A CN201010132695A CN101875543B CN 101875543 B CN101875543 B CN 101875543B CN 2010101326950 A CN2010101326950 A CN 2010101326950A CN 201010132695 A CN201010132695 A CN 201010132695A CN 101875543 B CN101875543 B CN 101875543B
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Abstract
The invention discloses attapulgite finely-carved oil sludge and a production method thereof. The technical scheme is characterized in that the attapulgite finely-carved oil sludge consists of high-viscosity attapulgite clay powder, tung oil, anatase titanium dioxide, superfine polyving akohol powder, modified carboxymethyl hydroxy propyl cellulose and deionized water. The production method comprises the steps of: dissolving the superfine polyving akohol powder and the modified carboxymethyl hydroxy propyl cellulose into the deionized water, then adding the high-viscosity attapulgite clay powder and the anatase titanium dioxide into the deionized water, stirring to obtain a semi-finished product of the attapulgite finely-carved oil sludge, slowly adding the tung oil into the semi-finished product of the attapulgite finely-carved oil sludge, and stirring to obtain the finished product of the attapulgite finely-carved oil sludge. The attapulgite finely-carved oil sludge can be cut, scraped, filled, rubbed and polished arbitrarily to prepare various models, which is time-saving and fast; a ready-made model can be preserved permanently in a non-deforming way; and the used oil sludge and the oil sludge scraped from the model with a scraper can be recycled for later use. The invention is suitable for industrial design model making and sculptures of arts and crafts articles.
Description
Technical field
The present invention relates to greasy filth, be specifically related to a kind of attapulgite carved oil sludge and production method thereof.
Background technology
Carved oil sludge is mainly used in elaboration prototype finishing impression, industrial design Modelling, quality is hard careful under the normal temperature, can work with great care, to temperature sensitive, tepor can be softened moulding or be repaired, and can soften with the hand temperature, moulding easy, suitable teaching in classroom exercises, not touching with one's hand, do not shrink, can use repeatedly, is the good material of artwork industry prototype.
The carved oil sludge of Xiao Shouing is made up of talcum powder, Paris white, breeze, butter, pigment and paraffin in the market.Talcum powder, Paris white and breeze with can not form the mineral colloid after water mixes, be to depend on grease and be bonded together fully.The plastic poor-performing of this greasy filth, the finished product after the making are easy to generate drying, cracking, distortion, mouldy and rotten, also can make the operator that a kind of greasy feeling is arranged on hand in making processes, and duration of service, long can the stimulation pointed, and influenced sense of touch, and touched with one's hand; Grease modelling can soften when being warm, even the distortion of caving in, and influences molding quality, and it is bad to reuse effect.
The Chinese patent publication number is: CN 101177532, open day: on May 14th, 2008, name is called " a kind of carved oil sludge and preparation method thereof ", disclose: " a kind of carved oil sludge and preparation method, it is formed by following weight part feedstock production: paraffin 30～50, soft wax 8～20; Vaseline 4～12; lime carbonate 60～130, toner 0.2～0.8, all the other are micro-moisture and impurity ".
The weak point of above-mentioned patent is that the carved oil sludge main raw material that this technology is produced is a lime carbonate, lime carbonate is a kind of white powder, with can not form the mineral colloid after water mixes, depend on paraffin, soft wax and the Vaseline after the fusing and be bonded together, directly have influence on the quality of carved oil sludge.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of attapulgite carved oil sludge and production method thereof are provided.
Attapulgite carved oil sludge is made up of the sticking attapulgite clay powder of height, tung oil, anatase thpe white powder, micronized polyethylene alcohol powder, modified carboxy methyl hydroxypropylcellulose and deionized water.After micronized polyethylene alcohol powder and modified carboxy methyl hydroxypropylcellulose are dissolved in deionized water, sticking attapulgite clay powder of height and anatase thpe white powder are added in the deionized water, stirring the back is the work in-process of attapulgite carved oil sludge, tung oil is slowly added in the work in-process of attapulgite carved oil sludge and stir, stirring the back is the finished product of attapulgite carved oil sludge.
Attapulgite clay has higher plasticity-under aqueous situation, good stability, and the hardness of attapulgite clay is Mohs 2～3 degree; Attapulgite clay is viscosity when moist, viscosity can reach more than the 3000mPas, the dry post-shrinkage ratio of attapulgite clay is little, and does not produce be full of cracks, and high sticking attapulgite clay powder is the powdery attapulgite stone clay that the complete processing of employing raising viscosity of attapulgite clay is produced.
Tung oil is a kind of natural vegetables oil, has that glossiness is good, characteristics such as strong adhesion, high temperature resistant, corrosion-resistant and excellent waterproofness.
Anatase thpe white powder has excellent water dispersible and remarkable optical property, form and aspect stability, and size-grade distribution is good, has the characteristics of high gloss, high reducing power, high covering power.
Micronized polyethylene alcohol powder is soluble in water, and at normal temperatures, its pH value of aqueous solution is generally 5～7, stable viscosity, be subjected to the influence of weak acid, weak base or organic solvent hardly, oil-proofness is high, easily film forming, the film water white transparency that forms has excellent mechanical intensity, any surface finish and not being clamminess.
The modified carboxy methyl hydroxypropylcellulose can be dissolved in cold water or hot water rapidly, has good thixotropy performance, salt tolerance and acid resistance superior performance, and the viscosity height, thickening material is effective.
The present invention is achieved by following technical proposals:
1, the batching of attapulgite carved oil sludge is made up of following component by weight percentage: high sticking attapulgite clay powder 55～75%, tung oil 2～15%, anatase thpe white powder 0.1～5%, micronized polyethylene alcohol powder 0.1～5%, modified carboxy methyl hydroxypropylcellulose 0.1～5% and deionized water 20～35%;
2, the production method of attapulgite carved oil sludge: (1) adds deionized water in the stirrer that has turned round earlier, then micronized polyethylene alcohol powder and modified carboxy methyl hydroxypropylcellulose is added in the deionized water; (2) micronized polyethylene alcohol powder and modified carboxy methyl hydroxypropylcellulose are gelating soln after being dissolved in deionized water, sticking attapulgite clay powder of height and anatase thpe white powder are added in the gelating soln, through stirring the back is the work in-process of attapulgite carved oil sludge, (3) tung oil is slowly added in the work in-process of attapulgite carved oil sludge and stir, the back that stirs is the finished product of attapulgite carved oil sludge.
The sticking attapulgite clay powder of described height is the attapulgite clay that adopts the complete processing production that improves viscosity of attapulgite clay, it is characterized in that, and from the attapulgite clay of mining area exploitation, need be through 30～120 days natural weathering; Modification processing method is: calculate by weight percentage, take from the attapulgite clay 94～98% after the right weathering, evenly add 2～6% yellow soda ash, import jointly in the fermentation vat, add clear water and soak ageing, soak time is 72～120 hours; Get the attapulgite clay after the immersion, stir in the input stirrer, and the attapulgite clay after will stirring, be extruded into thin slice through extrusion machine, its gauge control is at 0.5～2 millimeter, with the attapulgite clay thin slice, carry out airing, the attapulgite clay thin slice after the airing, its water content≤15%; Batching is calculated by weight percentage: the attapulgite clay 94～98% after the airing, High hydrophilous resin 0.5～5% and Mierocrystalline cellulose 0.5～3%, above-mentioned batching is stirred, and carry out abrasive dust in the back input grinding machine that stirs, particle fineness≤0.074 millimeter.
Above-mentioned production technique is to adopt " improving the complete processing of viscosity of attapulgite clay " in application on June 20th, 2005 by the inventor, and the Chinese patent Granted publication number is: CN 1317067C, Granted publication day: on May 23rd, 2007.
Attapulgite carved oil sludge can keep certain rigidity at normal temperatures, has outstanding operability, cutting, scraping arbitrarily, fills out deposited, reconditioning and various models are made in polishing, saves time fast; Ready-made model can forever be saved indeformablely, and the greasy filth after used greasy filth and scraper scrape from model can reuse after the recovery.
Attapulgite carved oil sludge viscosity height, the quality exquisiteness, soft plasticity-is good, water-retentivity is strong, shrinking percentage is little, indeformable, do not produce be full of cracks, nontoxic, non-corrosiveness and do not have the characteristics of greasy feeling.
The production technique of attapulgite carved oil sludge is simple, with low cost, the stronger market competitiveness is arranged.
Attapulgite carved oil sludge is applicable to industrial design Modelling and industrial art articles for use sculpture.
Embodiment
The invention will be further described below in conjunction with embodiment:
1, the batching of attapulgite carved oil sludge is made up of following component by weight percentage: high sticking attapulgite clay powder 62%, tung oil 12%, anatase thpe white powder 2%, micronized polyethylene alcohol powder 2%, modified carboxy methyl hydroxypropylcellulose 1% and deionized water 21%.
2, the production method of attapulgite carved oil sludge: (1) adds deionized water in the stirrer that has turned round earlier, then micronized polyethylene alcohol powder and modified carboxy methyl hydroxypropylcellulose is added in the deionized water; (2) after micronized polyethylene alcohol powder and modified carboxy methyl hydroxypropylcellulose are dissolved in deionized water, sticking attapulgite clay powder of height and anatase thpe white powder are added in the deionized water, through stirring the back is the work in-process of attapulgite carved oil sludge, (3) tung oil is slowly added in the work in-process of attapulgite carved oil sludge and stir, the back that stirs is the finished product of attapulgite carved oil sludge.
Claims (1)
1. attapulgite carved oil sludge, it is characterized in that the batching of attapulgite carved oil sludge is made up of following component by weight percentage: high sticking attapulgite clay powder 55～75%, tung oil 2～15%, anatase thpe white powder 0.1～5%, micronized polyethylene alcohol powder 0.1～5%, modified carboxy methyl hydroxypropylcellulose 0.1～5% and deionized water 20～35%;
The production method of described attapulgite carved oil sludge: (1) adds deionized water in the stirrer that has turned round earlier, then micronized polyethylene alcohol powder and modified carboxy methyl hydroxypropylcellulose is added in the deionized water; (2) micronized polyethylene alcohol powder and modified carboxy methyl hydroxypropylcellulose are gelating soln after being dissolved in deionized water, sticking attapulgite clay powder of height and anatase thpe white powder are added in the gelating soln, through stirring the back is the work in-process of attapulgite carved oil sludge, (3) tung oil is slowly added in the work in-process of attapulgite carved oil sludge and stir, the back that stirs is the finished product of attapulgite carved oil sludge;
The sticking attapulgite clay powder of described height is the attapulgite clay that adopts the complete processing production that improves viscosity of attapulgite clay, it is characterized in that, and from the attapulgite clay of mining area exploitation, need be through 30～120 days natural weathering; Modification processing method is: calculate by weight percentage, take from the attapulgite clay 94～98% after the right weathering, evenly add 2～6% yellow soda ash, import jointly in the fermentation vat, add clear water and soak ageing, soak time is 72～120 hours; Get the attapulgite clay after the immersion, stir in the input stirrer, and the attapulgite clay after will stirring, be extruded into thin slice through extrusion machine, its gauge control is at 0.5～2 millimeter, with the attapulgite clay thin slice, carry out airing, the attapulgite clay thin slice after the airing, its water content≤15%; Batching is calculated by weight percentage: the attapulgite clay 94～98% after the airing, High hydrophilous resin 0.5～5% and Mierocrystalline cellulose 0.5～3%, above-mentioned batching is stirred, and carry out abrasive dust in the back input grinding machine that stirs, particle fineness≤0.074 millimeter.
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| CN106830779B (en) * | 2016-12-25 | 2019-04-02 | 重庆腾通工业设计有限公司 | Waste oil mud reclaiming treatment process |
| CN106810192A (en) * | 2017-01-20 | 2017-06-09 | 杨忠敏 | A kind of new mud heap moulding material and preparation method thereof and application method |
| CN109503111A (en) * | 2018-11-20 | 2019-03-22 | 重庆奥图亚模型有限公司 | A kind of lightweight greasy filth and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1693425A (en) * | 2005-05-19 | 2005-11-09 | 许庆华 | Process for purifying waste diesel oil |
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| US6093669A (en) * | 1995-11-30 | 2000-07-25 | Oil-Dri Corporation Of America | Method for selecting raw material for bleaching clay |
| NL1020554C2 (en) * | 2002-05-08 | 2003-11-11 | Stichting Energie | Process for desulphurizing natural gas. |
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| CN1693425A (en) * | 2005-05-19 | 2005-11-09 | 许庆华 | Process for purifying waste diesel oil |
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