CN101554248B - Method for improving quality of tobacco shreds by storing tobacco shreds in oak barrel - Google Patents

Method for improving quality of tobacco shreds by storing tobacco shreds in oak barrel Download PDF

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CN101554248B
CN101554248B CN2008100472859A CN200810047285A CN101554248B CN 101554248 B CN101554248 B CN 101554248B CN 2008100472859 A CN2008100472859 A CN 2008100472859A CN 200810047285 A CN200810047285 A CN 200810047285A CN 101554248 B CN101554248 B CN 101554248B
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oak
oak barrel
tobacco
pipe tobacco
tobacco shreds
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CN101554248A (en
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王建新
叶明樵
张耀华
程占刚
吴凯
闫爱华
胡素霞
丁碧军
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Abstract

The invention discloses a method for improving the quality of tobacco shreds by storing the tobacco shreds in an oak barrel, belonging to the technical field of cigarettes. The method comprises the following steps: the formulation tobacco shreds are positioned in the oak barrel with a volume of 5-1000L; the oak barrel is positioned in a shady and dry room with the indoor temperature kept at 20-30 DEG C and the indoor humidity kept 50-70 percent; the tobacco shreds are taken out after being stored for 15-30 days so that the tobacco shreds can be improved in the taste quality. In the first two days of the storage, one side of a cover of the oak barrel is raised by 1cm so that gas can flow out between the cover and the inner wall of the barrel body; and since the third day, the cover and the barrel body are absolutely sealed. The oak barrel is made of moderately baked oak and is shaped to be similar to a Burgundy model, and the oak is Quercus robur grown in Changbai Mountain of China. Themethod is unique, utilizes the oak barrel to alcoholize the tobacco shreds, can be used both for laboratory tobacco shred alcoholization and production, organically combines the original aromas of th e oak barrel and the tobacco shreds and further improves the quality of the tobacco shreds.

Description

Store the method that pipe tobacco improves tobacco quality with oak barrel
Technical field
The invention belongs to technical field of cigarettes, be specifically related to the further processing method that cuts filler behind the flavoring and casing.
Background technology
Mostly existing pipe tobacco alcoholization mode for being irony wire-storing cabinet natural alcoholization, and the fragrance style of pipe tobacco controlled by pipe tobacco one's own department or unit fragrance, technological parameter and perfume (or spice), sugar material, and the fragrance style of product is mainly determined by tobacco leaf formulation and essence and flavoring agent.The applicant recognizes that the processes process also can be stabilized and increased product quality, product style is consolidated, but do not had the people to carry out significant work in this respect as yet.
Summary of the invention
Above-mentioned deficiency to prior art; The technical problem that the present invention will solve provides a kind of method of storing pipe tobacco raising tobacco quality with oak barrel; After it makes oak and pipe tobacco combines; Main component in the oak is diffused in the pipe tobacco, organically combines and make it alcoholization with the pipe tobacco aroma component, thereby brings the distinctive suction flavor of pipe tobacco style.
Technical scheme of the present invention is: using oak barrel to store method that pipe tobacco improves tobacco quality is that cutting filler of flavoring and casing put into volume is 5～1000 liters oak barrel; Place the indoor of shady and cool drying; Keep 20-30 ℃ of indoor temperature; Humidity 50-70% stores and takes out after 15-30 days, is used to improve the smoking quality of pipe tobacco.The beginning of said storage two days is raised 1cm with a side of the bung of oak barrel, so that let gas between bung and ladle body inwall, overflow, from the 3rd day bung and ladle body is sealed fully.Described oak barrel adopts the oak of moderate baking to make.The shape of described oak barrel adopts the oak of Bourgogne type shape to disclose.Described oak barrel adopts the summer oak on Chinese Changbai Mountain to make.
Method of the present invention is off the beaten track, utilizes oak barrel alcoholization pipe tobacco, both can be used to test the alcoholization of pipe tobacco, can be used for again producing, and this perfume of oak barrel and this perfume of pipe tobacco are organically combined, and further improves quality of tobacco shreds.
The specific embodiment
Be described in further detail with regard to the specific embodiment of the present invention and relevant technologies problem below.Through the applicant's research, find that the oak main component has 4 types of materials to produce facilitation to the alcoholization of tobacco, and carried out great deal of experimental.These 4 types of materials: 1 tannin: have better antioxidation, and have oak fragrance, comprising: woody flavour, sootiness and little spice flavor, this fragrance can be coordinated with cigarette is fragrant preferably, improves the fragrant quality of cigarette.2 Oak Lactones: have the smell of coconut and fresh wood, it has represented the most of fragrant potentiality of fresh wood, can produce acidic materials on the one hand; The alkalescence that suppresses flue gas neutral and alkali material; Make the acid-base balance appropriateness of flue gas, reduce excitant, produce gratifying jealous; On the other hand, prop up in the process of burning and sucking at cigarette, pyrolysis forms multiple aroma substance separately.3 glucides: comprise uronic acid, galactolipin, pentose, methylpentose etc., can increase cigarette fragrant big and fleshy sense and mouthfeel.4 other volatile fragrant components: mainly comprise vanillic aldehyde, syringaldehyde, furans materials (like furfural, furans alcohol) etc. can enrich cigarette perfume (or spice), increase the complexity of fragrance.
The characteristics of technical scheme of the present invention are: store pipe tobacco with oak barrel and can quicken the pipe tobacco alcoholization.The pipe tobacco that in oak barrel, refined has the intrinsic characteristics of pipe tobacco, fragrance, simultaneously through smell of oak own and the experiment of pipe tobacco fragrance harmony; Form unique processing process; Finally make pipe tobacco fragrance more plentiful, pure and mild, outstanding its exclusive suction flavor style makes the consumer more satisfied.Because oak itself contains " tannic acid ", but impurity screening makes pipe tobacco strong more naturally.Pipe tobacco can produce carbon dioxide in carrying out the alcoholization process, so just began 2 days what refine, can the bung of oak barrel not covered completely, leave certain gap so that let gas overflow; Again the bung of oak barrel is sealed fully after 2 days, place shady and cool dry indoor, temperature 20-30 ℃, store under the humidity 50-70% condition, total period of storage is 15-20 days.Because oak barrel itself also can absorb the organic substance in the pipe tobacco, thus make container become vacuum state gradually, and oxygen can see through the pore of oak and get into this moment, sees through this little slow oxidation and can further help the pipe tobacco alcoholization.
Embodiment 1
In the oak barrel of 100L, store the pipe tobacco prescription A of flavoring and casing, preceding 2 days, cover oak bung (not exclusively sealing), the bung with oak barrel seals fully then, places the indoor of shady and cool drying, 30 ℃ of temperature, humidity 70% was stored 20 days altogether.Take out pipe tobacco then and make cigarette.Smoke panel test with the pipe tobacco prescription A contrast of the flavoring and casing of natural alcoholization, and detect tar.Like table 1 and table 2.
Table 1, the oak barrel alcoholization of prescription A pipe tobacco and natural alcoholization contrast
The alcoholization type Sensory quality assessment
Natural alcoholization Blue foreign smell appears, and harmony is slightly poor, and the nasal cavity excitant has, and the oral cavity has slight residual
The oak barrel alcoholization Fragrance is plentiful, and harmony is better, and nasal cavity slightly stimulates, and pleasant impression is more comfortable
Table 2, the oak barrel alcoholization of prescription A pipe tobacco and natural alcoholization flue gas analysis contrast
Cigarette weight (g) Cigarette props up resistance to suction (H 2O) Puff number (mouth) Tar (mg) Nicotine (mg) CO (mg)
Natural alcoholization 0.92 1270 8.2 14.94 1.29 13.94
The oak barrel alcoholization 0.92 1210 8.2 15.00 1.30 14.81
By last 2 tables show that method of the present invention can improve the cigarette odor-absorbing endoplasm, but fume indication is not had big variation.
Embodiment 2
In the oak barrel of 1000L, store the pipe tobacco prescription B of flavoring and casing, place the indoor of shady and cool drying, 28 ℃ of temperature; Humidity 60% preceding 2 days, covers the gap that oak bung one of which side leaves 1cm; Bung with oak barrel seals fully two days later, stores altogether 20 days.Take out pipe tobacco then and make cigarette.Smoke panel test with pipe tobacco (flavoring and casing) contrast of natural alcoholization, and detect tar.Like table 3 and table 4.
Table 3 prescription B pipe tobacco oak barrel alcoholization and natural alcoholization contrast
The alcoholization type Sensory quality assessment
Natural alcoholization The soft exquisiteness of flue gas, it is slightly poor that fragrance passes through the property sent out, and conglobation property is better, the slightly sweet rhythm sense of flue gas
The oak barrel alcoholization The abundant sense of fragrance increases, and flue gas is fine and smooth, and conglobation property is good, and pleasant impression is comfortable
Table 4 prescription B pipe tobacco oak barrel alcoholization and natural alcoholization flue gas analysis contrast
Cigarette weight (g) Cigarette props up resistance to suction (H 2O) Puff number (mouth) Tar (mg) Nicotine (mg) CO (mg)
The oak barrel alcoholization 0.92 1200 8.0 14.06 1.25 13.69
Natural alcoholization 0.92 1240 8.2 14.46 1.42 16.48
Data declaration in the table, utilize oak barrel to store pipe tobacco after, the cigarette smoke index not have to influence basically, and that mouthfeel becomes relatively is comfortable, fragrance is soft, conglobation property is good.
The applicant has also carried out various tests and research to the time that cigarette shreds is stored, and finds that the resting period of pipe tobacco is better with 15-20 days, can make the pipe tobacco aesthetic quality basicly stable.
Table 5, the period of storage table of comparisons
Resting period (my god) Estimate
3 Pipe tobacco has had significantly timber breath near the bucket wall, but core do not have, and whole sense organ mass change is not obvious when smokeing panel test
6 Pipe tobacco has had tangible timber breath near the bucket wall, and the slightly timber breath of core pipe tobacco can be realized fragrance and become slightly abundant when smokeing panel test
9 Whole pipe tobacco has had significantly and the mixed breath of timber, smokes panel test and thinks that flue gas is more abundant, and aromatic shows slightly sinking
12 Whole pipe tobacco has had significantly and the mixed breath of timber, smokes panel test and thinks that flue gas is more mellow, and aromatic shows slightly sinking, and the spine sense slightly increases
15 Whole pipe tobacco has had the breath that significantly mixes with timber, smokes panel test and thinks that flue gas is mellow, and aromatic sinks, and the spine sense slightly increases
18 Whole pipe tobacco has had the breath that significantly mixes with timber, and for flue gas is mellow, aromatic sinks, and the spine sense slightly increases, and mass change is basicly stable
21 No significant change, whole pipe tobacco have had the breath that significantly mixes with timber, and for flue gas is mellow, aromatic sinks, and mass change is basicly stable
The purpose of storing pipe tobacco with oak barrel is to let pipe tobacco fully draw the elite of oak and gives pipe tobacco oxidation to a certain degree.The weight that pipe tobacco draws kind and the quantity and the degree of oxidation of material directly affects the sense organ of pipe tobacco, and this largely all depends on selected oak kind.The applicant through experiment selected the oak on Chinese Changbai Mountain.The special geographical position and the weather on Changbai Mountain have bred the high-quality oak, for the production of oak barrel provides prerequisite.Here with coexist about 45 ℃ of north latitude of French oak producing region, 611.5 meters of mean sea levels, pitchy soil; The continental monsoon climate in north temperate zone, 2000-3000 ℃ of year accumulated temperature, annual precipitation 750-1000mm; About 140 days frost-free periods, chief species are needlebush and leaf wood mixed forest.Therefore the Changbai Mountain oak has all advantages of French oak.The general fragrance of summer oak on China Changbai Mountain is more quiet and tastefully laid out careful, and volatile flavor and phenolic compound in it have equalization point preferably; Smell of timber own and pipe tobacco fragrance are coordinated, finally made pipe tobacco fragrance more plentiful, pure and mild.
Embodiment 3, and for this reason, we roll cigarette and prop up after adopting pipe tobacco prescription C to put into the wooden barrel storage, estimate, like table 6
The wooden barrel of table 6 unlike material is to pipe tobacco prescription C aesthetic quality's influence
Material Estimate
White oak Fragrance is abundant, and it is dull that fragrance shows slightly
The Sicily rubber Fragrance is inharmonious, and is outer fragrant overweight
The summer oak on Changbai Mountain Flue gas is mellow, and aromatic sinks
The specification and the model of oak barrel are a lot.Barrel shape has that bohr is many types of, Bourgogne type, sherry type or the like, capacity then have 30 liters, 100 liters, 225 liters, 228 liters, 300 liters, 500 liters, even a few kilolitre does not wait.Mainly need consider two factors when selecting the oak barrel model: the one, the convenience of operation; The 2nd, inner ratio surface area.Through a large amount of experiments, the applicant adopts the oak of the Bourgogne type shape of different size to disclose.This oak barrel not only has suitable surface area volumetric ratio, and move operation and cleaning etc. are all very convenient.
It is in order to draw the active ingredients such as aromatic substance tannic acid in the oak that pipe tobacco is stored in oak barrel.The extractible active ingredient of different oak barrel is different, and this depends primarily on the technology of " training is roasting " in the oak barrel manufacture craft.If the roasting degree of training is different, even oak kind, model are consistent, the local flavor of storing the pipe tobacco of the same race that comes out also has than big-difference.Through a large amount of experiments, the applicant adopts through the roasting oak barrel of moderate training, and this technology can give pipe tobacco more strong fragrant, more pleasant fragrance, and is also soft more full through the pipe tobacco mouthfeel of its alcoholization.
Embodiment 4, and for this reason, we roll cigarette and prop up after adopting pipe tobacco prescription D to put into the wooden barrel storage, estimate, like table 7.
Table 7, different oak are stored the contrast of pipe tobacco prescription D
Process condition Evaluation result
Slight baking Advantage: the abundant sense of fragrance increases, and harmony is better, the continuous alcohol of flue gas, and do not have and obviously expose the breath shortcoming: this perfume (or spice) of tobacco is slightly covered, excitant slightly increases
The moderate baking Advantage: the abundant sense of fragrance increases, and flue gas is pureer and milder, shortcoming: this perfume of tobacco and oak composition are coordinated, and excitant is little.
The severe baking Advantage: the simple and honest shortcoming of flue gas: fragrance becomes flat, and this perfume (or spice) of tobacco is covered obviously, and harmony is relatively poor, the flue gas roughening, and it is obvious to expose breath, and it is residual more obvious that excitant increases lingual surface.
The applicant also wooden barrel is stored tobacco sample and common tobacco sample flavor matter content compares, and comparative result is seen table 8.
The flavor matter content (microgram) of common tobacco sample of table 8. and wooden barrel alcoholization tobacco sample
Flavor matter Common pipe tobacco The wooden barrel pipe tobacco
Pyridine 0.04 0.27
3-amylene-2-ketone 0.00 0.01
Hexanal 0.00 0.10
Dihydro-2-methyl-3 (2H)-furanone 1.14 1.75
2-furans menthol 8.82 13.01
Furfural 15.78 21.80
5-methyl-2-furfural 0.87 1.64
Benzaldehyde 0.03 0.23
Phenmethylol 3.59 10.43
Phenylacetaldehyde 6.76 7.11
Linalool 0.81 0.76
Benzyl carbinol 3.31 4.63
Solanone 0.28 0.56
6-first-5-hepten-2-one 0.43 0.31
Isophorone 0.19 0.21
The 2-dorinone 15.65 23.76
Geranyl acetone 4.19 4.69
Dihydroactinidiolide 11.85 13.26
Megastigmatrienone 63.02 67.44
3-hydroxy-beta-damascenone 20.33 22.00
3-oxo-ionol 8.37 12.25
Farnesyl acetone 12.23 15.60
Tetradecylic acid 2.95 6.50
Hexadecylic acid 195.13 241.30
The 2-pentenals 0.00 0.09
3-methyl-2-butene aldehyde 0.00 0.08
2-methyl-2-pentenals 0.00 0.03
2, the 4-sorbic aldehyde 0.08 0.09
2-cyclopentene-1, the 4-diketone 3.51 7.07
Neophytadiene 844.57 705.60
Brown reaction product 26.66 38.58
The phenylalanine class 14.50 23.15
The carotenoid catabolite 136.24 159.52
Organic acid 198.09 247.79
Total amount (removing neophytadiene) 375.48 469.04
From table 7, can find out, the flavor matter except that neophytadiene, sample of the present invention all is higher than common tobacco sample; The flavor matter of some small-molecular weights particularly, 3-amylene-2-ketone, hexanal, 2-pentenals, 3-methyl-2-butene aldehyde, 2-methyl-2-pentenals do not detect in common tobacco sample; But content has reached detection line in wooden barrel alcoholization tobacco sample; Explanation is in wooden barrel alcoholization process, and macromolecular substances obtains degraded, has produced micromolecular flavor matter.The content of the western cypress alkanes material solanone of class in wooden barrel alcoholization sample has increased by one times than common tobacco sample.Important carotenoid catabolite content showed increased in sample such as damascenone, geranyl acetone, dihydroactinidiolide, Megastigmatrienone, farnesyl acetone.Wooden barrel alcoholization tobacco sample obviously reduces than common sample neophytadiene content.Neophytadiene content in tobacco leaf is the highest, and neophytadiene content reduces in the alcoholization process, changes into low molecular weight substance, can improve the quality of tobacco leaf.

Claims (5)

1. store the method that pipe tobacco improves tobacco quality with oak barrel for one kind; It is characterized in that: will be flavoring and casing cut filler that to put into volume be 5～1000 liters oak barrel; Place the indoor of shady and cool drying, keep 20-30 ℃ of indoor temperature, humidity 50-70%; Store and take out after 15-30 days, be used to improve the smoking quality of pipe tobacco.
2. method of storing pipe tobacco raising tobacco quality with oak barrel according to claim 1; It is characterized in that: the beginning of said storage two days; One side of the bung of oak barrel is raised 1cm; So that let gas between bung and ladle body inwall, overflow, bung and ladle body sealed fully from the 3rd day.
3. method of storing pipe tobacco raising tobacco quality with oak barrel according to claim 1 is characterized in that: described oak barrel adopts the oak of moderate baking to make.
4. method of storing pipe tobacco raising tobacco quality with oak barrel according to claim 1 is characterized in that: the shape of described oak barrel adopts the oak of Bourgogne type shape to disclose.
5. method of storing pipe tobacco raising tobacco quality with oak barrel according to claim 1 is characterized in that: described oak barrel adopts the summer oak on Chinese Changbai Mountain to make.
CN2008100472859A 2008-04-09 2008-04-09 Method for improving quality of tobacco shreds by storing tobacco shreds in oak barrel Active CN101554248B (en)

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CN102556564A (en) * 2011-12-20 2012-07-11 红云红河烟草(集团)有限责任公司 Flexible tobacco shred storage and distribution method
CN103110181A (en) * 2013-02-22 2013-05-22 川渝中烟工业有限责任公司 Barrel-type fermentation method for cigar tobacco leaves
CN103445289A (en) * 2013-08-30 2013-12-18 湖北中烟工业有限责任公司 Cigar alcoholization method
CN105950420A (en) * 2016-06-27 2016-09-21 四川理工学院 Method for enhancing vinosity by storing white wine in oak barrels
CN105907591A (en) * 2016-06-27 2016-08-31 泸州白酒庄园酿酒有限责任公司 Method for improving liquor quality by storing strength-flavor type white wine with oak barrel
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CN105936865A (en) * 2016-06-27 2016-09-14 泸州白酒庄园酿酒有限责任公司 Method using oak barrels to store Fen flavor liquor so as to improve quality of liquor
CN111103322B (en) * 2018-10-29 2023-02-28 贵州中烟工业有限责任公司 Tobacco mellowing determination method and tobacco mellowing determination device
KR102413848B1 (en) * 2020-02-21 2022-06-27 주식회사 케이티앤지 Aging method of smoking material using oak barrels and a smoking article manufactured by the same
CN111567840B (en) * 2020-04-23 2022-03-18 红云红河烟草(集团)有限责任公司 Scenting process for improving smoking quality of tobacco products

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CN2511147Y (en) * 2001-11-08 2002-09-18 车英勋 Tobacco adjustor
CN101058784A (en) * 2007-05-31 2007-10-24 中国长城葡萄酒有限公司 Dry red wine oak barrel fermentation process

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Publication number Priority date Publication date Assignee Title
CN1149622A (en) * 1995-10-28 1997-05-14 孙天星 Technology for producing brandy dried liquor
CN2511147Y (en) * 2001-11-08 2002-09-18 车英勋 Tobacco adjustor
CN101058784A (en) * 2007-05-31 2007-10-24 中国长城葡萄酒有限公司 Dry red wine oak barrel fermentation process

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