CN101861136A - Wet forming compact composition containing volatile silicone oil and silicone resin - Google Patents
Wet forming compact composition containing volatile silicone oil and silicone resin Download PDFInfo
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- CN101861136A CN101861136A CN200880116546A CN200880116546A CN101861136A CN 101861136 A CN101861136 A CN 101861136A CN 200880116546 A CN200880116546 A CN 200880116546A CN 200880116546 A CN200880116546 A CN 200880116546A CN 101861136 A CN101861136 A CN 101861136A
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- powder
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- composition
- organic siliconresin
- volatile silicone
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
Abstract
Disclosed herein is a cake-type, wet-molded compact cosmetic composition. More specifically, disclosed is a cake- type, wet-molded compact cosmetic composition which is prepared by wet molding using a mixed solvent of volatile silicone oil and silicone resin so as to have excellent durability and a soft touch feel.
Description
Technical field
The present invention relates to densification (compact) cosmetic composition a kind of pie (cake-type), wet moulding (wet-molded), particularly carry out densification cosmetic compositions pie, wet moulding that wet moulding prepares, thereby make said composition have good durability and softish sense of touch by the mixed solvent that utilizes volatile silicone oils (volatile silicone oil) and organic siliconresin (silicone resin).
Background technology
The fine and close cosmetic product of conventional pie uses conventional methods preparation, this traditional method is included in the agitator mixes extender pigment (extender pigment), pigment and Chinese white, and on the surface of mixture spray adhesive (binder).Yet well-known is to utilize this mixed method to be difficult to realize uniform mixing.For overcoming such shortcoming, developed so-called re-injection method (back-injection method), this method is the method (wet molding method) of wet moulding.
In the early stage of development of wet moulding method, the re-injection method was used widely in nineteen nineties.Application about the re-injection method, pie, the densification cosmetic compositions be by in the mixed solvent that the powder (powdercontent) of densification (in vinyl disc before the molding) is dispersed in isopropyl alcohol (IPA) and water with preparation pulpous state material (slurry-type content), by the re-injection method described pulpous state material is seated in the vinyl disc again, draw certain amount of solvent by suction machine (sucking machine), then described pulpous state cake is placed in the exsiccator to remove remaining solvent.This technology also once was widely used in preparing eye shadow cream (eye shadow) and kermes (blushers).In addition, because make water and isopropyl alcohol as solvent, so the problem that described fine and close cosmetic product exists is, the hydrophilic of solvent makes it be difficult to hold a large amount of powder that is coated with polydimethylsiloxane (dimethylpolysiloxane) or alkyl silane (alkylsilane) with homodisperse form, so durability is low.
Recently, for the homodisperse of the powder guaranteeing to apply with make the powder that holds a large amount of coatings become possibility, in wet moulding, use emulsifying agent to substitute the mixed solvent of isopropyl alcohol and water, thereby improve the durability of fine and close cosmetics.Yet, used emulsifying agent owing to contain the fine and close cosmetics of the powder of a large amount of coatings, therefore, can reduce resistance when using this densification cosmetic product for a long time, thereby seem greasy and blackout sebum and perspiration.
Open No 1999-40922 of Korean Patent and 2003-50531, the open No H3-204806 of Japan Patent and U.S. Patent Publication No 2005-0142089 disclose the compositions of utilizing silicone oil and organic siliconresin preparation.The prescription of these compositionss is liquid type foundation cream (liquid-type foundation) or bottoming breast (makeup bases).Under the situation of described liquid type foundation cream, generally emulsifying agent must be used so that oil and water disperse equably.But as mentioned above, because the use of emulsifying agent, described liquid type foundation cream has reduced the resistance to sebum and perspiration when long-time the use, thereby seems greasy and blackout.
Summary of the invention
Therefore, through research repeatedly, the present invention has developed a kind of densification cosmetic compositions with wet moulding of softish sense of touch and good durability, found that, the bottoming powder (makeup powder) that can will apply by the mixed solvent that uses silicone oil and organic siliconresin is evenly dispersed in the starch (slurrypowder), and do not need to use emulsifying agent, thereby improved durability, make this dispersion molding again, and the material drying that makes this molding is to remove described mixed solvent, thereby make wet moulding, the densification cosmetic compositions of pie, thus the present invention finished.
Therefore, the purpose of this invention is to provide a kind of densification cosmetic compositions with wet moulding of good durability and softish sense of touch.
For reaching above-mentioned target, the invention provides a kind of densification cosmetic compositions of wet moulding, this cosmetic composition contains the bottoming powder of coating, and this cosmetic composition uses the mixed solvent of volatile silicone oils and organic siliconresin and makes.
More particularly, contain basis bottoming powder and organic siliconresin according to densification cosmetic compositions of the present invention, and with the gross weight before the said composition wet moulding is benchmark, the volatile silicone oils by using 30-40 weight % and the mixed solvent of organic siliconresin with the bottoming powder of the coating of 60-70 weight % be dispersed in slurry mutually in, make this sizing material forming again, and the material drying that makes this molding is to remove used volatile silicone oils.
By following detailed description, above-mentioned and other target of the present invention, feature and advantage to one skilled in the art, are conspicuous.
Densification cosmetic compositions according to described wet moulding of the present invention makes by the mixed solvent that uses volatile silicone oils and organic siliconresin, and do not need to use any emulsifying agent, therefore, described cosmetic composition has excellent durability, shows softish sense of touch simultaneously.
The specific embodiment
Hereinafter, the present invention will describe in further detail.
In the present invention, for the densification cosmetic compositions that makes wet moulding has good durability and softish sense of touch, the powder coated material (power coating substance) and the selection of solvent types are very important.
In the present invention, in order to prepare the densification cosmetic compositions of wet moulding, use the bottoming powder that is coated with coating substance with good resistance to water and oil resistivity with softish sense of touch and excellent durability.
General polydimethylsiloxane with resistance to water and oil resistivity and the alkyl silane of adopting is as coating substance, but scope of the present invention is not limited thereto.Yet, in order to improve durability, the preferred powder that uses by wet-process coating (wet coating) preparation.In general, by the amount of the powder selecting to apply and the coating substance wanted, this powder and this coating substance are mixed in solvent, flush away or evaporate this solvent and make to have only described coating substance to be retained on the described powder is then to the powder heat treatment.
Simultaneously, the composition that is used for the bottoming powder of foundation cream product (makeup product) traditionally can comprise extender pigment, pigment and Chinese white.Especially, can use Talcum, Muscovitum, sericite, tripoli, nylon powder, silica flour, polymethyl methacrylate (PMMA), boron nitride powder and barium sulfate, but scope of the present invention is not limited in this.
According to described densification cosmetic compositions of the present invention, be benchmark with the gross weight of described compositions, the content of the bottoming powder of described coating is preferably 60-70 weight %.If the content of the bottoming powder of described coating is lower than 60 weight %, then this powder can flow out in forming process, thereby causes the problem of mouldability; And if be higher than 70 weight %, then the powder of this coating is difficult to homodisperse.In addition, described powder composition is the powder that is coated with silicones or alkyl silane, and this powder composition refers to the pie powder in the step before molding, and this powdery components contains extender pigment, pigment, Chinese white and spice.
In the present invention, for the bottoming powder that makes described coating be evenly dispersed in slurry mutually in, use by making volatile silicone oils and organic siliconresin mix the solvent that obtains in 97: 3 to 99: 1 with weight ratio.
According to the densification cosmetic compositions of described wet moulding of the present invention, be benchmark with the gross weight of described compositions, the content of described solvent is preferably 30-40 weight %.If the content of described solvent is lower than 30 weight %, then the bottoming powder of described coating can not uniform distribution, and if described content is higher than 40 weight %, the problem of mouldability then can appear, even with described composition molding, also the crack can appear when drying.
To one skilled in the art, volatile silicone oils used in the present invention can easily be selected from commercially available product.The example that can be used for volatile silicone oils in the present invention includes but not limited to available from the dimethicone DC 200 (0.65cs) of Dow Corning Corporation (Dow Corning) with available from the cyclomethicone DC 345 of Dow Corning Corporation.
In the present invention, in order when improving durability, to keep pie, use trimethylsiloxy group silicate (trimethylsiiloxysilicate) as described organic siliconresin.To one skilled in the art, described trimethylsiloxy group silicate can easily be selected from commercially available product.The example that can be used for the present invention's trimethylsiloxy group silicate includes but not limited to KF-7312F, KF-7312J, KF-7312K, KF-9001, X-21-5249, KF-9002, X-21-5250 and the KF-9021 available from Japanese Shinetsu.
Hereinafter, will the method for the wet moulding of mixture according to the present invention be described.
At first, the mixed solvent of volatile silicone oils and organic siliconresin is put into general agitator with the bottoming powder of coating and seal.Make about 5 minutes of the contents mixed of described agitator, a certain amount of mixture is loaded in the forming disk (molding dish), and carry out molding with the molding cloth that is applied to described forming disk (molding cloth), with absorption with remove the described solvent of about 30-60%.Then, the material of described molding was descended dry 2-12 hour, to remove remaining solvent fully in exsiccator at 60-150 ℃.
The compact composition of described wet moulding of the present invention can have conventional formulation, and said composition has good durability and softish sense of touch.For example, said composition can be made the form of paired cake (twin cake), powder box (compact), muffin (powder compact) and the close powder of compression (pressed powder).Compositions with each these prescription can additionally contain various suitable basis and the additive that needs in the prescription of described compositions, and concerning the staff of this area, the kind of these extra compositions and quantity can be selected easily.
Hereinafter, structure of the present invention and effect will be made further detailed description with test case in conjunction with the embodiments.These examples are for better elaboration the present invention, and scope of invention is not limited in these examples.
Embodiment 1: the fine and close cosmetic combinations of wet moulding
According to compositions as shown in table 1 below, the densification cosmetic compositions of preparation wet moulding.
Table 1
| Component | Content (weight %) |
| 1, is coated with the mixture of powders of polydimethylsiloxane | ??70 |
| 2, organic siliconresin (KF-9002) | ??0.5 |
| 3, silicone oil (DC 200/0.65cs) | ??29.5 |
The mixture of powders of raw material 1 by squalene and dimethicone are added to by Talcum, Muscovitum, sericite, tripoli, nylon powder, silica flour, polymethyl methacrylate (PMMA) as binding agent thereby, make in the powder formed of boron nitride powder and barium sulfate, this mixture of powders is coated with polydimethylsiloxane.
Preparation method: raw material 2 and 3 is mixed under low temperature and low speed in agitator.The mixture of described raw material 2 and 3 is added in the powder of described raw material 1, and make this powder disperse five minutes with preparation slurry phase.A certain amount of described slurry is filled in the forming disk, and the molding cloth that reuse is applied to described forming disk carries out molding, thereby removes the solvent of about 40-50%.Then, the material of this molding was descended dry 6 hours, to remove remaining solvent fully in exsiccator at 60-70 ℃.
Embodiment 2: the densification cosmetic compositions of wet moulding
According to compositions as shown in table 2 below, use the method identical to prepare the densification cosmetic compositions with embodiment 1.
Table 2
| Component | Content (weight %) |
| 1, is coated with the mixture of powders of polydimethylsiloxane | ??70 |
| 2, organic siliconresin (X-21-5250) | ??0.5 |
| 3, silicone oil (DC 200/0.65cs) | ??29.5 |
The mixture of powders of raw material 1 by squalene and dimethicone are added to by Talcum, Muscovitum, sericite, tripoli, nylon powder, silica flour, polymethyl methacrylate (PMMA) as binding agent thereby, make in the powder formed of boron nitride powder and barium sulfate, this mixture of powders is coated with polydimethylsiloxane.
Comparative Examples 1: the densification cosmetic compositions of general wet moulding
According to compositions as shown in table 3 below, use the method identical to prepare the densification cosmetic compositions of Comparative Examples 1 with embodiment 1.
Table 3
| Component | Content (weight %) |
| 1, uncoated mixture of powders | ??70 |
| 2, water-soluble thickening agent (Veegum HV) | ??2.0 |
| 3, water | ??28.0 |
The mixture of powders of raw material 1 by squalene and dimethicone are added to by Talcum, Muscovitum, sericite, tripoli, nylon powder, silica flour, polymethyl methacrylate (PMMA) as binding agent thereby, make in the powder formed of boron nitride powder and barium sulfate, this mixture of powders does not apply.
Comparative Examples 2: the densification cosmetic compositions of general wet moulding
According to compositions as shown in table 4 below, use the method identical to prepare the densification cosmetic compositions of Comparative Examples 2 with embodiment 1.
Table 4
| Component | Content (weight %) |
| 1, is coated with the mixture of powders of polydimethylsiloxane | ??70 |
| 2, water-soluble thickening agent (Veegum HV) | ??2.0 |
| 3, emulsifying agent (AbilEM 90) | ??1.0 |
| 3, water | ??27.0 |
The powder film mixture of raw material 1 by squalene and dimethicone are added to by Talcum, Muscovitum, sericite, tripoli, nylon powder, silica flour, polymethyl methacrylate (PMMA) as binding agent thereby, make in the powder formed of boron nitride powder and barium sulfate, this mixture of powders is coated with polydimethylsiloxane.Use cetyl PEG/PPG-10/1 dimethicone (Abil EM 90) as emulsifying agent.
Test case 1: Evaluation of Durability
To embodiment 1 and 2 and Comparative Examples 1 and 2 in the resistance to water and the oil resistivity of compositions of preparation compare evaluation.And, use after these compositionss by 10 the women consumers of 20-30 between year, the flexibility of these compositionss is compared evaluation.Evaluation result is as shown in table 5 below.
Table 5
| Stability | Resistance to water | Oil resistivity | Flexibility | |
| Embodiment 1 | Stable | ??◎(138°) | ??○(54°) | ??○ |
| Embodiment 2 | Stable | ??◎(134°) | ??○(45°) | ??○ |
| Comparative Examples 1 | Stable | * (can't measure) | * (can't measure) | ??○ |
| Comparative Examples 2 | Stable | ??△ | ??△ | ??△ |
The ※ evaluation criterion
◎: very good, zero: good, △: general, *: poor, and * *: very poor.
The ※ evaluation methodology
1) stability:, observe each compositions simultaneously and As time goes on whether can break, thereby estimate by each compact composition being stored under 37 ℃ the constant temperature.
2) resistance to water: estimate unmixability with water by measuring contact angle.
3) oil resistivity: estimate unmixability with sebum by measuring contact angle.
4) flexibility: test by the group of consumer after each said composition is executed the skin that is overlying on consumer and to assess.
From the result of table 5 as can be seen, for resistance to water and the oil resistivity measured by the measurement of contact angle, embodiment 1 and 2 compositions obviously are better than the compositions of Comparative Examples 1.And, with the compositions of the Comparative Examples 2 of the powder preparation that applies owing to used emulsifying agent, so its resistance to water and oil resistivity are inferior to the compositions of embodiment 1 and 2.
In the test of group of consumer, as can be seen, when consumer directly directly executes the skin that is overlying on consumer with said composition, go out and the similar flexibility of compositions according to the Comparative Examples 1 of existing method preparation according to the compositions display of embodiments of the invention 1.Based on The above results, the compact composition according to embodiments of the invention 1 and 2 has good durability as can be seen.
Claims (10)
1. the densification cosmetic compositions of a wet moulding, said composition contains the bottoming powder of coating, and said composition is used the mixed solvent of volatile silicone oils and organic siliconresin and made.
2. compositions according to claim 1, wherein, described volatile silicone oils and organic siliconresin are to mix in 97: 3 to 99: 1 with weight ratio.
3. compositions according to claim 1, wherein, the bottoming powder of described coating is coated with polydimethylsiloxane or alkyl silane.
4. compositions according to claim 1, wherein, the bottoming powder of described coating is to be selected from least a in the group of being made up of Talcum, Muscovitum, sericite, tripoli, nylon powder, silica flour, polymethyl methacrylate, boron nitride powder and barium sulfate.
5. compositions according to claim 1 wherein, is a benchmark with the gross weight of the described compositions that comprised described mixed solvent before wet moulding, and the content of the bottoming powder of described coating is 60-70 weight %.
6. compositions according to claim 1, wherein, described silicone oil is polydimethylsiloxane or cyclomethicone.
7. compositions according to claim 1, wherein, described organic siliconresin is a trimethylsiloxy group silicate.
8. according to any described compositions among the claim 1-7, wherein, said composition does not contain emulsifying agent.
9. according to any described compositions among the claim 1-7, wherein, said composition has the resistance to water and the oil resistivity of raising, and softish sense of touch is provided.
10. method for preparing the densification cosmetic compositions of wet moulding, this method may further comprise the steps:
1) the bottoming powder that is coated with polydimethylsiloxane or alkyl silane and the mixed solvent of volatile silicone oils and organic siliconresin are mixed in general agitator; And
2) mixture is seated in the compression forming dish, the mixture forming that makes this filling with the molding cloth that is applied to described forming disk to be removing the described solvent of part, and makes the material of this molding dry down to remove remaining solvent at 60-150 ℃ in exsiccator.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020070119349A KR101135252B1 (en) | 2007-11-21 | 2007-11-21 | Wet forming compact composition containing volatile silicone oil and silicone resin |
| KR10-2007-0119349 | 2007-11-21 | ||
| PCT/KR2008/005299 WO2009066862A1 (en) | 2007-11-21 | 2008-09-08 | Wet forming compact composition containing volatile silicone oil and silicone resin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101861136A true CN101861136A (en) | 2010-10-13 |
| CN101861136B CN101861136B (en) | 2012-11-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008801165466A Expired - Fee Related CN101861136B (en) | 2007-11-21 | 2008-09-08 | Wet forming compact composition containing volatile silicone oil and silicone resin |
Country Status (3)
| Country | Link |
|---|---|
| KR (1) | KR101135252B1 (en) |
| CN (1) | CN101861136B (en) |
| WO (1) | WO2009066862A1 (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102753136A (en) * | 2009-11-20 | 2012-10-24 | 株式会社爱茉莉太平洋 | Cosmetic composition containing inorganic powder |
| CN104825346A (en) * | 2015-05-04 | 2015-08-12 | 上海彤颜实业有限公司 | Silicone-containing water-in-oil BB cream |
| CN110996881A (en) * | 2017-07-14 | 2020-04-10 | 科丝美诗株式会社 | Method for forming solid cosmetic containing gelling agent |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101141983B1 (en) * | 2009-08-05 | 2012-05-07 | 한국세라믹기술원 | Boron nitride powder comprising nanoporous silicified phospholipid layers that can impregnate physiologically active material for cosmetic composition and manufacturing method thereof |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5073364A (en) * | 1990-06-19 | 1991-12-17 | Revlon, Inc. | Pressed powder cosmetic product |
| CZ290771B6 (en) * | 1993-10-02 | 2002-10-16 | The Procter & Gamble Company | Make-up composition |
| JP2000281533A (en) * | 1999-03-30 | 2000-10-10 | Pola Chem Ind Inc | Coated powder and composition containing the same |
| JP4602506B2 (en) * | 1999-07-08 | 2010-12-22 | 三好化成株式会社 | Novel coated powder having super-dispersibility and cosmetics containing the same |
| FR2813184B1 (en) * | 2000-08-30 | 2003-01-17 | Oreal | MATTE COSMETIC COMPOSITION COMPRISING A NON-VOLATILE HYDROCARBON OIL AND AN INERT PARTICULATE PHASE |
| US6964773B1 (en) * | 2000-11-22 | 2005-11-15 | L'oreal S.A. | Transfer resistant anhydrous cosmetic composition |
| JP4160273B2 (en) * | 2001-03-30 | 2008-10-01 | 株式会社資生堂 | Powder cosmetic and method for producing the same |
| FR2823100B1 (en) * | 2001-04-10 | 2003-05-30 | Oreal | TWO-LAYER MAKEUP PROCESS AND MAKEUP KIT CONTAINING FIRST AND SECOND COMPOSITIONS |
| US6811770B2 (en) * | 2001-04-10 | 2004-11-02 | L'oreal | Two-coat make-up process and a make-up kit containing first and second compositions |
| KR100663599B1 (en) * | 2001-12-20 | 2007-01-02 | 주식회사 엘지생활건강 | Poder typed color cosmetic |
-
2007
- 2007-11-21 KR KR1020070119349A patent/KR101135252B1/en active IP Right Grant
-
2008
- 2008-09-08 CN CN2008801165466A patent/CN101861136B/en not_active Expired - Fee Related
- 2008-09-08 WO PCT/KR2008/005299 patent/WO2009066862A1/en active Application Filing
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102753136A (en) * | 2009-11-20 | 2012-10-24 | 株式会社爱茉莉太平洋 | Cosmetic composition containing inorganic powder |
| CN102753136B (en) * | 2009-11-20 | 2016-08-03 | 株式会社爱茉莉太平洋 | Comprise the make-up composition of inorganic powder |
| CN104825346A (en) * | 2015-05-04 | 2015-08-12 | 上海彤颜实业有限公司 | Silicone-containing water-in-oil BB cream |
| CN110996881A (en) * | 2017-07-14 | 2020-04-10 | 科丝美诗株式会社 | Method for forming solid cosmetic containing gelling agent |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20090052719A (en) | 2009-05-26 |
| KR101135252B1 (en) | 2012-04-12 |
| CN101861136B (en) | 2012-11-28 |
| WO2009066862A1 (en) | 2009-05-28 |
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