CN101849543A - Compounded sterilizing agent of pyrimidine nucleoside antibiotics and alkene oxime amine - Google Patents
Compounded sterilizing agent of pyrimidine nucleoside antibiotics and alkene oxime amine Download PDFInfo
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- CN101849543A CN101849543A CN 201010184924 CN201010184924A CN101849543A CN 101849543 A CN101849543 A CN 101849543A CN 201010184924 CN201010184924 CN 201010184924 CN 201010184924 A CN201010184924 A CN 201010184924A CN 101849543 A CN101849543 A CN 101849543A
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- oxime amine
- alkene oxime
- pyrimidine nucleoside
- antibiotic
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Abstract
The invention relates to a compounded sterilizing agent of pyrimidine nucleoside antibiotics and alkene oxime amine, which belongs to the technical field of pesticide. The compounded sterilizing agent of the pyrimidine nucleoside antibiotics and the alkene oxime amine is characterized by comprising 0.1 to 50 percent of pyrimidine nucleoside antibiotics and 0.1 to 70 percent of alkene oxime amine. In the compounded sterilizing agent of the pyrimidine nucleoside antibiotics and the alkene oxime amine, the pyrimidine nucleoside antibiotics and the alkene oxime amine are compounded together; and the effect of the alkene oxime amine of inhibiting or killing pathogenic bacteria and the effect of agricultural antibiotic of curing the pathogenic bacteria are utilized. The compounded sterilizing agent of the pyrimidine nucleoside antibiotics and the alkene oxime amine has good effects of preventing and controlling thanatephorus cucumeris and rhizoctonia cerealis, and the preventing and controlling rate can reach over 96 percent through field experiments; the compounded sterilizing agent has high continuity, and the preventing and controlling rate can reach over 93 percent after 14 days when the agent is applied to preventing and controlling the thanatephorus cucumeris and the rhizoctonia cerealis; and the compounded sterilizing agent has low production cost which is over 50 percent lower than that of singly used alkene oxime amine.
Description
Technical field
The invention belongs to technical field of pesticide, be specifically related to a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide that can be used for preventing and treating crop pests such as rice sheath blight disease, wheat sharp eyespot.
Background technology
Rice sheath blight disease is the important disease of the normal property sent out on the paddy rice, on the south the Changjiang river rice district take place serious, thereby it is withered to make that with hazard rice blade, leaf sheath blade is done sth. in advance yellow, the paddy rice functional leaf be injured the back paddy rice can not normally ear from, cause ripening rate and thousand kernel weight to descend, thereby influence rice yield.Rice sheath blight disease all can be fallen ill in whole growth period duration of rice, and is the heaviest with morbidity in 7～September in the Yangtze river basin.The control of China's rice sheath blight disease uses mainly that jinggangmeisu, triazolone, standing grain fringe are peaceful, rice Feng Ling etc. is in premorbid or their early stage spraying control.But single is that control efficiency is bad with the common defective of this series bactericidal agent when preventing and treating rice sheath blight disease, also less stable.All can take place because rice sheath blight disease needs only temperature in rice plant of tillering stage to the maturing stage of earing, humidity is suitable, emergence period is long, and the control efficiency of control medicament is also not ideal, so needs repeatedly, dosage sprays medicine, to keep the control effect to rice sheath blight disease.Increased peasant's production cost like this, also strengthened, also agricultural product quality has been constituted considerable influence simultaneously environmental influence.
Wheat sharp eyespot has become China's wheat district regular incidence evil in recent years.After wheat was infected by the withered bacterium of line, symptoms such as mashed bud, the mashed stem of withered, the colored stalk of sick seedling, withered strain dead ears appearred at each growing stage.Mashed bud bud scale brown stain, back bud is withered to rot, and can not be unearthed; Sick seedling is withered to occur in for 3～4 leaf phases, first existing Intermediate grey on first leaf sheath only, and the scab of brown all around, the back is withered because of can not taking out the young leaves seedling that causes a disease; On the base portion leaf sheath, form Intermediate grey behind the mashed stem jointing of flower stalk, edge beige moire shape scab, after scab merged, basal part of stem was moire flower stalk shape; After withered strain dead ears scab is invaded the stem wall, taupe in the middle of forming, the subcircular of brown or oval eye spot cause stem wall dehydration necrosis all around, and that supply falls short of demand is withered because of nutrient, moisture for last diseased plant, forms withered strain dead ears.In addition, sometimes should disease also can form disease and invade the unconspicuous brown scab that has a common boundary.In recent years, because the change of kind, cropping system, fertilizer and water condition, disease increases the weight of year by year, and the lesion constantly enlarges from south to north.The morbidity underproduction 20～40% early, withered strain dead ears of serious formation or No kernels or seeds are gathered, as in a year of scarcity.The control of China's wheat sharp eyespot is mainly used jinggangmeisu, triazolone, Triadimenol etc. in premorbid or their early stage spraying control.But single is that control efficiency is bad with the common defective of this series bactericidal agent when preventing and treating wheat sharp eyespot, also less stable.
Antibiotic in pyrimidine nucleoside class is pesticide corrosion 120 again, is a kind of alkaline Nucleoside Agricultural Antibiotics, and its sterilizing mechanisms is directly hinder phytopathogen protein synthetic, causes germ death.Based on the prevention protective effect, have certain therapeutic action concurrently.Can be used for preventing and treating the disease such as powdery mildew, black spot, rust, eqpidemic disease, fusarium wilt, anthracnose, banded sclerotial blight of crops such as melon, tobacco, fruit tree, flowers, Chinese cabbage, tomato, watermelon, paddy rice, wheat.To the people, animal low toxicity, noresidue, free from environmental pollution, to crop and natural enemies security, and the effect that stimulates plant growing is arranged.
A large amount of biological activity research show: the alkene oxime amine fungicidal spectrum is wide, activity is high, have prevention and therapeutic action, with environmental organism good compatibility is arranged, the plurality of plant diseases that is caused by mastigomycetes, zygomycete, sac fungi, basidiomycetes and imperfect fungus there is good control efficiency, to powdery mildew, rust control efficiency brilliance.Alkene oxime amine acts on the mitochondrial respiratory of fungi, medicament by with the mitochondria electron transport chain in the combining of composite I II (Cyt bcl compound), to Cyt c, the ATP that destroys fungi is synthetic by Cyt bcl complex logistics for the blocking-up electronics, thereby plays the effect of inhibition or kill fungi.Can be used for preventing and treating plurality of plant diseases such as wheat rust, wheat powdery mildew, wheat sharp eyespot, rice sheath blight disease, false smut, powdery mildew of cucumber, cucumber downy mildew, downy mildew of garpe, alternaria leaf spot of apple, apple mildew, sigatoka, early blight of tomato, pear scab, powdery mildew of strawberry, rust of sunflower.Simultaneously, plant growth proterties and quality are improved significantly, and can improve output.But the alkene oxime amine price comparison is expensive, the use cost height.
Summary of the invention
At the problem that prior art exists, the objective of the invention is to design provide that a kind of lasting effect is long, control efficiency good, quick-acting fast and the pyridine ucleosides antibiotic of preventing and treating rice sheath blight disease, wheat sharp eyespot that cost is low and the technical scheme of alkene oxime amine composite bactericide.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide is characterized in that containing antibiotic in pyrimidine nucleoside class 0.1～50%, alkene oxime amine 0.1～70%.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 0.5～45%, the content of alkene oxime amine is 0.5～65%.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 0.5～40%, the content of alkene oxime amine is 0.5～40%.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 0.5～30%, the content of alkene oxime amine is 1～30%.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 1～20%, the content of alkene oxime amine is 2～25%.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 1～15%, the content of alkene oxime amine is 2～20%.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 2～10%, the content of alkene oxime amine is 2～15%.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 4～8%, the content of alkene oxime amine is 5～15%.
Described antibiotic in pyrimidine nucleoside class is a known substance, is produced and is provided by Ludun Biological Products Co., Ltd., Shaanxi.
Described alkene oxime amine is a known substance, is produced and is provided by Shenyang Kechuang chemicals Co., Ltd.
Described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide can be mixed with the conventional formulations of pesticide with existing conventional auxiliary agent and filling, as wetting powder, suspending agent or the like.
The method that described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide are used to prevent and treat rice sheath blight disease is: at the rice sheath blight disease initial stage of origination, convert 450～900 kilograms of thick mists of spray of water according to the consumption of antibiotic in pyrimidine nucleoside class in the per hectare and alkene oxime amine total amount 10～600 grams.
The method that described a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide are used to prevent and treat wheat sharp eyespot is: at the wheat sharp eyespot initial stage of origination, convert 450～900 kilograms of thick mists of spray of water according to the consumption of antibiotic in pyrimidine nucleoside class in the per hectare and alkene oxime amine total amount 10～600 grams.
Above-mentioned a kind of antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide are with antibiotic in pyrimidine nucleoside class and alkene oxime amine is composite is in the same place, utilized alkene oxime amine that germ is suppressed or the effect of kill pathogens and agricultural antibiotic to the therapeutic action of germ, the present invention is good to rice sheath blight disease, wheat sharp eyespot control efficiency, can reach more than 96% through its control rate of field trial; Continuation is strong, and after control paddy rice, the wheat sharp eyespot medication 14 days, its control rate can reach more than 93%; Production cost is low, reduces more than 50% than independent use alkene oxime amine.
The proportioning that relates among the present invention is the percentage by weight of the pure material of active ingredient.
Embodiment
Below further specify the present invention by specific embodiment.Recompounded pesticide of the present invention can adopt following proportioning to produce:
Prescription one: antibiotic in pyrimidine nucleoside class 0.1%, alkene oxime amine 70%.
Prescription two: antibiotic in pyrimidine nucleoside class 0.5%, alkene oxime amine 65%.
Prescription three: antibiotic in pyrimidine nucleoside class 0.5%, alkene oxime amine 40%.
Prescription four: antibiotic in pyrimidine nucleoside class 1%, alkene oxime amine 25%.
Prescription five: antibiotic in pyrimidine nucleoside class 5%, alkene oxime amine 5%.
Prescription six: antibiotic in pyrimidine nucleoside class 7%, alkene oxime amine 13%.
Prescription seven: antibiotic in pyrimidine nucleoside class 8%, alkene oxime amine 7%.
Prescription eight: antibiotic in pyrimidine nucleoside class 10%, alkene oxime amine 15%.
Prescription nine: antibiotic in pyrimidine nucleoside class 12%, alkene oxime amine 13%.
Prescription ten: antibiotic in pyrimidine nucleoside class 45%, alkene oxime amine 1%.
Fill a prescription 11: antibiotic in pyrimidine nucleoside class 50%, alkene oxime amine 0.1%.
Configuration technology is:
One wetting powder mixes antibiotic in pyrimidine nucleoside class and alkene oxime amine according to the above ratio, add conventional auxiliary agent dodecyl sodium naphthalene sulfonate, bitter edible plant sulfonic acid and formaldehyde, white carbon, fine particle calcium carbonate etc. then, after fully mixing, after the ultrafine crusher pulverizing, both obtained wetting powder.
Two suspending agents mix antibiotic in pyrimidine nucleoside class and alkene oxime amine according to the above ratio, add conventional auxiliary agent methyl naphthalene sulfonate formaldehyde condensate, white carbon black, ethylene glycol, silicone, water then, in sand mill, mill, and have both obtained suspending agent.
One, stripped biological activity test
Stripped biological activity determination all adopts toxic dielectric method, promptly adds quantitative reagent agent (test dose is by active ingredient) in the PD^ medium respectively, and inoculation test pathogen in cooling back is cultivated under 25 ℃ of dark conditions.When treating that the blank colony diameter grows to 40～50mm, measure the colony growth diameter of different disposal respectively, calculate bacteriostasis rate and ECso value that each is handled.Result of the test: the stripped biologically active of mixture has obvious synergistic effect apparently higher than two single agent of contrast, sees example 1～2 for details.
Example 1 rice sheath blight disease
Example 2 wheat sharp eyespots
Through test, the biological activity determination that exsomatizes of other prescriptions among the present invention also can reach and the five and six identical technique effects of filling a prescription.
Two, field control effect test
Carry out the agricultural production routinely of the cultivation management of trial crops under the test field condition.The reagent agent that field efficacy is measured is all established 3 dosage, establishes the blank of not dispenser, 4 repetitions.Test is not fallen ill in the field or the their early stage dispenser, and spraying equipment is a knapsack hand sprayer.Natural occurrence is carried out result's investigation when the blank of not dispenser is fully fallen ill.Disease classification, preventive effect computational methods are all carried out State Standard of the People's Republic of China's [pesticide field efficacy medicine test criterion].Result of the test shows that antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide have very excellent preventive and therapeutic effect to disease, see example 3～4 for details.
Example 3 25% suspending agents are to the field efficacy (prescription nine) of rice sheath blight disease
Example 4 15% suspending agents are to the field efficacy (prescription seven) of wheat sharp eyespot
Through test, other prescriptions among the present invention carry out the field control effect test, also can reach and the seven and nine identical technique effects of filling a prescription.
Claims (8)
1. antibiotic in pyrimidine nucleoside class and alkene oxime amine composite bactericide is characterized in that containing antibiotic in pyrimidine nucleoside class 0.1～50%, alkene oxime amine 0.1～70%.
2. a kind of antibiotic in pyrimidine nucleoside class as claimed in claim 1 and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 0.5～45%, the content of alkene oxime amine is 0.5～65%.
3. a kind of antibiotic in pyrimidine nucleoside class as claimed in claim 1 and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 0.5～40%, the content of alkene oxime amine is 0.5～40%.
4. a kind of antibiotic in pyrimidine nucleoside class as claimed in claim 1 and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 0.5～30%, the content of alkene oxime amine is 1～30%.
5. a kind of antibiotic in pyrimidine nucleoside class as claimed in claim 1 and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 1～20%, the content of alkene oxime amine is 2～25%.
6. a kind of antibiotic in pyrimidine nucleoside class as claimed in claim 1 and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 1～15%, the content of alkene oxime amine is 2～20%.
7. a kind of antibiotic in pyrimidine nucleoside class as claimed in claim 1 and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 2～10%, the content of alkene oxime amine is 2～15%.
8. a kind of antibiotic in pyrimidine nucleoside class as claimed in claim 1 and alkene oxime amine composite bactericide, the content that it is characterized in that antibiotic in pyrimidine nucleoside class is 4～8%, the content of alkene oxime amine is 5～15%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010184924 CN101849543A (en) | 2010-05-27 | 2010-05-27 | Compounded sterilizing agent of pyrimidine nucleoside antibiotics and alkene oxime amine |
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| CN 201010184924 CN101849543A (en) | 2010-05-27 | 2010-05-27 | Compounded sterilizing agent of pyrimidine nucleoside antibiotics and alkene oxime amine |
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| CN101849543A true CN101849543A (en) | 2010-10-06 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103355354A (en) * | 2012-04-09 | 2013-10-23 | 陕西韦尔奇作物保护有限公司 | Bacteriocidal composition containing pyrimidine nucleoside antibiotics and triazoles |
| CN103355352A (en) * | 2012-04-07 | 2013-10-23 | 陕西韦尔奇作物保护有限公司 | Pyrimidine nucleoside antibiotic/methoxy acrylate bactericidal composition |
| CN103371185A (en) * | 2012-04-12 | 2013-10-30 | 陕西韦尔奇作物保护有限公司 | Synergistic antibacterial composition containing pyrimidine nucleoside antibiotics |
| CN103371187A (en) * | 2012-04-13 | 2013-10-30 | 陕西韦尔奇作物保护有限公司 | Bactericidal composition containing agricultural antibiotic |
| CN103535381A (en) * | 2012-07-12 | 2014-01-29 | 陕西美邦农药有限公司 | Triazolone-containing bactericidal composition |
| CN103621561A (en) * | 2012-08-23 | 2014-03-12 | 陕西美邦农药有限公司 | High-efficient bactericidal composition containing hexamethylene flusulfamide |
| CN104336080A (en) * | 2014-10-30 | 2015-02-11 | 陕西绿盾生物制品有限责任公司 | Bactericidal composition containing pyrimidine nucleoside antibiotic and hymexazol and application of bactericidal composition |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103355352A (en) * | 2012-04-07 | 2013-10-23 | 陕西韦尔奇作物保护有限公司 | Pyrimidine nucleoside antibiotic/methoxy acrylate bactericidal composition |
| CN103355352B (en) * | 2012-04-07 | 2016-12-14 | 陕西韦尔奇作物保护有限公司 | Bactericidal composition containing antibiotic in pyrimidine nucleoside class Yu methoxy acrylic |
| CN103355354B (en) * | 2012-04-09 | 2017-02-15 | 青岛金尔农化研制开发有限公司 | Bacteriocidal composition containing pyrimidine nucleoside antibiotics and triazoles |
| CN103355354A (en) * | 2012-04-09 | 2013-10-23 | 陕西韦尔奇作物保护有限公司 | Bacteriocidal composition containing pyrimidine nucleoside antibiotics and triazoles |
| CN103371185A (en) * | 2012-04-12 | 2013-10-30 | 陕西韦尔奇作物保护有限公司 | Synergistic antibacterial composition containing pyrimidine nucleoside antibiotics |
| CN103371185B (en) * | 2012-04-12 | 2017-02-15 | 马国丰 | Synergistic antibacterial composition containing pyrimidine nucleoside antibiotics |
| CN103371187A (en) * | 2012-04-13 | 2013-10-30 | 陕西韦尔奇作物保护有限公司 | Bactericidal composition containing agricultural antibiotic |
| CN103371187B (en) * | 2012-04-13 | 2017-03-08 | 林芬兰 | Bactericidal composition containing antibiotic in pyrimidine nucleoside class |
| CN103535381A (en) * | 2012-07-12 | 2014-01-29 | 陕西美邦农药有限公司 | Triazolone-containing bactericidal composition |
| CN103535381B (en) * | 2012-07-12 | 2015-04-15 | 陕西美邦农药有限公司 | Triazolone-containing bactericidal composition |
| CN103621561A (en) * | 2012-08-23 | 2014-03-12 | 陕西美邦农药有限公司 | High-efficient bactericidal composition containing hexamethylene flusulfamide |
| CN103621561B (en) * | 2012-08-23 | 2015-04-15 | 陕西美邦农药有限公司 | High-efficient bactericidal composition containing hexamethylene flusulfamide |
| CN104336080A (en) * | 2014-10-30 | 2015-02-11 | 陕西绿盾生物制品有限责任公司 | Bactericidal composition containing pyrimidine nucleoside antibiotic and hymexazol and application of bactericidal composition |
| CN104336080B (en) * | 2014-10-30 | 2016-08-24 | 陕西麦可罗生物科技有限公司 | A kind of containing antibiotic in pyrimidine nucleoside class and the bactericidal composition of hymexazol and application |
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Application publication date: 20101006 |