CN102787037A - Transparent soap - Google Patents

Transparent soap Download PDF

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Publication number
CN102787037A
CN102787037A CN2012103149659A CN201210314965A CN102787037A CN 102787037 A CN102787037 A CN 102787037A CN 2012103149659 A CN2012103149659 A CN 2012103149659A CN 201210314965 A CN201210314965 A CN 201210314965A CN 102787037 A CN102787037 A CN 102787037A
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CN
China
Prior art keywords
acid
transparent soap
soap
aes
transparent
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Granted
Application number
CN2012103149659A
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Chinese (zh)
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CN102787037B (en
Inventor
黄宏光
杨壮荣
韦炳君
潘泳言
何建峰
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GUANGXI AOQILI CO Ltd
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GUANGXI AOQILI CO Ltd
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Priority to CN201210314965.9A priority Critical patent/CN102787037B/en
Publication of CN102787037A publication Critical patent/CN102787037A/en
Application granted granted Critical
Publication of CN102787037B publication Critical patent/CN102787037B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention provides a transparent soap which is prepared from the following raw materials in percentage by weight through fine processing: 20-35% of glycerol, 20-35% of sorbierite, 2-8% of propylene glycol, 2-6% of dodecanoic acid, 1-4% of tetradecanoic acid, 2-6% of hexadecanoic acid, 8-12% of octadecanoic acid, 8-10% of 30% liquid alkali, 0-1% of potassium hydroxide, 8-13% of sodium alcohol ether sulfate (AES), 0-0.5% of sodium carbonate and 2-8% of de-ionized water. The transparent soap provided by the invention has functions of cleaning and moisturizing skin. By improvement of the traditional prescription, the production cost is lowered, the discharge of wastewater, waste gas and waste residue in a production process is decreased, the pollution of industrial production to the environment is effectively reduced, the skin-moisturizing function of the transparent soap is added, and the is transparent soap suitable for daily cleaning and cosmetic skin care.

Description

A kind of transparent soap
Technical field:
The present invention relates to a kind of transparent soap, particularly a kind of transparent fully, have the best proportioning of the transparent soap and the raw materials for production thereof of cleaning, skin moisten effect.
Background technology:
Developing rapidly of detergent industry forces also constantly progressive and self-breakthrough of this conventional washing agent of soap.Along with the cleaning product competition is increasing, the human consumer improves the requirement of soap day by day, and soap series products such as transparent soap, crystal soap arise at the historic moment, and are developing rapidly in recent years, have obtained the consistent of producers and consumers and have approved.For the purpose of standard, Ministry of Light Industry is " transparent soap " in industry standard title " translucent washing soap " revision with issue in 1994 and enforcement in 2004, and translucent washing soap, transparent laundry soap, crystal soap and band look product thereof are referred to as transparent soap.
The glittering and translucent outward appearance of transparent soap is given pure luxurious sensation, and includes wetting Agent for Printing Inks, and is just more and more popular to people.Transparent soap is main raw material with various natural fats and oils, softener and wetting Agent for Printing Inks mainly, through saponification reaction, and the moulding cooling, transparent slaking is washed the mill shaping and is formed.It is transparent, and rich color is easy to moulding, and is low to skin irritation, and comprehensive clearing power is good, flush away nature sebum within reason again, and the composition of preserving moisture is abundant, is the high-grade personal-care supplies that integrate cleaning the present age, improve looks, preserve moisture.
The conventional transparent soap is a main raw material with plam oil, Semen Maydis oil, Viscotrol C, coconut wet goods Vegetable oil lipoprotein, through operations such as decolouring, deodorizing, saponification, is accompanied by the discharging of waste water, waste gas and waste residue in the production process.Environment is caused severe contamination, run counter to the requirement of the strategy of sustainable development.
Summary of the invention:
It is precise and appropriate to the objective of the invention is to invent a kind of proportioning raw materials, can reduce the industrial pollution that causes in process of production, keeps to use effect constant, has cleaning function, and performance is gentle, nourishes skin moisten, is applicable to the transparent soap of daily cleaning and beauty and skin care.
Transparent soap of the present invention is characterized in that it is processed through precision work by the formula material that comprises following weight percent: glycerine 20-35%, sorbyl alcohol 20-35%, Ucar 35 2-8%, dodecylic acid 2-6%, tetradecanoic acid 1-4%, hexadecanoic acid 2-6%, octadecanoic acid 8-12%, 30% liquid caustic soda 8-10%, Pottasium Hydroxide 0-1%, polyoxyethylenated alcohol sodium sulfate (AES) 8-13%, yellow soda ash 0-0.5%, deionized water 2-8%.
The optimum weight per-cent of its raw material is: glycerine 26%, sorbyl alcohol 28%, Ucar 35 5%, dodecylic acid 3%, tetradecanoic acid 2%, hexadecanoic acid 4%, octadecanoic acid 9%, 30% liquid caustic soda 8.5%, Pottasium Hydroxide 0.4%, polyoxyethylenated alcohol sodium sulfate (AES) 11%, yellow soda ash 0.1%, deionized water 3%.
In the above-mentioned raw materials, in lipid acid and the alkali with after become soap, glycerine, sorbyl alcohol, Ucar 35, AES are composite transparent agent and softener, they promptly can be made into the transparent soap with above-mentioned characteristic after mixing by suitable technology.
Dodecylic acid is a raw material of producing perfumed soap, washing composition, makeup tensio-active agent and man-made fiber finish; Tetradecanoic acid is main as the raw material of producing tensio-active agent; Hexadecanoic acid is a kind of saturated higher fatty acid, as precipitation agent, chemical reagent and water-resisting agent; Octadecanoic acid is a kind of staple that constitutes the animal and plant grease, can be used for products such as pharmaceutical prepn, ointment, soap and suppository; Glycerine have preserve moisture, special efficacy such as anti-oxidant, short alcoholization; Sorbyl alcohol as antidesiccant, can strengthen the extensibility and the oilness of emulsifying agent in makeup, little to skin irritation; AES has good decontamination, emulsification, foam performance and anti-performance of hard water, and gentle washing character can injured skin.
Gained finished product of the present invention meets following requirement:
Index name The sense organ requirement Content (%)
Outward appearance Transparent
Color and luster Faint yellow
Total working substance ≥60
Moisture and volatile matter content ≤30
Total free alkali (in NaOH) ≤0.3
Free caustic alkali (in NaOH) ≤0.1
Muriate (in NaCl) ≤1.0
Advantage of the present invention is:
Through improvement to conventional transparent soap raw material, rely on perfect production unit and the production technique of Ao Qili limited-liability company, when guaranteeing that the transparent soap functions of use is constant, raw material is carried out precise and appropriate compatibility, reduce production costs; Reduce the transparent soap discharging of waste water, waste gas and waste residue in process of production, effectively reduce the pollution of industrial production environment; Increase the skin moisten function of transparent soap.
Embodiment:
Prescription 1: glycerine 26kg, sorbyl alcohol 28kg, Ucar 35 5kg, dodecylic acid 3kg, tetradecanoic acid 2kg, hexadecanoic acid 4kg, octadecanoic acid 9kg, 30% liquid caustic soda 8.5kg, Pottasium Hydroxide 0.4kg, polyoxyethylenated alcohol sodium sulfate (AES) 11kg, yellow soda ash 0.1kg, deionized water 3kg.
Prescription 2: glycerine 35kg, sorbyl alcohol 20kg, Ucar 35 4kg, dodecylic acid 2kg, tetradecanoic acid 4kg, hexadecanoic acid 2kg, octadecanoic acid 10kg, 30% liquid caustic soda 9.1kg, Pottasium Hydroxide 0.2kg, polyoxyethylenated alcohol sodium sulfate (AES) 10kg, yellow soda ash 0.1kg, deionized water 3.6kg.
Prescription 3: glycerine 20kg, sorbyl alcohol 35kg, Ucar 35 4kg, dodecylic acid 2kg, tetradecanoic acid 1kg, hexadecanoic acid 6kg, octadecanoic acid 9kg, 30% liquid caustic soda 8.8kg, Pottasium Hydroxide 0.1kg, polyoxyethylenated alcohol sodium sulfate (AES) 10kg, yellow soda ash 0.2kg, deionized water 3.9kg.
Prescription 4: glycerine 28kg, sorbyl alcohol 25kg, Ucar 35 4kg, dodecylic acid 2kg, tetradecanoic acid 4kg, hexadecanoic acid 2kg, octadecanoic acid 10kg, 30% liquid caustic soda 9.1kg, Pottasium Hydroxide 0.2kg, polyoxyethylenated alcohol sodium sulfate (AES) 10kg, yellow soda ash 0.1kg, deionized water 5.6kg.
Prescription 5: glycerine 23kg, sorbyl alcohol 30kg, Ucar 35 4kg, dodecylic acid 2kg, tetradecanoic acid 1kg, hexadecanoic acid 6kg, octadecanoic acid 9kg, 30% liquid caustic soda 8.8kg, Pottasium Hydroxide 0.1kg, polyoxyethylenated alcohol sodium sulfate (AES) 10kg, yellow soda ash 0.2kg, deionized water 5.9kg.
Making method is:
(1) accurately takes by weighing raw material by above-mentioned prescription;
(2) with heating in sorbyl alcohol, glycerine and the AES adding premix pot and stirring;
(3) in driving the material pot, add Ucar 35, glycerine, dodecylic acid, tetradecanoic acid, hexadecanoic acid, octadecanoic acid and deionized water and be heated to 65-75 ℃, and stir;
(4) adding Pottasium Hydroxide and alkali lye neutralize time 3-10 minute in above-mentioned (3);
(5) mixed solution in above-mentioned (2) is added in (4);
(6) extracting work in-process chemically examines;
(7) confirm the amount of required yellow soda ash according to result of laboratory test, the dissolving back adds in above-mentioned (5) stirred 5-10 minute, and it is stirred;
(8) discharging, moulding, cooling forming.

Claims (2)

1. a transparent soap is characterized in that it is to be processed through precision work by the formula material of following weight percent: glycerine 20-35%, sorbyl alcohol 20-35%, Ucar 35 2-8%, dodecylic acid 2-6%, tetradecanoic acid 1-4%, hexadecanoic acid 2-6%, octadecanoic acid 8-12%, 30% liquid caustic soda 8-10%, Pottasium Hydroxide 0-1%, polyoxyethylenated alcohol sodium sulfate (AES) 8-13%, yellow soda ash 0-0.5%, deionized water 2-8%.
2. transparent soap according to claim 1, the best that it is characterized in that its composition of raw materials is formed weight percent and is: glycerine 26%, sorbyl alcohol 28%, Ucar 35 5%, two alkanoic acids 3%, tetradecanoic acid 2%, hexadecanoic acid 4%, octadecanoic acid 9%, 0% liquid caustic soda 8.5%, Pottasium Hydroxide 0.4%, polyoxyethylenated alcohol sodium sulfate (AES) 11%, yellow soda ash 0.1%, deionized water 3%.
CN201210314965.9A 2012-08-28 2012-08-28 Transparent soap Expired - Fee Related CN102787037B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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CN102787037B CN102787037B (en) 2014-05-14

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013715A (en) * 2012-12-20 2013-04-03 广东鹏锦实业有限公司 Transparent soap
CN104250593A (en) * 2013-06-28 2014-12-31 蔡佐良 Light-transmitting soap base and light-transmitting flower soap body prepared by applying same
CN105886171A (en) * 2016-04-18 2016-08-24 广西南宁皂和奇迹科技有限公司 Transparent soap and preparation method thereof
CN109666545A (en) * 2018-12-28 2019-04-23 中山市天图精细化工有限公司 A kind of efficient cleaning toilet foam aerosol and preparation method thereof
CN110257199A (en) * 2019-08-01 2019-09-20 广州倾镜生物科技有限公司 A kind of handmade soap soap base formula and preparation method thereof
CN110564529A (en) * 2019-09-19 2019-12-13 广州倾镜生物科技有限公司 preparation method of handmade soap base and handmade soap base
CN110846158A (en) * 2019-11-28 2020-02-28 安徽倾镜生物科技有限公司 Preparation method of amino acid soap and amino acid soap
CN111205943A (en) * 2020-02-27 2020-05-29 广州倾镜生物科技有限公司 Preparation method of efficient mite-killing handmade soap and efficient mite-killing handmade soap

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5529714A (en) * 1993-10-25 1996-06-25 Avon Products Inc. Transparent soap formulations and methods of making same
CN101245293A (en) * 2008-03-18 2008-08-20 湖南丽臣实业有限责任公司 Household soap and preparing technique thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5529714A (en) * 1993-10-25 1996-06-25 Avon Products Inc. Transparent soap formulations and methods of making same
CN101245293A (en) * 2008-03-18 2008-08-20 湖南丽臣实业有限责任公司 Household soap and preparing technique thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李俊博: "半透明皂的透明度影响因素及其工艺过程控制", 《日用化学工业》 *

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013715A (en) * 2012-12-20 2013-04-03 广东鹏锦实业有限公司 Transparent soap
CN103013715B (en) * 2012-12-20 2015-04-22 广东鹏锦实业有限公司 Transparent soap
CN104250593A (en) * 2013-06-28 2014-12-31 蔡佐良 Light-transmitting soap base and light-transmitting flower soap body prepared by applying same
CN105886171A (en) * 2016-04-18 2016-08-24 广西南宁皂和奇迹科技有限公司 Transparent soap and preparation method thereof
CN109666545A (en) * 2018-12-28 2019-04-23 中山市天图精细化工有限公司 A kind of efficient cleaning toilet foam aerosol and preparation method thereof
CN109666545B (en) * 2018-12-28 2020-10-02 中山市天图精细化工有限公司 Efficient toilet cleaning foam aerosol and preparation method thereof
CN110257199A (en) * 2019-08-01 2019-09-20 广州倾镜生物科技有限公司 A kind of handmade soap soap base formula and preparation method thereof
CN110564529A (en) * 2019-09-19 2019-12-13 广州倾镜生物科技有限公司 preparation method of handmade soap base and handmade soap base
CN110846158A (en) * 2019-11-28 2020-02-28 安徽倾镜生物科技有限公司 Preparation method of amino acid soap and amino acid soap
CN111205943A (en) * 2020-02-27 2020-05-29 广州倾镜生物科技有限公司 Preparation method of efficient mite-killing handmade soap and efficient mite-killing handmade soap

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