CN101725059B - Method for non-bath dyeing and stuffing of leather - Google Patents

Method for non-bath dyeing and stuffing of leather Download PDF

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Publication number
CN101725059B
CN101725059B CN2009101177351A CN200910117735A CN101725059B CN 101725059 B CN101725059 B CN 101725059B CN 2009101177351 A CN2009101177351 A CN 2009101177351A CN 200910117735 A CN200910117735 A CN 200910117735A CN 101725059 B CN101725059 B CN 101725059B
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China
Prior art keywords
leather
water
dyeing
stuffing
water squeezing
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Expired - Fee Related
Application number
CN2009101177351A
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Chinese (zh)
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CN101725059A (en
Inventor
尹岳涛
李臣
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GANSU HONGLIANG LEATHER CO Ltd
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GANSU HONGLIANG LEATHER CO Ltd
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Priority to CN2009101177351A priority Critical patent/CN101725059B/en
Publication of CN101725059A publication Critical patent/CN101725059A/en
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Publication of CN101725059B publication Critical patent/CN101725059B/en
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Abstract

The invention provides a method for non-bath dyeing and stuffing of leather. The process steps comprise retanning neutralization, water squeezing, dyeing and stuffing, out-of-drum and horse stacking, water squeezing, vacuum drying, hanging drying, moisture regaining, milling, surface cleaning, toggling and crush leather obtaining. In the water squeezing step, a passage water squeezing machine is used, and after the water squeezing step, the water content in wet blue leather is 35 to 40 percent. In the method, the dyeing and the stuffing are performed under a non-bath liquid condition, so that under the condition that the dyeing and stuffing effects of the leather are not lowered, the water and the energy are greatly saved; more than 5 tons of water can be saved when one ton of blue wet leather is processed, the discharge of sewage and waste water is reduced; waste water is basically not discharged in the step of dyeing and the stuffing; and thus, the production cost and the environmental protection cost are saved, and water is also saved.

Description

Method for non-bath dyeing and stuffing of leather
Technical field
The present invention relates to the leather processing technical field, is a kind of method for non-bath dyeing and stuffing of leather specifically.
Background technology
Traditional dyeing stuffing raw materials technology is the blue wet pelt leather behind the shaving, weighs as the materials benchmark process:
Temperature adjustment-70 ℃ hot water temperature adjustment is controlled water to 50-55 ℃, and the raffinate ratio is about 1.5, and promptly surplus water is 150%, and the actual used water amount is 250-300%; Stuffing-ammoniacal liquor 0.5%, dyestuff 0-5% changeed 30 minutes, and fatting agent 18-22% changeed 90 minutes, and formic acid 1% 15 minutes at interval adds at twice and fixes, and rotates then 30 minutes; Washing cooling-normal temperature waterside adds limit control water, and the interior temperature of drum is reduced to below 45 ℃ gradually, and the washing water is 200-300%; Go out drum; Take horse; Water squeezing is stretched; Extension dries dry.Traditional leather coloring stuffing need be carried out under the condition of 1.5-2.5 times of liquor ratio, 50-55 ℃.Temperature adjustment will be used 70 ℃ of hot water, and the water yield of using in the dyeing course is bigger, also can produce industrial wastewater in a large number simultaneously.Leather manufacturing enterprise needs corresponding techniques, finishing agent and personnel to support for sewage disposal, causes production cost to strengthen.
Summary of the invention
Technical problem to be solved by this invention is under the condition of no body lotion, to carry out stuffing dyeing; When not reducing leather coloring oiling effect; Save water and energy and reduce the discharging of sewage, waste water, thereby reduce production costs and the environmental protection cost, a kind of method for non-bath dyeing and stuffing of leather is provided for this reason.
Technical problem of the present invention solves through following technical proposals:
A kind of method for non-bath dyeing and stuffing of leather is characterized in that processing step comprises: retanning neutralization-water squeezing-dyeing and fat-liquoring-go out drum take horse-water squeezing-vacuumize-extension dry dry-soft-crust leather of washing one's face-toggling-process gets damp again-falls.
Through type wringing machine, wet blue moisture 35-40% after the water squeezing are adopted in described water squeezing.
Described dyeing and fat-liquoring is: do not have to bathe, normal temperature is the materials benchmark with the weight of the blue wet pelt behind the shaving,
Fatting agent 20-22% and dyestuff 0-5% are melted with 70 ℃ of hot water, add the high speed rotary drum and rotated 10 minutes, the wet blue rotating speed 45-50 commentaries on classics/min after the adding water squeezing changeed 90 minutes;
Inspection: the dyestuff fatting agent is scattered in leather, evenly absorbed by skin;
10 times of warm water dilutions of formic acid 1.2% usefulness of concentration content 40% slowly add from axis hole while rotating, and are rotated further 30 minutes, and dyestuff, fatting agent, retanning agent and hide fiber are combined securely;
Inspection: the dyestuff fatting agent absorbs fully, the no greasy feeling in surface.
The present invention carries out stuffing dyeing under the condition of no body lotion; When not reducing leather coloring oiling effect; Significantly save water and energy, process 1 ton of wet blue water saving more than 5 tons, and reduce the discharging of sewage, waste water; The basic non-wastewater discharge of dyeing and fat-liquoring operation, thus reduce production costs and the water saving of environmental protection cost.
The specific embodiment
Below in conjunction with embodiment the present invention is further elaborated.
Embodiment 1
(1) weighs: take by weighing 100 kilograms of blue wet pelts behind the shaving, as following materials foundation.
(2) retanning neutralization: conventional method is carried out.
(3) water squeezing: through type wringing machine, wet blue moisture 35% after the water squeezing.
(4) dyeing and fat-liquoring: 100 kilograms that do not have to bathe the blue wet pelt of normal temperature after with shaving is the materials benchmark, 20 kilograms of fatting agents, 5 kilograms of dyestuffs, and 70 ℃ of hot water melt, and add the high speed rotary drum, rotate 10 minutes.
(5) wet blue after the adding water squeezing adds one by one, prevents to twine, and rotating speed 45-50 commentaries on classics/min changeed 90 fens;
Inspection: the dyestuff fatting agent is scattered in leather, evenly absorbed by skin;
(6) with 1.2 kilograms in the formic acid of concentration 40%, with the dilution of 12 intensification water, slowly add from axis hole while rotating, be rotated further 30 minutes, dyestuff, fatting agent, retanning agent and hide fiber are combined securely;
Inspection: the dyestuff fatting agent absorbs fully, the no greasy feeling in surface.
(7) conventional method go out drum take horse-water squeezing-vacuumize-extension dry dry-soft-crust leather of washing one's face-toggling-process gets damp again-falls.
Embodiment 2
(1) weighs: take by weighing 100 kilograms of blue wet pelts behind the shaving, as following materials foundation.
(2) retanning neutralization: conventional method is carried out.
(3) water squeezing: through type wringing machine, wet blue moisture 40% after the water squeezing.
(4) dyeing and fat-liquoring: do not have bathing the blue wet pelt of normal temperature after with shaving is the materials benchmark for 100 kilograms, 22 kilograms of fatting agents, and the leather of true qualities need not add dyestuff, and without dyestuff, 70 ℃ of hot water melt, and add the high speed rotary drum and rotate 10 minutes;
(5) wet blue after the adding water squeezing adds one by one, prevents to twine, and rotating speed 45-50 commentaries on classics/min changeed 90 fens;
Inspection: the dyestuff fatting agent is uniformly dispersed.
(6) with 1.2 kilograms in the formic acid of concentration 40%, with the dilution of 12 intensification water, slowly add from axis hole while rotating, be rotated further 30 minutes;
Inspection: the dyestuff fatting agent absorbs fully, the no greasy feeling in surface.
(7) conventional method go out drum take horse-water squeezing-vacuumize-extension dry dry-soft-crust leather of washing one's face-toggling-process gets damp again-falls.

Claims (2)

1. method for non-bath dyeing and stuffing of leather is characterized in that processing step comprises: retanning neutralization-water squeezing-dyeing and fat-liquoring-go out drum take horse-water squeezing-vacuumize-extension dry dry-soft-crust leather of washing one's face-toggling-process gets damp again-falls;
Described dyeing and fat-liquoring is: do not have to bathe, normal temperature is the materials benchmark with the weight of the blue wet pelt behind the shaving; Fatting agent 20-22% and dyestuff 0-5% are melted with 70 ℃ of hot water; Add the high speed rotary drum and rotated 10 minutes, the wet blue rotating speed 45-50 commentaries on classics/min after the adding water squeezing changeed 90 minutes;
Inspection: the dyestuff fatting agent is scattered in leather, evenly absorbed by skin;
10 times of warm water dilutions of formic acid 1.2% usefulness of concentration 40% slowly add from axis hole while rotating, and are rotated further 30 minutes, and dyestuff, fatting agent, retanning agent and hide fiber are combined securely;
Inspection: the dyestuff fatting agent absorbs fully, the no greasy feeling in surface.
2. a kind of non-bath dyeing and stuffing of leather technology according to claim 1 is characterized in that described water squeezing employing through type wringing machine, wet blue moisture 35-40% after the water squeezing.
CN2009101177351A 2009-12-14 2009-12-14 Method for non-bath dyeing and stuffing of leather Expired - Fee Related CN101725059B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009101177351A CN101725059B (en) 2009-12-14 2009-12-14 Method for non-bath dyeing and stuffing of leather

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Application Number Priority Date Filing Date Title
CN2009101177351A CN101725059B (en) 2009-12-14 2009-12-14 Method for non-bath dyeing and stuffing of leather

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CN101725059B true CN101725059B (en) 2012-01-18

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104032599B (en) * 2014-05-27 2016-02-10 上海应用技术学院 A kind of colouring method of cortical fibers
CN104032598B (en) * 2014-05-27 2016-02-10 上海应用技术学院 A kind of non-impregnated colouring method of cortical fibers

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1048905A (en) * 1990-05-30 1991-01-30 惠彬 Dye stuff polymerzation bathless dry dyeing method for leather dyeing
CN1079003A (en) * 1993-05-06 1993-12-01 师昌友 The production method of elastic goat soft leather
CN1492057A (en) * 2003-09-23 2004-04-28 杭州水乡渔业有限公司 Tanning method for fish skin and after finishing method for fish skin leather

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1048905A (en) * 1990-05-30 1991-01-30 惠彬 Dye stuff polymerzation bathless dry dyeing method for leather dyeing
CN1079003A (en) * 1993-05-06 1993-12-01 师昌友 The production method of elastic goat soft leather
CN1492057A (en) * 2003-09-23 2004-04-28 杭州水乡渔业有限公司 Tanning method for fish skin and after finishing method for fish skin leather

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
单志华.黄牛全粒面汽车坐垫生产工艺.《制革化学与工艺学》.科学出版社,2005,第371-373页. *

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