CN101608150A - Formula of foaming agent in the neutral soap - Google Patents
Formula of foaming agent in the neutral soap Download PDFInfo
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- CN101608150A CN101608150A CNA2009101821279A CN200910182127A CN101608150A CN 101608150 A CN101608150 A CN 101608150A CN A2009101821279 A CNA2009101821279 A CN A2009101821279A CN 200910182127 A CN200910182127 A CN 200910182127A CN 101608150 A CN101608150 A CN 101608150A
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- massfraction
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- foaming agent
- soap
- igepon
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Abstract
Formula of foaming agent in the neutral soap belongs to the household chemicals technical field.Pore forming material of the present invention mainly is made up of anion surfactant, amphoterics and nonionogenic tenside, and the anion surfactant that adds among the present invention has: Igepon A (Igepon A), sodium soap, sulfo-succinic acid fatty alcohol-polyoxyethylene ether ester disodium (MES); Amphoterics is cocamidopropyl betaine (CAB); Nonionogenic tenside is Vykamol Sorbitol 8B (Tween).Pore forming material is composite by tensio-active agent, has improved the foaming and the foam stability energy of neutral perfumed soap.
Description
Technical field
The present invention relates to a kind of formula of foaming agent of articles for washing, particularly the formula of foaming agent that is added in the neutral soap belongs to the household chemicals technical field.
Background technology
Perfumed soap is a kind of daily chemical products commonly used, though the kind of articles for washing is various day by day at present, constantly has product innovation to come out, and perfumed soap still has the very big using value and the market share as a kind of traditional articles for washing.Mostly domestic prior art is with the sodium soap to be that main raw material is produced perfumed soap, and these perfumed soap alkalescence are stronger, though have good washing clean effect, but it easily makes skin dry and astringent, bigger to skin irritation, select the abundant perfumed soap of lipid content, this situation is improved.
Neutral soap involved in the present invention is exactly a kind of superfatted soap, and this perfumed soap is a main raw material with Igepon A (IgeponA).IgeponA is a kind of anion surfactant, is slightly acidic, and degrease power is low, the performance gentleness, pungency is little, and foam is abundant fine and smooth, with after can give to feel as the skin silk, resistance to hard water is strong, and biological degradability is good, with other tensio-active agent excellent compatibility is arranged.The free fatty acids that adds in the neutral soap plays the effect of soft skin moisten, and extremely the human consumer parent looks at.But, the foaming properties of the main raw material of neutral soap has been produced restraining effect just because of the existence of free fatty acids.Carrying out compositely so add other tensio-active agent in prescription, can be very necessary with foaming and the foam stability that improves neutral soap.
Summary of the invention
The prescription that the purpose of this invention is to provide the pore forming material that adds in a kind of neutral soap is used to improve the lathering property and the foam stability energy of neutral soap.
Technical scheme of the present invention: the pore forming material in the neutral soap, prescription mainly comprises anion surfactant, amphoterics and nonionogenic tenside.Wherein anion surfactant is Igepon A (Igepon A), sodium soap, sulfo-succinic acid fatty alcohol-polyoxyethylene ether ester disodium (MES); Amphoterics is cocamidopropyl betaine (CAB); Nonionogenic tenside is Vykamol Sorbitol 8B (Tween).In the formula of foaming agent, each components contents is as follows:
(1) massfraction of Igepon A in formula of foaming agent is 60%～80%.
(2) massfraction of sodium soap in formula of foaming agent is 8%～20%.
(3) massfraction of MES in formula of foaming agent is 0～6%.
(4) massfraction of CAB in formula of foaming agent is 4%～15%.
(5) massfraction of Tween in formula of foaming agent is 1%～10%.
Beneficial effect of the present invention: pore forming material is composite by tensio-active agent, has improved the foaming and the foam stability energy of neutral perfumed soap.
Embodiment
Embodiment 1
Raw material and originate as follows in the prescription:
Igepon A self-control
Oil chemistry Industrial Co., Ltd in sodium soap (neat soap 8020) Shanghai is good
CAB-35 (35%) Chengdu industry development company limited of HTC of section
MES (30%) Guangdong Research Institute Petrochemical Industry
Yixing, Tween-20 Jiangsu tonneau chemical industry goods and materials company limited
Tween-80 Jiangsu Yixing Kai Lida chemistry company limited
Lipid acid (lauric acid: tetradecanoic acid: stearic acid mass ratio 3: 5: 2)
Lianyun Harbour Yi Hai oiling Industrial Co., Ltd
With Igepon A massfraction 72.5%, sodium soap massfraction 14.5%, CAB-35 massfraction 11.6%, Tween-20 massfraction 1.4%, preparation pore forming material 1 mixes through stirrer.
With Igrepon A massfraction 80%, lipid acid massfraction 20%, preparation sample 1, stirrer stirs, and grinds 6 times with three-roll grinder again, makes each component thorough mixing;
With the massfraction 80% of pore forming material 1, lipid acid massfraction 20% is prepared sample 2, presses the hybrid mode mixing of sample 1.
The foaming properties test is with reference to China's national standard (GB/T 7462-94), and promptly the Ross-Miles method is carried out, and key step is as follows:
(1) takes by weighing 1.000g sample 1 respectively or sample 2 is put into beaker, add the Ca of 50mL 3mmol/L
2+Hard water, heating is all dissolved sample, solution is quantitatively moved in the volumetric flask of 1000mL with hard water then, and constant volume is put into water bath with thermostatic control constant temperature 30min in the time of 50 ℃, then as solution to be measured.
(2) the Luo Shi Latherometer feeds recirculated water, constant temperature to 50 ± 0.5 ℃.With solution rinse Luo Shi Latherometer to be measured, and solution to be measured is added to the 50mL scale place of Luo Shi Latherometer lower end.
(3) draw solution to be measured to its 200mL scale place with the supporting dropping funnel of Luo Shi Latherometer, solution is all flowed down on the chuck graduated cylinder top of Luo Shi Latherometer, produce foam.Foam height when after this writing down 30s, 3min, 5min, 10min, 15min, 20min.
(4) parallel laboratory test is carried out in repeating step (2), (3), writes down 3 times foam height, averages.Its whipability of mean value sign of foam height during 30s, its foam stability of mean value sign of foam height during 10min.
Table 1 sample 1 foaming properties is measured
Table 2 sample 2 foaming properties are measured
The foaming properties measurement result of sample 1, sample 2 is shown in table 1, table 2.The mass percent of lipid acid is about 20% in the neutral soap prescription, therefore adds 20% lipid acid in sample, to investigate the foaming properties of pore forming material.Mixed whipability of Igepon A and lipid acid and foam stability all are suppressed.With the tensio-active agent of other kinds and Igepon A composite after, as pore forming material 1, whipability and foam stability are improved, the foam height during 30s has increased by 1 times, the foam height during 10min has increased by 1.5 times.
Embodiment 2:
Raw material and source are with embodiment 1 in the prescription.With IgeponA massfraction 71.0%, sodium soap massfraction 10.5%, MES massfraction 3.0%, CAB-35 massfraction 12.0%, Tween-20 massfraction 3.5%, preparation pore forming material 2 mixes through stirrer.
With the massfraction 80% of pore forming material 2, lipid acid massfraction 20%, preparation sample 3, stirrer stirs, and grinds 6 times with three-roll grinder again, makes each component thorough mixing.
Press the whipability and the foam stability of foaming properties test determines sample 3 among the embodiment 1, the results are shown in Table 3.
Table 3 sample 3 foaming properties are measured
Embodiment 3:
Raw material and source are with embodiment 1 in the prescription.With IgeponA massfraction 67.5%, sodium soap massfraction 15.5%, CAB-35 massfraction 13%, Tween-80 massfraction 4%, preparation pore forming material 3 mixes through stirrer.
With the massfraction 80% of pore forming material 3, lipid acid massfraction 20%, preparation sample 4, stirrer stirs, and grinds 6 times with three-roll grinder again, makes each component thorough mixing.
Press the whipability and the foam stability of foaming properties test determines sample 4 among the embodiment 1, the results are shown in Table 4.
Table 4 sample 4 foaming properties are measured
Claims (1)
1, the pore forming material in the neutral soap is characterized in that comprising anion surfactant, amphoterics and nonionogenic tenside in the prescription;
The anion surfactant that adds is Igepon A Igepon A, sodium soap, sulfo-succinic acid fatty alcohol-polyoxyethylene ether ester disodium MES;
The amphoterics that adds is cocamidopropyl betaine CAB;
The nonionogenic tenside that adds is Vykamol Sorbitol 8B Tween;
In the formula of foaming agent, each components contents is as follows:
The massfraction of Igepon A in formula of foaming agent is 60%～80%;
The massfraction of sodium soap in formula of foaming agent is 8%～20%;
The massfraction of MES in formula of foaming agent is 0～6%;
The massfraction of CAB in formula of foaming agent is 4%～15%;
The massfraction of Tween in formula of foaming agent is 1%～10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101821279A CN101608150B (en) | 2009-07-14 | 2009-07-14 | Formula of foaming agent in neutral soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101821279A CN101608150B (en) | 2009-07-14 | 2009-07-14 | Formula of foaming agent in neutral soap |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101608150A true CN101608150A (en) | 2009-12-23 |
| CN101608150B CN101608150B (en) | 2011-05-11 |
Family
ID=41482060
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009101821279A Expired - Fee Related CN101608150B (en) | 2009-07-14 | 2009-07-14 | Formula of foaming agent in neutral soap |
Country Status (1)
| Country | Link |
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| CN (1) | CN101608150B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101831285A (en) * | 2010-05-24 | 2010-09-15 | 中国石油集团川庆钻探工程有限公司 | Foaming agent resisting high temperature, high salt and condensate oil for fracturing and preparation method thereof |
| CN112317136A (en) * | 2020-10-16 | 2021-02-05 | 吉安天卓选矿药剂有限公司 | Odorless environment-friendly foaming agent and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| HUT65146A (en) * | 1991-03-21 | 1994-04-28 | Procter & Gamble | Mild personal cleansig bar produced by improved method |
| US5294363A (en) * | 1991-09-23 | 1994-03-15 | The Procter & Gamble Company | Mild personal cleansing bar composition with balanced surfactants, fatty acids, and paraffin wax |
| ES2201107T3 (en) * | 1994-05-10 | 2004-03-16 | THE PROCTER & GAMBLE COMPANY | COMPOSITIONS FOR SYNTHETIC SOAP PAD FOR PERSONAL HYGIENE WITH LOW LEVELS OF NON-ION POLYMERS POLYETHYLENE / POLYPROPYLENE GLYCOL THAT IMPROVE SOFTENING. |
-
2009
- 2009-07-14 CN CN2009101821279A patent/CN101608150B/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101831285A (en) * | 2010-05-24 | 2010-09-15 | 中国石油集团川庆钻探工程有限公司 | Foaming agent resisting high temperature, high salt and condensate oil for fracturing and preparation method thereof |
| CN101831285B (en) * | 2010-05-24 | 2013-03-13 | 中国石油集团川庆钻探工程有限公司 | Foaming agent resisting high temperature, high salt and condensate oil for fracturing and preparation method thereof |
| CN112317136A (en) * | 2020-10-16 | 2021-02-05 | 吉安天卓选矿药剂有限公司 | Odorless environment-friendly foaming agent and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101608150B (en) | 2011-05-11 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110511 Termination date: 20130714 |