CN101508940A - High-efficiency disinfection washing powder - Google Patents
High-efficiency disinfection washing powder Download PDFInfo
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- CN101508940A CN101508940A CNA2008101017714A CN200810101771A CN101508940A CN 101508940 A CN101508940 A CN 101508940A CN A2008101017714 A CNA2008101017714 A CN A2008101017714A CN 200810101771 A CN200810101771 A CN 200810101771A CN 101508940 A CN101508940 A CN 101508940A
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- washing powder
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- powder
- sterilant
- active agent
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Abstract
The invention discloses an efficient sterilizing washing-powder, belonging to the field of hygienic product. The invention aims at providing an efficient and safe product which is processed by modern biotechnology. The formulation of the invention comprises surface active agent, bactericide, thickening agent, essence, etc. The washing-powder has the advantages of simple technique, low cost, strong sterilizing power, safety, low price and high technology content. The bactericide which is processed by pure natural fermentation material through modern biotechnology and added in the washing-powder has the function of anticorrosion and the characteristics of being safe and efficient.
Description
Technical field:
The invention belongs to field of hygiene products, relate to special washing powder.
Background technology:
Washing powder is indispensable daily necessities in people's daily life.At present, the washing powder of selling on the market is normally by several tensio-active agents, and the adding washing assistant processes.This class washing powder has only the effect of washing usually, can not the bacterium on the clothing effectively be killed.At present, locate in family, hotel, railway, airport, school etc., washing machine has obtained using widely.If the easy breed bacteria of washing machine not to its disinfection, then causes people's infection easily, and people's health is brought threat.
On the market, some have also occurred and had the washing powder of disinfecting and sterilizing functions.Mainly be to have added some sterilizing agents and Chinese medicinal materials etc., make washing powder have certain germicidal efficacy.These sterilizing agents, some is not really safe to people, if rinsing is unclean, people's skin is had certain stimulation.Some sterilizing agent costs an arm and a leg, and is unfavorable for reducing production costs and increasing competitiveness of product.At present, it is strong to be starved of a kind of soil removability on the market, and sterilizing power is strong, safety, cheap washing powder.
At present, the disinfectant sterilization washing powder great majority of selling on the market are to have added chemical bactericide.In the market, having the washing soap of sterilizing function, mainly is to have the characteristic of killing common intestinal bacteria, Salmonellas and streptococcus aureus.
Summary of the invention:
The purpose of this invention is to provide a kind of highly effective and safe, adopt the bactericidal washing powder product of modern biotechnology product processing.
Component of the present invention comprises tensio-active agent, washing assistant, additive, spices, enzyme, sterilant.
The weight percent of each component is in the high-efficiency disinfection washing powder: tensio-active agent 20～40%, washing assistant 48～60%, additive 0.1～2%, zymin 0.5～5%, sterilant 0.1～2%, spices 0.0001～0.001%.
Described tensio-active agent mainly comprises the anion surfactant that present washing powder is commonly used and the tensio-active agent of non-ionic type.Comprise sodium laurylsulfonate and polyoxyethylenated alcohol sodium sulfate etc.
Washing assistant mainly contains washing assistant commonly used such as yellow soda ash, water glass, zeolite.
Additive is mainly sodium cellulose glycolate.
Enzyme addn such as low-temperature lipase, Sumizyme MP is the enzyme preparation product of producing by modern biotechnology, and kind is more at present, can live according to the characteristic of the variant production of each different company and enzyme and select the rational amount of adding.
Major technique feature of the present invention be added have inexpensive, highly effective and safe, the sterilant through modern biotechnology processing of All Pure Nature.The used sterilant of the present invention is the inventor's an invention achievement.Sterilant is subtilis LD-8 (Bacillus subtilis LD-8) fermentation broth extract, culture presevation is in China Microbial Culture Preservation Commission common micro-organisms center, Datun Road, Chaoyang District, Beijing City, preservation address, preservation date on December 18th, 2007, culture presevation numbering CGMCC 2294.
Fungus characteristic is as follows:
1. somatic cells is life or the living Gram-positive of near-end in direct rod shape, the gemma.
2. colony characteristics is that white is circular, protuberance, and smooth surface, opaque, moistening, provoke adhesion.
3. can utilize various saccharides, as glucose, semi-lactosi, wood sugar, cellobiose, raffinose etc.; Produce amylase, proteolytic enzyme, can gelatin hydrolysate, V.P, the methyl red positive.
4. 37 ℃ of the suitableeest culture temperature, optimal pH 7.0.
This bacterium classification status is as follows: bacterium territory (Bacteria); Firmicutes (Firmicutes); Genus bacillus guiding principle (Bacillales); Genus bacillus order (Bacillaceae); Bacillaceae (Bacillus); Bacillus (Bacillus); Bacillus subtilis bacterial classification (Bacillus subtilis).
The preparation method of fermentation broth extract is as follows among the present invention:
The seed culture medium of bacterial strain is a broth culture, extractum carnis 3g wherein, peptone 10g, NaCl 5g, water 1000ml, pH value 7.0～7.2, high pressure steam sterilization.
The seed liquor culture condition: culture temperature is 37 ℃, and shaking speed is 140 rev/mins, and fermentation time is 10～14 hours.
Inoculum size is 6%～10% o'clock, helps the formation of antibacterial substance.
The fermention medium of optimizing consists of: sucrose 0.3%, and peptone 1%, NaCl 0.5%, MgSO
47H
2O 0.7%, KH
2PO
40.7%, pH8.0.
The fermentation culture conditions of optimizing is: culture temperature is 37 ℃, and shaking speed is 140 rev/mins, and fermentation time is about 24 hours.
Extracting the antibacterial substance method from fermented liquid is organic solvent precipitation method.The available organic solvent is acetone, methyl alcohol, ethanol.
At first with fermented liquid, add supercentrifuge, temperature 0-4 ℃, rotating speed is 10000 rev/mins, centrifugal ten minutes, remove precipitation, and keep supernatant liquor.
With the supernatant that obtains, add isopyknic methyl alcohol, the temperature of system is reduced to-5 ℃ rapidly, preserved 2 hours for-5 ℃.Collect organic phase, adopt vacuum distillation method to remove organic solvent.Distillation temperature 30-60 ℃, distilled 20 minutes, organic solvent is removed.The collecting precipitation material.This promptly is the crude extract of our bacteriocidal substance that obtains.
The crude extract of bacteriocidal substance, after water dissolution, concentration is 1% (mass volume ratio).Lysate can kill common pathogenic bacterium effectively.For example not only can kill intestinal bacteria effectively, Salmonellas, the pathogenic micro-organism that golden yellow common coccus etc. are common, and can kill the common coccus of methicillin-resistant staphylococcus.
This disinfecting liquid has high security, in the emergency toxicology experiment, we gavage 5 groups of 200 mouse with this disinfecting liquid, and the mouse of experimental group none occur dead, and subtilis is present in occurring in nature widely, and many important industrial bacterial strains are exactly subtilis.Substantially can conclude that this disinfecting liquid is safe for the user, can relievedly use.After adding it to washing powder, find that it still has good fungicidal activity.
Method for making of the present invention is simple.With tensio-active agent, washing assistant, additive waits raw material to make the washing powder particle according to technologies such as the pressurization of aftertreatment, the slip of batching, slip, spraying drying, screenings, adds zymin, sterilant, spices then and mixes and get final product.
Beneficial effect:
The present invention realized that not only washing powder removes the function of dirt, and washability is outstanding, and strong detergency is easy to use, has especially possessed good sterilization and disinfectant function, particularly can kill the characteristic of methicillin-resistant staphylococcus aureus.The emergency toxicology experiment has also verified the sterilant that adds in this washing powder people and animals to be had very high security.Scientist has found methicillin-resistant staphylococcus aureus in 1961, find that at present it spreads all over the world, and becomes important infectious bacteria, has brought great threat for people's health.The production of the sterilant that adds in the washing powder utilizes fermentation raw material with low cost, adopts modern biotechnology, and technology is simple, and is with low cost.Make the present invention, it is outstanding to become a kind of washability, and sterilizing power is strong, safety, cheapness, washing powder with high content of technology.
That adds among the present invention has the rot-resistant function by the pure natural fermentation raw material through the sterilant that modern biotechnology processes, and has characteristics safely and efficiently.Need not to add again sanitas in the washing powder.
Specific embodiment:
The invention will be further described below in conjunction with specific embodiment, but be not limited to embodiment.
Select sodium laurylsulfonate 180kg, polyoxyethylenated alcohol sodium sulfate 120kg, yellow soda ash 150kg, water glass 150kg, zeolite 200kg, sodium cellulose glycolate 7kg, the 0.5kg rose compound adds agitator, the preliminary mixing, add the 500L deionized water, be controlled at 60 ℃ with agitator is stable, mixing speed is unsuitable too high, can be controlled in 20～30 rev/mins; After treating basic dissolving, remove by filter insoluble particle; The feed liquid of having filtered is outgased, adopt vacuum outgas, negative pressure can be controlled in 5Mpa, removes the bubble that forms in the stirring and dissolving process, reduces the air content of material; After the degassing is finished, grind, grind and adopt colloidal mill, colloidal mill gets abrasive disk space and is controlled at 2mm, and speed of grinding plate is 500 rev/mins, and material can be more even after grinding, and stops up spray gun when preventing spraying drying; Will be through grinding the material of mixing, with the high-pressure pump high-pressure fog tower of making a gift to someone, spray tower adopts swirl atomizer, and it is 8Mpa that nozzle bore can adopt the 2mm input pressure, and temperature is controlled at 90 ℃ in the tower, and the cat head negative pressure is controlled at 10～20Pa, and feed liquid forms dry powder in tower; Washing powder draws off at the bottom of tower, and temperature is about 60～80 ℃, after wearing out through lowering the temperature, just can carry out the back batching; With the 2.5kg sterilant, add Sumizyme MP (Savinase 8.0, Novo company), amylase (Termamyl, Novo company), alkaline low-temperature lipase (Lipolase, Novo) each 10kg joins in the washing powder, carries out mixing and can obtain high-efficiency disinfection washing powder.
Get 5% concentration product of the present invention, adopt conventional microorganism detection sterilization effect, test-results shows that product sterilization effect of the present invention reaches more than 90%, and sterilization effect is obvious.Microorganism is selected intestinal bacteria, Salmonellas, golden yellow common coccus.
Claims (4)
1. a high-efficiency disinfection washing powder comprises tensio-active agent, washing assistant, additive and enzyme composition, it is characterized in that containing sterilant, and described sterilant is the fermentation broth extract of subtilis CGMCC 2294.
2. according to the described high-efficiency disinfection washing powder of claim 1, it is characterized in that each weight percentages of components is in the described washing powder: tensio-active agent 20～40%, washing assistant 48～60%, additive 0.1～2%, zymin 0.5～5%, sterilant 0.1～2%, spices 0.0001～0.001%.
3. according to the described high-efficiency disinfection washing powder of claim 1, it is characterized in that described tensio-active agent is at least a in sodium laurylsulfonate or the polyoxyethylenated alcohol sodium sulfate.
4. according to the described high-efficiency disinfection washing powder of claim 1, it is characterized in that described washing assistant is at least a in yellow soda ash, water glass or the zeolite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101017714A CN101508940B (en) | 2008-03-12 | 2008-03-12 | High-efficiency disinfection washing powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101017714A CN101508940B (en) | 2008-03-12 | 2008-03-12 | High-efficiency disinfection washing powder |
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| Publication Number | Publication Date |
|---|---|
| CN101508940A true CN101508940A (en) | 2009-08-19 |
| CN101508940B CN101508940B (en) | 2011-03-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008101017714A Active CN101508940B (en) | 2008-03-12 | 2008-03-12 | High-efficiency disinfection washing powder |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102994242A (en) * | 2012-11-26 | 2013-03-27 | 广州市浪奇实业股份有限公司 | Hyperconcentration detergent powder |
| CN107083285A (en) * | 2017-03-07 | 2017-08-22 | 杭州诺诚洗涤科技有限公司 | The washing process of green non-pollution hotel towel |
| CN107287051A (en) * | 2017-07-31 | 2017-10-24 | 王瑜琳 | A kind of high-efficiency disinfection washing powder and preparation method thereof |
| CN108034521A (en) * | 2017-12-29 | 2018-05-15 | 广州慈康生物科技有限公司 | A kind of concentration liquid detergent with long-acting bacteriostatic |
| CN110885715A (en) * | 2018-09-07 | 2020-03-17 | 深圳市环保洁贸易有限公司 | Novel biological environment-friendly cleaning solution and preparation method thereof |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103146498A (en) * | 2012-07-14 | 2013-06-12 | 邵素英 | Washing powder |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85100011B (en) * | 1985-04-01 | 1988-08-10 | 张书林 | Production and use of insectofungicidal detergent |
-
2008
- 2008-03-12 CN CN2008101017714A patent/CN101508940B/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102994242A (en) * | 2012-11-26 | 2013-03-27 | 广州市浪奇实业股份有限公司 | Hyperconcentration detergent powder |
| CN102994242B (en) * | 2012-11-26 | 2015-07-08 | 广州市浪奇实业股份有限公司 | Hyperconcentration detergent powder |
| CN107083285A (en) * | 2017-03-07 | 2017-08-22 | 杭州诺诚洗涤科技有限公司 | The washing process of green non-pollution hotel towel |
| CN107287051A (en) * | 2017-07-31 | 2017-10-24 | 王瑜琳 | A kind of high-efficiency disinfection washing powder and preparation method thereof |
| CN108034521A (en) * | 2017-12-29 | 2018-05-15 | 广州慈康生物科技有限公司 | A kind of concentration liquid detergent with long-acting bacteriostatic |
| CN110885715A (en) * | 2018-09-07 | 2020-03-17 | 深圳市环保洁贸易有限公司 | Novel biological environment-friendly cleaning solution and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101508940B (en) | 2011-03-16 |
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Effective date of registration: 20200407 Address after: 053000 workshop of Hengshui Shangde Fuel Cell Technology Co., Ltd., Taocheng high tech Zone, Taocheng District, Hengshui City, Hebei Province Patentee after: Shengyi Hengshui Daily Chemical Co., Ltd Address before: 101121, 1 Cui Lu, Liyuan, Tongzhou District, Beijing, Zhenjiang Patentee before: BEIJING LVDAOYUAN BEE PRODUCT Co.,Ltd. |