CN101507436B - 含精喹禾灵、氟磺胺草醚和广灭灵的除草组合剂型及其制备方法 - Google Patents
含精喹禾灵、氟磺胺草醚和广灭灵的除草组合剂型及其制备方法 Download PDFInfo
- Publication number
- CN101507436B CN101507436B CN2009101317982A CN200910131798A CN101507436B CN 101507436 B CN101507436 B CN 101507436B CN 2009101317982 A CN2009101317982 A CN 2009101317982A CN 200910131798 A CN200910131798 A CN 200910131798A CN 101507436 B CN101507436 B CN 101507436B
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- CN
- China
- Prior art keywords
- fomesafen
- ethyl
- clomazone
- quizalotop
- vegetable oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- BGZZWXTVIYUUEY-UHFFFAOYSA-N fomesafen Chemical compound C1=C([N+]([O-])=O)C(C(=O)NS(=O)(=O)C)=CC(OC=2C(=CC(=CC=2)C(F)(F)F)Cl)=C1 BGZZWXTVIYUUEY-UHFFFAOYSA-N 0.000 title claims abstract description 43
- 239000005499 Clomazone Substances 0.000 title claims abstract description 33
- KIEDNEWSYUYDSN-UHFFFAOYSA-N clomazone Chemical compound O=C1C(C)(C)CON1CC1=CC=CC=C1Cl KIEDNEWSYUYDSN-UHFFFAOYSA-N 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000005614 Quizalofop-P-ethyl Substances 0.000 title abstract 4
- OSUHJPCHFDQAIT-GFCCVEGCSA-N quizalofop-P-ethyl Chemical group C1=CC(O[C@H](C)C(=O)OCC)=CC=C1OC1=CN=C(C=C(Cl)C=C2)C2=N1 OSUHJPCHFDQAIT-GFCCVEGCSA-N 0.000 title abstract 4
- 239000002131 composite material Substances 0.000 title description 2
- 239000000203 mixture Substances 0.000 claims abstract description 25
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 25
- 239000008158 vegetable oil Substances 0.000 claims abstract description 25
- 150000001412 amines Chemical class 0.000 claims abstract description 17
- 239000002904 solvent Substances 0.000 claims abstract description 16
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000003814 drug Substances 0.000 claims abstract description 12
- -1 amine salts Chemical class 0.000 claims abstract description 9
- 238000009472 formulation Methods 0.000 claims abstract description 9
- 150000003839 salts Chemical class 0.000 claims abstract description 7
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 6
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 23
- 238000009333 weeding Methods 0.000 claims description 16
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000003921 oil Substances 0.000 claims description 9
- 235000019198 oils Nutrition 0.000 claims description 9
- 244000068988 Glycine max Species 0.000 claims description 7
- 235000010469 Glycine max Nutrition 0.000 claims description 7
- 239000003945 anionic surfactant Substances 0.000 claims description 7
- 239000004094 surface-active agent Substances 0.000 claims description 7
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 6
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 claims description 6
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 5
- LVGKNOAMLMIIKO-UHFFFAOYSA-N Elaidinsaeure-aethylester Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC LVGKNOAMLMIIKO-UHFFFAOYSA-N 0.000 claims description 4
- 238000013019 agitation Methods 0.000 claims description 4
- 235000019438 castor oil Nutrition 0.000 claims description 4
- 239000004359 castor oil Substances 0.000 claims description 4
- 229960001777 castor oil Drugs 0.000 claims description 4
- QYDYPVFESGNLHU-UHFFFAOYSA-N elaidic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCC(=O)OC QYDYPVFESGNLHU-UHFFFAOYSA-N 0.000 claims description 4
- LVGKNOAMLMIIKO-QXMHVHEDSA-N ethyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC LVGKNOAMLMIIKO-QXMHVHEDSA-N 0.000 claims description 4
- 229940093471 ethyl oleate Drugs 0.000 claims description 4
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 4
- 239000000944 linseed oil Substances 0.000 claims description 4
- 235000021388 linseed oil Nutrition 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- QYDYPVFESGNLHU-KHPPLWFESA-N methyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC QYDYPVFESGNLHU-KHPPLWFESA-N 0.000 claims description 4
- 229940073769 methyl oleate Drugs 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- OOCMUZJPDXYRFD-UHFFFAOYSA-L calcium;2-dodecylbenzenesulfonate Chemical group [Ca+2].CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O.CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O OOCMUZJPDXYRFD-UHFFFAOYSA-L 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000004495 emulsifiable concentrate Substances 0.000 claims description 2
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 abstract description 10
- 241000196324 Embryophyta Species 0.000 abstract description 9
- 239000000126 substance Substances 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 2
- 229940079593 drug Drugs 0.000 abstract 1
- 229940035429 isobutyl alcohol Drugs 0.000 abstract 1
- 230000002363 herbicidal effect Effects 0.000 description 7
- 239000004009 herbicide Substances 0.000 description 7
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 6
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 4
- 235000019441 ethanol Nutrition 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 244000025254 Cannabis sativa Species 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- YZHUMGUJCQRKBT-UHFFFAOYSA-M sodium chlorate Chemical compound [Na+].[O-]Cl(=O)=O YZHUMGUJCQRKBT-UHFFFAOYSA-M 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 244000047855 Acalypha wilkesiana Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 240000006122 Chenopodium album Species 0.000 description 1
- 235000009344 Chenopodium album Nutrition 0.000 description 1
- 240000001579 Cirsium arvense Species 0.000 description 1
- 235000005918 Cirsium arvense Nutrition 0.000 description 1
- 244000058871 Echinochloa crus-galli Species 0.000 description 1
- 244000025670 Eleusine indica Species 0.000 description 1
- 235000014716 Eleusine indica Nutrition 0.000 description 1
- 241001553700 Euphorbia lathyris Species 0.000 description 1
- 244000292697 Polygonum aviculare Species 0.000 description 1
- 235000006386 Polygonum aviculare Nutrition 0.000 description 1
- 240000003461 Setaria viridis Species 0.000 description 1
- 235000002248 Setaria viridis Nutrition 0.000 description 1
- 235000010086 Setaria viridis var. viridis Nutrition 0.000 description 1
- 244000111146 Sonchus arvensis Species 0.000 description 1
- 235000006731 Sonchus arvensis Nutrition 0.000 description 1
- 241001251949 Xanthium sibiricum Species 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- HCWYXKWQOMTBKY-UHFFFAOYSA-N calcium;dodecyl benzenesulfonate Chemical class [Ca].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 HCWYXKWQOMTBKY-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 125000005909 ethyl alcohol group Chemical group 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- HZAXFHJVJLSVMW-UHFFFAOYSA-N monoethanolamine hydrochloride Natural products NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000010773 plant oil Substances 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 235000005040 sarson Nutrition 0.000 description 1
- 244000128879 sarson Species 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
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CN2009101317982A CN101507436B (zh) | 2009-04-02 | 2009-04-02 | 含精喹禾灵、氟磺胺草醚和广灭灵的除草组合剂型及其制备方法 |
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CN2009101317982A CN101507436B (zh) | 2009-04-02 | 2009-04-02 | 含精喹禾灵、氟磺胺草醚和广灭灵的除草组合剂型及其制备方法 |
Publications (2)
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CN101507436A CN101507436A (zh) | 2009-08-19 |
CN101507436B true CN101507436B (zh) | 2010-07-21 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2509431A (en) * | 2014-03-26 | 2014-07-02 | Rotam Agrochem Int Co Ltd | Herbicidal composition comprises clomazone microcapsules |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2442656A4 (en) * | 2009-06-15 | 2014-04-16 | Accuform Technologies Llc | REDUCED VAPORIZATION COMPOSITIONS AND CORRESPONDING METHODS |
CN103598177A (zh) * | 2013-11-29 | 2014-02-26 | 苏州佳辉化工有限公司 | 一种含苄草丹的环保型除草剂 |
CN110250189A (zh) * | 2019-06-26 | 2019-09-20 | 轩凯生物科技(滁州)有限公司 | 一种含γ-聚谷氨酸的组合型除草剂 |
-
2009
- 2009-04-02 CN CN2009101317982A patent/CN101507436B/zh active Active
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2509431A (en) * | 2014-03-26 | 2014-07-02 | Rotam Agrochem Int Co Ltd | Herbicidal composition comprises clomazone microcapsules |
GB2509431B (en) * | 2014-03-26 | 2016-09-14 | Rotam Agrochem Int Co Ltd | Herbicidal composition, a method for its preparation and the use thereof |
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Publication number | Publication date |
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CN101507436A (zh) | 2009-08-19 |
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C06 | Publication | ||
PB01 | Publication | ||
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SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Weed-control composite containing quizalofop-p-ethyl, fomesafen and clomazone and preparation method thereof Effective date of registration: 20140718 Granted publication date: 20100721 Pledgee: Shandong science and technology finance Company limited by guarantee Pledgor: Jinan Kesai Agrochem Co., Ltd. Registration number: 2014370000006 |
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PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20151118 Granted publication date: 20100721 Pledgee: Shandong science and technology finance Company limited by guarantee Pledgor: Jinan Kesai Agrochem Co., Ltd. Registration number: 2014370000006 |
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PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Weed-control composite containing quizalofop-p-ethyl, fomesafen and clomazone and preparation method thereof Effective date of registration: 20151130 Granted publication date: 20100721 Pledgee: Agricultural capital of Shandong province Company limited by guarantee Pledgor: Jinan Kesai Agrochem Co., Ltd. Registration number: 2015370000060 |
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PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
CP03 | Change of name, title or address |
Address after: 250100 Shandong, Ji'nan, Licheng District, Zhejiang Province Patentee after: Shandong Kesai Agriculture Biotechnology Co. Ltd. Address before: 250100 456, room two, overseas Pioneer Park, 69 Huayang Road, Licheng District, Ji'nan, Shandong. Patentee before: Jinan Kesai Agrochem Co., Ltd. Address after: 250100 Shandong, Ji'nan, Licheng District, Zhejiang Province Patentee after: Shandong Kesai Agriculture Biotechnology Co. Ltd. Address before: 250100 456, room two, overseas Pioneer Park, 69 Huayang Road, Licheng District, Ji'nan, Shandong. Patentee before: Jinan Kesai Agrochem Co., Ltd. |
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CP03 | Change of name, title or address | ||
CI03 | Correction of invention patent |
Correction item: Effective pledgee registered in patent pledge contract Correct: Shandong agricultural financing Company limited by guarantee False: Agricultural capital of Shandong province Company limited by guarantee Number: 51 Volume: 31 |
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CI03 | Correction of invention patent | ||
PM01 | Change of the registration of the contract for pledge of patent right |
Change date: 20181207 Registration number: 2015370000060 Pledgor after: Shandong Kesai Agriculture Biotechnology Co. Ltd. Pledgor before: Jinan Kesai Agrochem Co., Ltd. Change date: 20181207 Registration number: 2015370000060 Pledgor after: Shandong Kesai Agriculture Biotechnology Co. Ltd. Pledgor before: Jinan Kesai Agrochem Co., Ltd. |
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PM01 | Change of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20181218 Granted publication date: 20100721 Pledgee: Shandong agricultural financing Company limited by guarantee Pledgor: Shandong Kesai Agriculture Biotechnology Co. Ltd. Registration number: 2015370000060 Date of cancellation: 20181218 Granted publication date: 20100721 Pledgee: Shandong agricultural financing Company limited by guarantee Pledgor: Shandong Kesai Agriculture Biotechnology Co. Ltd. Registration number: 2015370000060 |
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TR01 | Transfer of patent right |
Effective date of registration: 20190402 Address after: 261000 Lingang Chemical Park, Weifang Binhai Economic Development Zone, Shandong Province Patentee after: Shandong Dehao Chemical Co., Ltd. Address before: 250100 Shandong, Ji'nan, Licheng District, Zhejiang Province Patentee before: Shandong Kesai Agriculture Biotechnology Co. Ltd. Effective date of registration: 20190402 Address after: 261000 Lingang Chemical Park, Weifang Binhai Economic Development Zone, Shandong Province Patentee after: Shandong Dehao Chemical Co., Ltd. Address before: 250100 Shandong, Ji'nan, Licheng District, Zhejiang Province Patentee before: Shandong Kesai Agriculture Biotechnology Co. Ltd. |
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