CN101633822A - Additive capable of removing unhealthy smell in cigarette contact glue, preparation method and use method thereof - Google Patents
Additive capable of removing unhealthy smell in cigarette contact glue, preparation method and use method thereof Download PDFInfo
- Publication number
- CN101633822A CN101633822A CN200910094659A CN200910094659A CN101633822A CN 101633822 A CN101633822 A CN 101633822A CN 200910094659 A CN200910094659 A CN 200910094659A CN 200910094659 A CN200910094659 A CN 200910094659A CN 101633822 A CN101633822 A CN 101633822A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- chinese date
- parts
- additive
- overlapping glue
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses an additive capable of removing unhealthy smell in cigarette contact glue, a preparation method and a use method thereof. The additive is obtained after 25 portions of jujube volatile, 1 portion of vanilline, 22 portions of cigarette flavoring agent, 2 portions of phenyl ethyl cinnamate and 50 portions of solvent are evenly mixed. The additive is added to cigarette contact glue by 0.05% of use quantity. Fragrance and materials are added to the cigarette contact glue for the first time. After being applied, the additive obviously enhances the original fragrance of a cigarette and improves unhealthy smell brought by the combustion of the cigarette contact glue. Moreover, the gluing efficiency of the treated cigarette contact glue is not reduced to any degree. The preparation method has the advantages of simpleness, convenience and low cost and can be applied to large-scale industrial production.
Description
Technical field
The invention belongs to cigarette and use the meat flavor formulating technology field, be specifically related to a kind of additive that can remove cigarette with adverse chemical breath in tackiness agent, the particularly cigarette overlapping glue.Simultaneously, the invention still further relates to the preparation method of this additive.
Background technology
At present, along with people to improving constantly that cigarette quality requires, cigarette jealous, inhale flavor and burning back the hazard rating of human body all become the focus that numerous smokers pay close attention to.And cigarette uses tackiness agent as one of important auxiliary material of cigarette, for the suction quality of cigarette and the biological safety of cigarette material impact is arranged all.They generally are made up of base-material, solidifying agent, thinner, softening agent, filler, coupling agent and other subsidiary material.The tackiness agent of different purposes has in various degree influence for the suction quality of cigarette, this wherein, the overlapping glue of participating in cigarette burning directly is very big for the suction quality influence of cigarette.In the combustion processes of overlapping glue, can produce volatile matter such as benzene,toluene,xylene, normal hexane, acetone, ethyl acetate, not only influence the cigarette smoking quality but also can work the mischief human body.Therefore, it is significant to carry out the technical study of removing the adverse chemical breath at cigarette tackiness agent, particularly overlapping glue.But not seeing as yet in the prior art has good terms of settlement.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of additive that can give cigarette tackiness agent tobacco bad assorted gas fragrant naturally, that produce when covering the overlapping glue burning is provided.
The present invention also aims to provide a kind of method for preparing described additive.
Purpose of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage ratio of the present invention is weight percentage.
A kind of additive that can remove bad breath in the cigarette overlapping glue is made by the raw material of following weight part: 25 parts of Chinese date volatile matters, 1 part of vanillin food grade,1000.000000ine mesh, 22 parts in tobacco flavouring base, 50 parts of 2 parts of phenyl ethyl cinnamates and solvents.
Prepare the above-mentioned method that can remove the additive of bad breath in the cigarette overlapping glue, may further comprise the steps:
1, preparation Chinese date volatile matter:
1. raw materials pretreatment: fresh Chinese date cleaned remove silt and seed, at 80 ± 2 ℃ of following forced air drying 3h, the control water ratio is 5%～10%, and the raw material after the oven dry was crushed to 120 orders～150 mesh sieves immediately;
2. alcohol reflux: with 5 times heavy 75% ethanol, 80 ℃ of refluxing extraction 3 times, each 1h obtains the Chinese date tincture after the filtration;
3. the pre-treatment of resin: before the dress post, polymeric adsorbent is handled with dilute sodium chloride and sodium carbonate solution, and washing is with the sanitas of removing trace and residual monomeric compound;
4. it is refining to cross post: Chinese date tincture upper prop is used water and 3 times of 20% ethanol elution of 6 times of resin volumes respectively near saturated, then with 60% ethanol elution Chinese date effective constituent, again through vacuum concentration, obtains the Chinese date separated portion after the lyophilize;
5. adopt steam distillation to distill separated portion, in the collection, lower boiling volatile constituent, promptly get the Chinese date volatile matter behind the concentrate drying;
2, with 25 parts of Chinese date volatile matters, 1 part of vanillin food grade,1000.000000ine mesh promptly obtains the required additive that can remove bad breath in the cigarette overlapping glue after 22 parts in tobacco flavouring base, 50 parts of 2 parts of phenyl ethyl cinnamates and solvents mix.
The above-mentioned using method that can remove the additive of bad breath in the cigarette overlapping glue: overlapping glue is placed the polymeric kettle that has whipping appts and condenser, be warming up to 90 ± 2 ℃, stir overlapping glue to even matter, be cooled to 75 ℃, add emulsifying agent and defoamer (add-on of the two is controlled in 3%), continue to be cooled to 50 ℃, then slowly add described additive, addition is 0.05% of an overlapping glue consumption, and begins to stir with the rotating speed of 120rpm, keeps fixed temperature and humidity in the whipping process, the joining day of essence is controlled at about 0.5h, continue after essence adds to keep stirring 1h, add the pH regulator agent, plastic emitting behind the stirring 0.5h.
With respect to prior art, the present invention has the following advantages:
1, the flavoring and casing technology is one of gordian technique that improves the cigarette smoking quality always, but at present, is mainly used in also that tobacco perfuming is reinforced, aspects such as stem flavoring and casing, thin slice flavoring and casing and filter tip flavoring and casing.The present invention launches the flavoring and casing technical study at the overlapping glue that participates in cigarette burning first, with the additive and the conventional overlapping glue that make mix join after, can obviously improve this perfume (or spice) of tobacco of cigarette, improve the bad breath that cigarette overlapping glue burns and brings.
2, contain more tobacco aroma component in the Chinese date volatile matter, these aroma components can play increases cigarette perfume (or spice), improve the effect that cigarette is jealous, cover bad assorted gas.Meanwhile, can not bring assorted gas again, influence the Harmony of cigarette cigarette itself.
3, the use of this additive can reduce the generation of organic compound such as overlapping glue burning back benzene,toluene,xylene, normal hexane, acetone, ethyl acetate, improve the biological safety of cigarette, and can improve to a certain extent and inhale flavor, improve the suction comfortableness, the highlight products personal characteristics.
4, the domestic effective binding speed of high speed cigarette glue of being produced at present can reach 6000/minute, and through the cigarette glue after this flavoring and casing technical finesse, its adhesion efficiency is without any the reduction of degree.
5, preparation method of the present invention is easy, and is with low cost, can be applicable to large-scale industrial production.
Embodiment
The present invention is described further below in conjunction with embodiment, but they are not limitation of the invention.
Embodiment 1
Preparation can be removed the additive of bad breath in the cigarette overlapping glue.With fresh Chinese date clean remove silt and seed after, at 80 ± 2 ℃ of following forced air drying 3h, the control water ratio is 7%, the raw material after the oven dry was crushed to 130 mesh sieves immediately.With 5 times heavy 75% ethanol, 80 ℃ of refluxing extraction 3 times, each 1h obtains the Chinese date tincture after the filtration.Before the dress post, polymeric adsorbent is handled with dilute sodium chloride and sodium carbonate solution, and washing is with the sanitas of removing trace and residual monomeric compound.Chinese date tincture upper prop is used water and 3 times of 20% ethanol elution of 6 times of resin volumes respectively near saturated, then with 60% ethanol elution Chinese date effective constituent, again through vacuum concentration, obtains the Chinese date separated portion after the lyophilize.Adopt steam distillation to distill separated portion, in the collection, lower boiling volatile constituent, promptly get the Chinese date volatile matter behind the concentrate drying.Take by weighing 25 parts of Chinese date volatile matters, 1 part of vanillin food grade,1000.000000ine mesh makes required additive after 22 parts in tobacco flavouring base, 50 parts of 2 parts of phenyl ethyl cinnamates and solvents mix.
Embodiment 2
Repeat embodiment 1, following difference is arranged: Chinese date is dried to water ratio 5%, is crushed to 120 mesh sieves.
Embodiment 3
Repeat embodiment 1, following difference is arranged: Chinese date is dried to water ratio 10%, is crushed to 150 mesh sieves.
Application Example 1
Overlapping glue is placed the polymeric kettle that has whipping appts and condenser, be warming up to 90 ± 2 ℃, stir overlapping glue to even matter, be cooled to 75 ℃, add emulsifying agent and defoamer, the add-on of the two is controlled in 3%, continue to be cooled to 50 ℃, then slowly add embodiment 1 gained additive, addition is 0.05% of an overlapping glue consumption, and begin to stir with the rotating speed of 120rpm, keep fixed temperature and humidity in the whipping process, the joining day of essence is controlled at 0.5h, and essence adds the back and continues to keep stirring 1h, add the pH regulator agent, plastic emitting behind the stirring 0.5h.
Overlapping glue behind the perfuming is applied to red production of converging a cloud and mist, and the overlapping glue add-on is carried out with reference to high speed cigarette glue industry add-on standard.
Sensory evaluation scores
At the cigarette product behind the perfuming according to the test of smokeing panel test of evaluation and analysis standard.Evaluation and analysis group is made up of ten cigarette sensory evaluation experts, selects for use the blind mode of commenting to carry out sensory evaluation and marking.Sense organ marking is the result show, the scoring on assorted gas of the product behind the perfuming increases by 0.4.
Instrument detecting
Select for use the Pintsch process gas chromatography-mass spectrography that overlapping glue cracking composition before and after the perfuming is carried out analyzing and testing.Concrete analytical procedure is, get a certain amount of sample and put into the cracking dedicated quartz tube of thermo-cracking instrument, place the heater strip of the cracking head of thermo-cracking instrument then, the cracking head inserts in the homemade Glass Containers, carries out thermo-cracking respectively under the cracking temperature of 400 ℃ and 700 ℃.After thermo-cracking finishes, use solid phase micro-extracting head in 70 ℃ of following enrichment thermal cracking products 20min respectively, then extracting head is inserted desorption in the gas-chromatography high-temperature evaporation chamber (temperature is 240 ℃), the desorption time is 2min, at last, thermal cracking products enters gas chromatography/mass spectrometry (GC/MS) and separates and identify.Analysis condition is: the thermo-cracking condition is for to carry out the aerobic cracking in atmospheric environment, wherein free air temperature is 30 ℃.The GC/MS condition is: injector temperature: 240 ℃; Carrier gas: He, 1mL/min; Heating schedule: 50 ℃ (keeping 1min)--5 ℃/min--100 ℃ (keeping 1min)--8 ℃/min--260 ℃ (keeping 1min); GC-MS interface temperature: 280 ℃; Ion source (EI) temperature: 250 ℃; Ionizing energy: 70eV; Mass scanning scope: 35～455amu.Using NIST98 standard spectrum storehouse retrieves.Detecting the back by analysis finds, adopt the overlapping glue after this flavoring and casing technology, in its split product, the content of benzene,toluene,xylene, normal hexane, acetone, ethyl acetate reduces by 32.5%, 39.6%, 41.2%, 38.6%, 30.8%, 37.1% respectively, can effectively reduce the organic content more than 30% that brings the adverse chemical breath so this technological invention has reached.
Application Example 2
Overlapping glue behind the perfuming is applied to a red production of Red Hill tea cigarette of converging, and the overlapping glue add-on is carried out with reference to high speed cigarette glue industry add-on standard.Sense organ marking is the result show, the scoring on assorted gas of the product behind the perfuming increases by 0.2.
Application Example 3
Overlapping glue behind the perfuming is applied to red production of converging ball tea steamed twisted roll cigarette, and the overlapping glue add-on is carried out with reference to high speed cigarette glue industry add-on standard.Sense organ marking is the result show, the scoring on assorted gas of the product behind the perfuming increases by 0.5.
Application Example 4
Overlapping glue behind the perfuming is applied to a red production of lesser panda cigarette of converging, and the overlapping glue add-on is carried out with reference to high speed cigarette glue industry add-on standard.Sense organ marking is the result show, the scoring on assorted gas of the product behind the perfuming respectively increases by 0.4.
Claims (3)
1, a kind of additive that can remove bad breath in the cigarette overlapping glue is made by the raw material of following weight part: 25 parts of Chinese date volatile matters, 1 part of vanillin food grade,1000.000000ine mesh, 22 parts in tobacco flavouring base, 50 parts of 2 parts of phenyl ethyl cinnamates and solvents.
2, prepare the method for the described additive of claim 1, may further comprise the steps:
(1) preparation Chinese date volatile matter:
1. raw materials pretreatment: fresh Chinese date cleaned remove silt and seed, at 80 ± 2 ℃ of following forced air drying 3h, the control water ratio is 5%～10%, and the raw material after the oven dry was crushed to 120 orders～150 mesh sieves immediately;
2. alcohol reflux: with 5 times heavy 75% ethanol, 80 ℃ of refluxing extraction 3 times, each 1h obtains the Chinese date tincture after the filtration;
3. the pre-treatment of resin: before the dress post, polymeric adsorbent is handled with dilute sodium chloride and sodium carbonate solution, and washing is with the sanitas of removing trace and residual monomeric compound;
4. it is refining to cross post: Chinese date tincture upper prop is used water and 3 times of 20% ethanol elution of 6 times of resin volumes respectively near saturated, then with 60% ethanol elution Chinese date effective constituent, again through vacuum concentration, obtains the Chinese date separated portion after the lyophilize;
5. adopt steam distillation to distill separated portion, in the collection, lower boiling volatile constituent, promptly get the Chinese date volatile matter behind the concentrate drying;
(2) with 25 parts of Chinese date volatile matters, 1 part of vanillin food grade,1000.000000ine mesh promptly obtains the required additive that can remove bad breath in the cigarette overlapping glue after 22 parts in tobacco flavouring base, 50 parts of 2 parts of phenyl ethyl cinnamates and solvents mix.
3, the using method of the described additive of claim 1, it is characterized in that: overlapping glue is placed the polymeric kettle that has whipping appts and condenser, be warming up to 90 ± 2 ℃, stir overlapping glue to even matter, be cooled to 75 ℃, add emulsifying agent and defoamer, the add-on of the two continues to be cooled to 50 ℃ in 3%, then slowly add described additive, addition is 0.05% of an overlapping glue consumption, and begins to stir with the rotating speed of 120rpm, keeps fixed temperature and humidity in the whipping process, the joining day of essence is controlled at about 0.5h, continue after essence adds to keep stirring 1h, add the pH regulator agent, plastic emitting behind the stirring 0.5h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910094659A CN101633822A (en) | 2009-06-25 | 2009-06-25 | Additive capable of removing unhealthy smell in cigarette contact glue, preparation method and use method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910094659A CN101633822A (en) | 2009-06-25 | 2009-06-25 | Additive capable of removing unhealthy smell in cigarette contact glue, preparation method and use method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101633822A true CN101633822A (en) | 2010-01-27 |
Family
ID=41593164
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910094659A Pending CN101633822A (en) | 2009-06-25 | 2009-06-25 | Additive capable of removing unhealthy smell in cigarette contact glue, preparation method and use method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101633822A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029692A (en) * | 2015-06-01 | 2015-11-11 | 湖北中烟工业有限责任公司 | Cigarette with fragrant lap adhesive colored tape and manufacturing method of cigarette |
| CN109123754A (en) * | 2018-09-20 | 2019-01-04 | 云南中烟工业有限责任公司 | A kind of high efficiency preparation method and purposes of jujube absolute oil |
| CN113403000A (en) * | 2021-05-28 | 2021-09-17 | 湖北中烟工业有限责任公司 | Mouth-connecting glue for slow-release cigarette and preparation method and application thereof |
-
2009
- 2009-06-25 CN CN200910094659A patent/CN101633822A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029692A (en) * | 2015-06-01 | 2015-11-11 | 湖北中烟工业有限责任公司 | Cigarette with fragrant lap adhesive colored tape and manufacturing method of cigarette |
| CN109123754A (en) * | 2018-09-20 | 2019-01-04 | 云南中烟工业有限责任公司 | A kind of high efficiency preparation method and purposes of jujube absolute oil |
| CN109123754B (en) * | 2018-09-20 | 2021-02-26 | 云南中烟工业有限责任公司 | Efficient preparation method and application of red date absolute |
| CN113403000A (en) * | 2021-05-28 | 2021-09-17 | 湖北中烟工业有限责任公司 | Mouth-connecting glue for slow-release cigarette and preparation method and application thereof |
| CN113403000B (en) * | 2021-05-28 | 2022-05-17 | 湖北中烟工业有限责任公司 | Mouth-connecting glue for slow-release fragrance-holding cigarette and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101586057B (en) | Essence for cigarette mouth building adhesive and preparing and using method thereof | |
| CN103045369B (en) | Preparation method for reaction type spice for cigarette and application of reaction type spice to cigarette | |
| CN106165906B (en) | Suitable for the burnt fragrant and sweet spices of the malt of cigarette products and the application tobacco product | |
| CN103436363B (en) | Preparation method of aroma substance in Zimbabwe tobacco extractive as well as products and application of aroma substance | |
| CN105105318B (en) | Aroma brewing flavor for cigarettes and application thereof in improving smoking quality of cigarettes | |
| CN104489910A (en) | Flue-cured type electronic cigarette liquid | |
| CN103966027B (en) | A kind of preparation method of the composite extract of Herba Rosmarini Officinalis | |
| CN106263013A (en) | A kind of high fragrance tobacco extract and application thereof | |
| CN105831792A (en) | Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco | |
| CN108504454A (en) | A kind of modified form cigarette preparation method of liquor tailing fragrance and its application in cigarette | |
| CN106010797B (en) | A kind of burnt fragrant and sweet fragrance of the malt prepared using melanoidin malt as raw material and its application in electronic cigarette | |
| CN108244594A (en) | A kind of Zanthoxylum essential oil and preparation method thereof | |
| CN101633822A (en) | Additive capable of removing unhealthy smell in cigarette contact glue, preparation method and use method thereof | |
| CN111849636A (en) | Spice for wine-roasted Chinese angelica cigarette and preparation method and application thereof | |
| CN106723315A (en) | A kind of preparation method of electronic cigarette raw material | |
| CN102229862A (en) | Preparation of mulberry leaf volatile oil and application thereof in tobacco flavoring | |
| CN111004679B (en) | Lysimachia capillipes extract and essence | |
| CN107677754A (en) | A kind of medicinal extract class tobacco aromaticss analysis of aroma components pre-treating method | |
| CN103013667B (en) | Tobacco fragrance as well as preparation method and application thereof | |
| CN109393568A (en) | It is a kind of for heating the burley tobaccos extract and preparation method thereof for the cigarette that do not burn | |
| JP6714502B2 (en) | Method for roasting coffee beans and method for producing coffee extract for enhancing fruity aroma | |
| CN101323817A (en) | Cooked puerh tea essential oil, preparation and use thereof | |
| CN102993159B (en) | Method for separating oxacyclopentadecane-2-ketone from bamboo fungus | |
| CN114634842A (en) | Tobacco flavor, preparation method and application thereof | |
| CN104489929B (en) | Cigar type electronic cigarette liquid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Open date: 20100127 |