CN101774793A - Preparation method of environment-friendly dry powder pointing agent - Google Patents

Preparation method of environment-friendly dry powder pointing agent Download PDF

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Publication number
CN101774793A
CN101774793A CN200910199591A CN200910199591A CN101774793A CN 101774793 A CN101774793 A CN 101774793A CN 200910199591 A CN200910199591 A CN 200910199591A CN 200910199591 A CN200910199591 A CN 200910199591A CN 101774793 A CN101774793 A CN 101774793A
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CN
China
Prior art keywords
powder
environment
dry powder
friendly dry
percent
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN200910199591A
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Chinese (zh)
Other versions
CN101774793B (en
Inventor
杨佳俊
郑爱新
陆文雄
麻新闻
曹栋樑
李小亮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANGHAI BEIHENG CHEMICAL BUILDING MATERIAL CO Ltd
Shanghai Haili Industry & Trading Co Ltd
University of Shanghai for Science and Technology
Original Assignee
SHANGHAI BEIHENG CHEMICAL BUILDING MATERIAL CO Ltd
Shanghai Haili Industry & Trading Co Ltd
University of Shanghai for Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by SHANGHAI BEIHENG CHEMICAL BUILDING MATERIAL CO Ltd, Shanghai Haili Industry & Trading Co Ltd, University of Shanghai for Science and Technology filed Critical SHANGHAI BEIHENG CHEMICAL BUILDING MATERIAL CO Ltd
Priority to CN2009101995919A priority Critical patent/CN101774793B/en
Publication of CN101774793A publication Critical patent/CN101774793A/en
Application granted granted Critical
Publication of CN101774793B publication Critical patent/CN101774793B/en
Expired - Fee Related legal-status Critical Current
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Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00017Aspects relating to the protection of the environment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00034Physico-chemical characteristics of the mixtures
    • C04B2111/00215Mortar or concrete mixtures defined by their oxide composition
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00663Uses not provided for elsewhere in C04B2111/00 as filling material for cavities or the like
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention relates to a preparation method of an environment-friendly dry powder pointing agent taking slag powder as main raw materials, belonging to the technical field of building material preparation processes. The environment-friendly dry powder pointing agent comprises the raw materials in percentage by weight: 55-75 percent of slag powder, 2-10 percent of cement, 10-30 percent of calcite powder, 2-5 percent of re-dispersible emulsoid powder and 0.05-0.3 percent of thickening agent. The environment-friendly dry powder pointing agent has good caking property, good durability and high antiseepage grade, is not in contact with a tapestry brick, generates no cracks, and can effectively inhibit saltpetering. The invention widens a new approach for the resource utilization of the slag powder and has better social efficiency and economic benefit.

Description

The preparation method of environment-friendly dry powder pointing agent
Technical field
The present invention relates to a kind of is the preparation method of the environment-friendly dry powder pointing agent of main raw material with the slag micropowder, belongs to material of construction fabricating technology field.
Background technology
The tile pointing agent claims that again spackling and caulking agent are the joint fillers that is used to fill slit between ceramic tile or stone material, and the facing that provides attractive in appearance and guarantee bonding and antiseepage between the facing tile matches with finishing material such as ceramic tile, stone materials.Along with the fast development of Building Trade in China, more and more higher to the requirement of tile pointing agent, consumption is also increasing.In the raw material of jointing agent, cement is an indispensable part.Yet cement is big because of its rigidity, fragility is alkaline strong, occurs the crack and the accumulation of salt in the surface soil easily, causes infiltration and variable color.Therefore releasing and utilize industrial residue to produce the problem of jointing agent, is the needs of solid waste resource recovery and recycling economy, also is the needs of jointing agent Materials science development.Researcher is utilizing slag micropowder as main raw material at present, prepares environment-friendly dry powder pointing agent.
Summary of the invention
The purpose of this invention is to provide a kind of is the preparation method of the environment-friendly dry powder pointing agent of main raw material with the slag micropowder.
The present invention is a kind of to be the preparation method of main raw material with the slag micropowder, it is characterized in that having following process and step:
A. design determines that the raw material of jointing agent is formed and weight percent is:
Slag micropowder 55~75%;
Cement 2~10%;
Calcite in powder 10~30%;
Redispersable latex powder 2~5%;
Thickening material 0.05~0.3%;
The chemical ingredients of described slag micropowder is: (wt%)
SiO 230.5, Al 2O 313.9 CaO 40.9, MgO 8.6, Fe 2O 30.4, TiO 20.7 MnO 0.2, P 2O 50.05 S 2.5; Specific surface area 〉=500m 2/ kg;
Described cement is commercially available 42.5 grades of ordinary Portland cements;
Described calcite in powder, its fineness are 100~150 orders;
Described redispersable latex powder is any in styrene-propene yogurt rubber powder, acrylate latex powder, the vinyl acetate-ethylene latex powder; Its fineness is 100 orders;
Described thickening material is any in Natvosol, hydroxyethylmethyl-cellulose, the hydroxypropylcellulose;
B. press above-mentioned raw materials prescription weigh batching,, above-mentioned each raw material is put into mixing machine successively close, after fully mixing, promptly get the environment-friendly dry powder pointing agent that can suppress the accumulation of salt in the surface soil by the traditional technology method.
When granulated blast-furnace slag is iron work ironmaking, the waste residue that from blast furnace, produces.Granulated blast-furnace slag and cement are more approaching on main component, and its main chemical compositions is SiO 2, CaO, Al 2O 3, MgO, Fe 2O 3Deng, have the potential activity, after levigate, the slag activity is brought into play.Can be used to replace part cement.The specific surface area of the blast-furnace cinder micro-powder after levigate is generally at 400~600m 2/ kg, more less than the particle of 30 μ m, size-grade distribution is optimized, and after cement mixing, the further density of refinforced cement slurry has been improved the impermeability of cement.Slag is prepared the tile pointing agent as main raw material, can obviously suppress the accumulation of salt in the surface soil and variable color.Consider that from environment, technology, economical effectiveness equal angles it is coming that breeze is carried out recycling.
Characteristics of the present invention and advantage are as follows:
(1), the environment-friendly dry powder pointing agent cohesiveness that makes of the present invention is good, can closely contact with facing tile, do not produce the crack.Its good endurance, impervious grade height, effectively waterproof.
(2), the present invention is because to adopt ironmaking waste residue slag micropowder be main raw material, so cost is low, and production technique is simple, helps suitability for industrialized production and applies.
(3), cement industry is the industry of the unsustainable development of heavily contaminated, it is main raw material that the present invention adopts slag micropowder, can reduce the consumption of cement, prepares a kind of high-performance environmentally-friendly type dry powder pointing agent, it can effectively suppress the accumulation of salt in the surface soil.
(4), the present invention adds the thickening material of significant quantity, has water retaining function, and can strengthen anti-the contraction and splitting resistance, improves the thixotropy and the sag resistance of product, plays certain thickening power.
Embodiment
After now specific embodiments of the invention being described in.
Embodiment 1: proportioning at first in accordance with regulations takes by weighing 10kg42.5 level ordinary Portland cement, slag micropowder 60kg, calcite in powder 25.9kg, redispersable latex powder 4kg and thickening material 0.1kg, above-mentioned admixtion is put into mixing machine, after fully mixing, can obtain environment-friendly dry powder pointing agent.
Embodiment 2: proportioning at first in accordance with regulations takes by weighing 42.5 grades of ordinary Portland cements of 3kg, slag micropowder 75g, calcite in powder 19.3kg, redispersable latex powder 2.5g and thickening material 0.2g, above-mentioned admixtion is put into mixing machine, after fully mixing, can obtain environment-friendly dry powder pointing agent.
Get the above-mentioned environment-friendly dry powder pointing agent 1kg that makes, add water 0.4kg, be stirred well to paste, placed 10 minutes, promptly can be used for the jointing of facing tiles such as ceramic tile or stone material.
The prepared environment-friendly dry powder pointing agent of the foregoing description all can meet every technical performance index of relative national standards regulation.

Claims (1)

1. the preparation method's of an environment-friendly dry powder pointing agent preparation method is characterized in that having following process and step:
A. design determines that the raw material of jointing agent is formed and weight percent is:
Slag micropowder 55~75%;
Cement 2~10%;
Calcite in powder 10~30%;
Redispersable latex powder 2~5%;
Thickening material 0.05~0.3%;
The chemical ingredients of described slag micropowder is: (wt%)
SiO 230.5, Al 2O 313.9 CaO 40.9, MgO 8.6, Fe 2O 30.4, TiO 20.7 MnO 0.2, P 2O 50.05 S 2.5; Specific surface area 500m 2/ kg;
Described cement is commercially available 42.5 grades of ordinary Portland cements;
Described calcite in powder, its fineness are 100~150 orders;
Described redispersable latex powder is any in styrene-propene yogurt rubber powder, acrylate latex powder, the vinyl acetate-ethylene latex powder; Its fineness is 100 orders;
Described thickening material is any in Natvosol, hydroxyethylmethyl-cellulose, the hydroxypropylcellulose;
B. press above-mentioned raw materials prescription weigh batching,, above-mentioned each raw material is put into mixing machine successively, after fully mixing, promptly get the environment-friendly dry powder pointing agent that can suppress the accumulation of salt in the surface soil by the traditional technology method.
CN2009101995919A 2009-11-26 2009-11-26 Preparation method of environment-friendly dry powder pointing agent Expired - Fee Related CN101774793B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009101995919A CN101774793B (en) 2009-11-26 2009-11-26 Preparation method of environment-friendly dry powder pointing agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2009101995919A CN101774793B (en) 2009-11-26 2009-11-26 Preparation method of environment-friendly dry powder pointing agent

Publications (2)

Publication Number Publication Date
CN101774793A true CN101774793A (en) 2010-07-14
CN101774793B CN101774793B (en) 2012-11-07

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102674761A (en) * 2012-04-24 2012-09-19 广州绿宇建筑材料有限公司 Method for preparing joint sealant by utilizing construction wastes
CN103159447A (en) * 2013-03-13 2013-06-19 厦门路桥翔通建材科技有限公司 Composition and its preparation method and use
CN103570324A (en) * 2012-08-08 2014-02-12 吉安市艾生建材科技有限公司 Economical crack-sealer as well as production method thereof
CN104496374A (en) * 2014-12-08 2015-04-08 青阳县天工预拌商品砂浆有限公司 Environmental-friendly inorganic concrete and preparation method thereof
CN104529320A (en) * 2014-12-08 2015-04-22 青阳县天工预拌商品砂浆有限公司 Energy-saving type impervious waterproof building concrete and preparation method thereof
WO2016062233A1 (en) * 2014-10-21 2016-04-28 Silverloy Company Limited Antibacterial product and antibacterial structure
CN105884269A (en) * 2014-11-25 2016-08-24 重庆益生宜居建材科技有限公司 Tile grout
CN108504283A (en) * 2018-05-15 2018-09-07 合肥语林装饰工程有限公司 A kind of resistant antibiotic ceramic tile gap filler and preparation method thereof
CN113582630A (en) * 2021-09-07 2021-11-02 河北金铎建设工程有限公司 Thermal insulation wall body decorative layer dry material, mortar and wall body

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1280222C (en) * 2004-04-07 2006-10-18 上海宝田新型建材有限公司 Modified gypsum composite binding material and its producing method
CN1781866A (en) * 2004-11-29 2006-06-07 王正深 Polymer modified cement
CN101531478A (en) * 2008-03-14 2009-09-16 杨荣福 High performance mineral additive

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102674761B (en) * 2012-04-24 2015-05-20 广州世正环保科技发展有限公司 Method for preparing joint sealant by utilizing construction wastes
CN102674761A (en) * 2012-04-24 2012-09-19 广州绿宇建筑材料有限公司 Method for preparing joint sealant by utilizing construction wastes
CN103570324B (en) * 2012-08-08 2016-04-06 吉安市艾生建材科技有限公司 A kind of economical jointing agent and production method
CN103570324A (en) * 2012-08-08 2014-02-12 吉安市艾生建材科技有限公司 Economical crack-sealer as well as production method thereof
CN103159447B (en) * 2013-03-13 2014-11-05 厦门路桥翔通建材科技有限公司 Composition and its preparation method and use
CN103159447A (en) * 2013-03-13 2013-06-19 厦门路桥翔通建材科技有限公司 Composition and its preparation method and use
WO2016062233A1 (en) * 2014-10-21 2016-04-28 Silverloy Company Limited Antibacterial product and antibacterial structure
CN105884269A (en) * 2014-11-25 2016-08-24 重庆益生宜居建材科技有限公司 Tile grout
CN104529320A (en) * 2014-12-08 2015-04-22 青阳县天工预拌商品砂浆有限公司 Energy-saving type impervious waterproof building concrete and preparation method thereof
CN104496374A (en) * 2014-12-08 2015-04-08 青阳县天工预拌商品砂浆有限公司 Environmental-friendly inorganic concrete and preparation method thereof
CN108504283A (en) * 2018-05-15 2018-09-07 合肥语林装饰工程有限公司 A kind of resistant antibiotic ceramic tile gap filler and preparation method thereof
CN113582630A (en) * 2021-09-07 2021-11-02 河北金铎建设工程有限公司 Thermal insulation wall body decorative layer dry material, mortar and wall body
CN113582630B (en) * 2021-09-07 2022-05-27 河北金铎建设工程有限公司 Thermal insulation wall body decorative layer dry material, mortar and wall body

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