CN101862058B - Method for manufacturing chinlon thread gluing strip capable of shielding far infrared rays - Google Patents

Method for manufacturing chinlon thread gluing strip capable of shielding far infrared rays Download PDF

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CN101862058B
CN101862058B CN 200910215813 CN200910215813A CN101862058B CN 101862058 B CN101862058 B CN 101862058B CN 200910215813 CN200910215813 CN 200910215813 CN 200910215813 A CN200910215813 A CN 200910215813A CN 101862058 B CN101862058 B CN 101862058B
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mother liquor
chinlon
gluing
far infrared
infrared rays
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CN101862058A (en
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郑国烟
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Jiangsu Baihong Composite Material Technology Co ltd
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Wuxi Baihe Weaving Co Ltd
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Abstract

The invention discloses a method for manufacturing a chinlon thread gluing strip capable of shielding far infrared rays, which comprises the steps of cleaning the chinlon thread gluing strip, confecting a dye mother liquor capable of absorbing the far infrared rays, dying the chinlon thread gluing strip, and performing after treatment and sizing treatment. The chinlon thread gluing strip capable of shielding the far infrared rays, which is manufactured by the method, is optimized by using different dyes capable of absorbing the far infrared rays and can absorb the far infrared rays in a certain wave length range after being compounded to certain concentration, and graphite powder in the sizing treatment absorbs the far infrared rays in a certain wave length range to ensure that the chinlon thread gluing strip capable of shielding the far infrared rays makes the far infrared rays in a wave length range of 750 to 1,200 nm reduced within 25 to 52 percent, and can be used as a thread gluing strip matched with a military invisible costume, and an infrared night vision meter cannot observe a person wearing the invisible costume, so the application of the thread gluing strip is expanded, and the added value is improved.

Description

A kind of manufacture method of chinlon thread gluing strip capable of shielding far infrared rays
Technical field:
The present invention relates to a kind of processing and treating method of cingulum, relate in particular to a kind of manufacture method of chinlon thread gluing strip capable of shielding far infrared rays.
Background technology:
Existing common chinlon gluing buckle, when being used for military concealing suit assembly set magic tape, can not absorb a large amount of far infrareds that human body sends, but distribute a large amount of far infrareds that human body sends, easily observed by infrared viewing device, can not be used for stealthy clothes magic tape, limit the purposes of chinlon gluing buckle, reduce surcharge.
Summary of the invention:
One of purpose of the present invention is to overcome the defective that prior art exists, and a kind of manufacture method of chinlon thread gluing strip capable of shielding far infrared rays is provided.
This purpose of the present invention and other purpose will and be described by following detailed description and further set forth and embody.
The manufacture method of chinlon thread gluing strip capable of shielding far infrared rays of the present invention is chinlon gluing buckle to be put in the impregnating mangle to clean with cleaning fluid first, cleans complete chinlon gluing buckle to be taken out from impregnating mangle; Then modulated energy absorbs the dye mother solution of far infrared; Preparation dyeing mother liquor and adding auxiliary agent in impregnating mangle; In the impregnating mangle that fills dyeing mother liquor and auxiliary agent, add water preparation dyeing working solution; Drop into the chinlon gluing buckle after cleaning, start impregnating mangle dyeing, hot water wash after the dyeing, cold wash is to wash the dyeing loose colour off; Chinlon gluing buckle after the washing is dewatered in dewaterer; Chinlon gluing buckle after the dehydration is carried out the gluing arrangement with glue and auxiliary agent (graphite powder that contains the far infrared absorption function) in gluing machine; At last the chinlon gluing buckle after the gluing arrangement is dried in drying baker.
The manufacture method of chinlon thread gluing strip capable of shielding far infrared rays of the present invention, comprise chinlon gluing buckle is cleaned, modulated energy absorbs the dye mother solution of far infrared, chinlon gluing buckle is dyeed, post processing and gluing step, wherein, the prescription of described dye mother solution is: 1 kilogram of red RED NHF-S dyestuff, be watered the 900-1100 liter, make red mother liquor, 1 kilogram of blue BLUE NHF-S dyestuff, be watered the 900-1100 liter, make blue mother liquor, 1 kilogram of olive green OLIVS SG dyestuff, be watered the 900-1100 liter, make the olive green mother liquor, in impregnating mangle, with red mother liquor, blue mother liquor and olive green mother liquor are hybridly prepared into the dyeing mother liquor, 10 kilograms of chinlon gluing buckles of every processing, red mother liquor, the consumption of blue mother liquor and olive green mother liquor is: red mother liquor 0.06-0.08 liter, blue mother liquor 0.5-0.8 liter, olive green mother liquor 4.5-7.0 liter.
In the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays of the present invention, described cleaning step cleans chinlon gluing buckle for elder generation's cleaning fluid with 80-90 ℃ in impregnating mangle, scavenging period 20-30min, and wherein the prescription of cleaning fluid is:
Emulsifying agent LF100 800-900 gram
Sodium carbonate 250-300 gram
Water 3500-3700 kilogram.
In the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays of the present invention, described chinlon gluing buckle is carried out staining procedure for above-mentioned red mother liquor, making the mother liquor cumulative volume that dyes after blue mother liquor and olive green mother liquor mix by 1: 1: 1 part by weight is the 5.06-7.88 liter, then in the dyeing mother liquor, add auxiliary agent: glacial acetic acid HAc 0.4-0.6 grams per liter, levelling agent BS 0.20-0.4 grams per liter, in the impregnating mangle that dyeing mother liquor and auxiliary agent are housed, add again the 194.9-292.1 premium on currency according to bath raio 1: 20-30 (chinlon gluing buckle weight/dyeing working solution weight), be mixed with the dyeing working solution, then starting impregnating mangle dyes, the dyeing condition is: be raised to 95-105 ℃ with the programming rate of 3 ℃ of the per minutes work liquid temp that will dye, at 95-105 ℃ of insulation 40-50min, after be cooled to 70 ℃, it is complete to dye.
In the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays of the present invention, described post processing is that the chinlon gluing buckle warm water with 60-80 ℃ in impregnating mangle after will dyeing washs 8-12min, and then with cold water washing 8-12 minute, with the chinlon gluing buckle 4-6min that in dewaterer, dewaters after the washing.
In the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays of the present invention, described gluing step is for carrying out the gluing arrangement of 4-10min at 60-100 ℃ to the chinlon gluing buckle after the dehydration with glue and auxiliary agent in gluing machine, wherein glue and auxiliary agent with respect to the percentage by weight prescription of chinlon gluing buckle are:
Graphite powder 0.1-0.2%
Resin YC-1900NDS 80-100%
Butanone MEK 70-150%
Resin YC-1870HD 30-50%
Glue crosslinking agent CA-860D 30-50%
Glue crosslinking agent CA-800D 10-14%
Ultra-violet absorber 10012 0.2-0.4%
Antioxidant 168 0.2-0.4%
In drying baker, the chinlon gluing buckle after the gluing at 50-55 prebake 3-5min, is dried 3-5min at 110-130 ℃ more at last.
With the prepared chinlon thread gluing strip capable of shielding far infrared rays of the inventive method, use the different dyes optimization that absorbs far infrared, the composite far infrared that can absorb certain wave-length coverage to certain concentration, absorbed again the far infrared of certain wave-length coverage by the graphite powder in the gluing, so that the far infrared transmissivity of chinlon thread gluing strip capable of shielding far infrared rays in wavelength 750-1200nm scope drops in the 25-52%, can be used for military concealing suit assembly set magic tape, infrared viewing device can not be observed the people who wears stealthy clothes, enlarge the purposes of magic tape, improved surcharge.
In the present invention, if not refer in particular to, all percentage by weights are all take the gross weight of magic tape as radix, and all raw materials comprise that dyestuff, auxiliary agent and additive and equipment all can buy from market the conventional method in field under the compound method of finishing agent all adopts.
The specific embodiment:
Specific embodiment given below can further specify the present invention.But they are not limitation of the invention.
Embodiment 1
When 1, chinlon gluing buckle being cleaned, 80 ℃ of cleaning temperatures, time 20min, every processing 180-200 kilogram chinlon gluing buckle, the prescription of cleaning fluid is:
Emulsifying agent LF100 800 grams
Sheet alkali PJ 250 grams
3500 kilograms in water
When 2, modulating dye mother solution, the compound method of dye mother solution is:
1 kilogram of red RED NHF-S dyestuff is watered 900 liters, makes red mother liquor;
1 kilogram of blue BLUE NHF-S dyestuff is watered 900 liters, makes blue mother liquor;
1 kilogram of olive green OLIVS SG dyestuff is watered 900 liters, makes the olive green mother liquor.
3, in impregnating mangle, red mother liquor, blue mother liquor and olive green mother liquor are hybridly prepared into the dyeing mother liquor, 10 kilograms of chinlon gluing buckles of every processing, the consumption of red mother liquor, blue mother liquor and olive green mother liquor is:
40.06 liters in red mother liquor
40.50 liters in blue mother liquor
44.50 liters in olive green mother liquor
Mixing poststaining mother liquor cumulative volume is 5.06 liters, and add auxiliary agent this moment in the dyeing mother liquor, and auxiliary dosage is:
Glacial acetic acid HAc 0.4 grams per liter
Levelling agent BS 0.2 grams per liter.
4, the bath raio of preparation dyeing working solution is: 1: 20 (chinlon gluing buckle weight/dyeing working solution weight) adds 194.9 premium on currency again in the impregnating mangle that dyeing mother liquor and auxiliary agent are housed.
5, the process conditions that dye are:
Be raised to 95 ℃ with the programming rate of 3 ℃ of the per minutes work liquid temp that will dye, at 95 ℃ of insulation 40min, after be cooled to 70 ℃, it is complete to dye.
6, the process conditions of Warm Wash and cold wash are:
With 60 ℃ warm water washing 8min, and then with cold water washing 8 minutes.
7, chinlon gluing buckle is dewatered dewatering time 4min.
8, at 60 ℃ the chinlon gluing buckle after the dehydration is carried out the gluing arrangement of 4min with glue and auxiliary agent in gluing machine, wherein glue and auxiliary agent with respect to the percentage by weight prescription of chinlon gluing buckle are:
Graphite powder 0.1%
Resin YC-1900NDS 80%
Butanone MEK 70%
Resin YC-1870HD 30%
Glue crosslinking agent CA-860D 30%
Glue crosslinking agent CA-800D 10%
Ultra-violet absorber 10,012 0.2%
Antioxidant 168 0.2%.
9, in drying baker, the chinlon gluing buckle after the gluing at 50 ℃ of prebake 3min, is dried 3min at 110 ℃ again.
Embodiment 2
When 1, chinlon gluing buckle being cleaned, 85 ℃ of cleaning temperatures, time 25min, every processing 180-200 kilogram chinlon gluing buckle, the prescription of cleaning fluid is:
Emulsifying agent LF100 4850 grams
Sheet alkali PJ 4280 grams
43600 kilograms in water.
When 2, modulating dye mother solution, the compound method of dye mother solution is:
1 kilogram of red RED NHF-S dyestuff is watered 10 liters, makes red mother liquor;
1 kilogram of blue BLUE NHF-S dyestuff is watered 1000 liters, makes blue mother liquor;
1 kilogram of olive green OLIVS SG dyestuff is watered 1000 liters, makes the olive green mother liquor.
3, in impregnating mangle, red mother liquor, blue mother liquor and olive green mother liquor are hybridly prepared into the dyeing mother liquor, 10 kilograms of chinlon gluing buckles of every processing, the consumption of red mother liquor, blue mother liquor and olive green mother liquor is:
0.07 liter in red mother liquor
0.65 liter in blue mother liquor
5.50 liters in olive green mother liquor
Mixing poststaining mother liquor cumulative volume is 6.22 liters, and add auxiliary agent this moment in the dyeing mother liquor, and auxiliary dosage is:
Glacial acetic acid HAc 0.5 grams per liter
Levelling agent BS 0.3 grams per liter.
4, the bath raio of preparation dyeing working solution is: 1: 25 (chinlon gluing buckle weight/dyeing working solution weight) adds 244.0 premium on currency again in the impregnating mangle that dyeing mother liquor and auxiliary agent are housed.
5, the process conditions that dye are:
Be raised to 100 ℃ with the programming rate of 3 ℃ of the per minutes work liquid temp that will dye, at 100 ℃ of insulation 45min, after be cooled to 70 ℃, it is complete to dye.
6, the process conditions of Warm Wash and cold wash are:
With 70 ℃ warm water washing 10min, and then with cold water washing 10 minutes.
7, chinlon gluing buckle is dewatered dewatering time 5min.
8, at 85 ℃ the chinlon gluing buckle after the dehydration is carried out the gluing arrangement of 7min with glue and auxiliary agent in gluing machine, wherein glue and auxiliary agent with respect to the percentage by weight prescription of chinlon gluing buckle are:
Graphite powder 0.15%
Resin YC-1900NDS 90%
Butanone MEK 100%
Resin YC-1870HD 40%
Glue crosslinking agent CA-860D 40%
Glue crosslinking agent CA-800D 12%
Ultra-violet absorber 10,012 0.3%
Antioxidant 168 0.3%.
9, in drying baker, the chinlon gluing buckle after the gluing at 52 ℃ of prebake 4min, is dried 4min at 120 ℃ again.
Embodiment 3
When 1, chinlon gluing buckle being cleaned, every processing 180-200 kilogram chinlon gluing buckle, the prescription of cleaning fluid is:
Emulsifying agent LF100 900 grams
Sheet alkali PJ 300 grams
3700 kilograms in water.
When 2, modulating dye mother solution, the compound method of dye mother solution is:
1 kilogram of red RED NHF-S dyestuff is watered 1100 liters, makes red mother liquor;
1 kilogram of blue BLUE NHF-S dyestuff is watered 1100 liters, makes blue mother liquor;
1 kilogram of olive green OLIVS SG dyestuff is watered 1100 liters, makes the olive green mother liquor.
3, in impregnating mangle, red mother liquor, blue mother liquor and olive green mother liquor are hybridly prepared into the dyeing mother liquor, 10 kilograms of chinlon gluing buckles of every processing, the consumption of red mother liquor, blue mother liquor and olive green mother liquor is:
0.08 liter in red mother liquor
0.80 liter in blue mother liquor
7.00 liters in olive green mother liquor
Mixing poststaining mother liquor cumulative volume is 7.88 liters, and add auxiliary agent this moment in the dyeing mother liquor, and auxiliary dosage is:
Glacial acetic acid HAc 0.6 grams per liter
Levelling agent BS 0.4 grams per liter.
4, the bath raio of preparation dyeing working solution is: 1: 30 (chinlon gluing buckle weight/dyeing working solution weight) adds 292.1 premium on currency again in the impregnating mangle that dyeing mother liquor and auxiliary agent are housed.
5, the process conditions that dye are:
Be raised to 105 ℃ with the programming rate of 3 ℃ of the per minutes work liquid temp that will dye, at 105 ℃ of insulation 50min, after be cooled to 70 ℃, it is complete to dye.
6, the process conditions of Warm Wash and cold wash are:
With 80 ℃ warm water washing 12min, and then with cold water washing 12 minutes.
7, chinlon gluing buckle is dewatered dewatering time 6min.
8, at 60-100 ℃ the chinlon gluing buckle after the dehydration is carried out the gluing arrangement of 10min with glue and auxiliary agent in gluing machine, wherein glue and auxiliary agent with respect to the percentage by weight prescription of chinlon gluing buckle are:
Graphite powder 0.2%
Resin YC-1900NDS 100%
Butanone MEK 150%
Resin YC-1870HD 50%
Glue crosslinking agent CA-860D 50%
Glue crosslinking agent CA-800D 14%
Ultra-violet absorber 10,012 0.4%
Antioxidant 168 0.4%.
9, at last in drying baker, with the chinlon gluing buckle after the gluing at 55 ℃ of prebake 5min, again at 130 ℃ of oven dry 5min.
Shielding far-infrared nylon magic tape of the present invention and existing common chinlon gluing buckle contrast and experiment are as shown in table 1:
Table 1
Code name Sample 750-1200nm wavelength period far infrared transmissivity (%)
1 Existing common chinlon gluing buckle 76
2 The chinlon thread gluing strip capable of shielding far infrared rays of the embodiment of the invention 1 48
3 The chinlon thread gluing strip capable of shielding far infrared rays of the embodiment of the invention 2 25
4 The chinlon thread gluing strip capable of shielding far infrared rays of the embodiment of the invention 3 50
As seen from Table 1, the chinlon thread gluing strip capable of shielding far infrared rays made from the inventive method is than little many of common chinlon gluing buckle shielding far infrared rays emissivity, good many of function of shielding.

Claims (7)

1. the manufacture method of a chinlon thread gluing strip capable of shielding far infrared rays, it is characterized in that comprising chinlon gluing buckle is cleaned, modulated energy absorbs the dye mother solution of far infrared, chinlon gluing buckle is dyeed, post processing and gluing step, wherein, the prescription of described dye mother solution is: 1 kilogram of red RED NHF-S dyestuff, be watered the 900-1100 liter, make red mother liquor, 1 kilogram of blue BLUE NHF-S dyestuff, be watered the 900-1100 liter, make blue mother liquor, 1 kilogram of olive green OLIVS SG dyestuff is watered the 900-1100 liter, makes the olive green mother liquor, in impregnating mangle, with red mother liquor, blue mother liquor and olive green mother liquor are hybridly prepared into the dyeing mother liquor, 10 kilograms of chinlon gluing buckles of every processing, red mother liquor, the consumption of blue mother liquor and olive green mother liquor is:
Red mother liquor 0.06-0.08 liter
Blue mother liquor 0.5-0.8 liter
Olive green mother liquor 4.5-7.0 liter.
2. the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays according to claim 1 is characterized in that 10 kilograms of chinlon gluing buckles of every processing, and the consumption of red mother liquor, blue mother liquor and olive green mother liquor is:
0.07 liter in red mother liquor
0.65 liter in blue mother liquor
5.50 liters in olive green mother liquor.
3. the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays according to claim 1 and 2, it is characterized in that described cleaning step cleans chinlon gluing buckle for elder generation's cleaning fluid with 80-90 ℃ in impregnating mangle, scavenging period 20-30min, wherein the prescription of cleaning fluid is:
Emulsifying agent LF100 800-900 gram
Sodium carbonate 250-300 gram
Water 3500-3700 kilogram.
4. the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays according to claim 1 and 2 is characterized in that chinlon gluing buckle is carried out staining procedure is:
(1) red mother liquor, blue mother liquor and olive green mother liquor are mixed, making dyeing mother liquor cumulative volume is the 5.06-7.88 liter;
(2) in the dyeing mother liquor, add auxiliary agent:
Glacial acetic acid HAc 0.4-0.6 grams per liter
Levelling agent BS 0.20-0.4 grams per liter
In the impregnating mangle that dyeing mother liquor and auxiliary agent are housed, add again 194.9-292.11 water according to bath raio 1:20-30, be mixed with the dyeing working solution;
(3) start impregnating mangle, be raised to 95-105 ℃ with the programming rate of 3 ℃ of the per minutes work liquid temp that will dye, be cooled to 70 ℃ behind the insulation 40-50min.
5. the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays according to claim 1 and 2, it is characterized in that described post processing washs 8-12min for the warm water with 60-80 ℃ in impregnating mangle of the chinlon gluing buckle after will dye, and then with cold water washing 8-12 minute, with the chinlon gluing buckle 4-6min that in dewaterer, dewaters after the washing.
6. the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays according to claim 1 and 2, it is characterized in that described gluing step at 60-100 ℃ the chinlon gluing buckle after the dehydration is carried out the gluing arrangement of 4-10min with glue and auxiliary agent in gluing machine, wherein glue and auxiliary agent with respect to the percentage by weight prescription of chinlon gluing buckle are:
Figure FSB00000948889600021
Figure FSB00000948889600031
Chinlon gluing buckle after the gluing at 50-55 ℃ of prebake 3-5min, is dried 3-5min at 110-130 ℃ again.
7. the manufacture method of chinlon thread gluing strip capable of shielding far infrared rays according to claim 6, it is characterized in that described gluing step at 85 ℃ the chinlon gluing buckle after the dehydration is carried out the gluing arrangement of 7min with glue and auxiliary agent in gluing machine, wherein glue and auxiliary agent with respect to the percentage by weight prescription of chinlon gluing buckle are:
In drying baker, the chinlon gluing buckle after the gluing at 52 ℃ of prebake 4min, is dried 4min at 120 ℃ again.
CN 200910215813 2009-12-30 2009-12-30 Method for manufacturing chinlon thread gluing strip capable of shielding far infrared rays Active CN101862058B (en)

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Publication number Priority date Publication date Assignee Title
CN102805459A (en) * 2012-08-21 2012-12-05 杭州三信织造有限公司 Ultra-thin lint-free adherent buckle belt and manufacturing method thereof
CN102978968A (en) * 2012-12-03 2013-03-20 吴江市鼎佳纺织有限公司 Improved garment material
CN103147293A (en) * 2013-03-19 2013-06-12 东华大学 Method for preparing anti-ultraviolet and anti-sulphur nylon fabric for shoes
CN103774409B (en) * 2014-01-06 2015-12-09 浙江新建纺织有限公司 A kind of Camouflage printing with infrared resistance technique of high-performance BLENDED FABRIC

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CN1143013A (en) * 1996-06-03 1997-02-19 刘光恩 Anti-ultraviolet ray cool and health fabric and it producing method
US6521038B2 (en) * 2000-12-21 2003-02-18 Dainichiseika Color & Chemicals Mfg. Co., Ltd. Near-infrared reflecting composite pigments
CN101033357A (en) * 2007-04-12 2007-09-12 武汉大学 Transparent coating capable of absorbing visible light and infrared light, preparing method and use thereof
CN101413219A (en) * 2008-10-09 2009-04-22 东华大学 Method for preparing near-infrared concealed cotton textiles

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1143013A (en) * 1996-06-03 1997-02-19 刘光恩 Anti-ultraviolet ray cool and health fabric and it producing method
US6521038B2 (en) * 2000-12-21 2003-02-18 Dainichiseika Color & Chemicals Mfg. Co., Ltd. Near-infrared reflecting composite pigments
CN101033357A (en) * 2007-04-12 2007-09-12 武汉大学 Transparent coating capable of absorbing visible light and infrared light, preparing method and use thereof
CN101413219A (en) * 2008-10-09 2009-04-22 东华大学 Method for preparing near-infrared concealed cotton textiles

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