CN101485392B - Method for processing composite aminoacid small peptide chelated microelement feed addictive - Google Patents
Method for processing composite aminoacid small peptide chelated microelement feed addictive Download PDFInfo
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- CN101485392B CN101485392B CN2009100089141A CN200910008914A CN101485392B CN 101485392 B CN101485392 B CN 101485392B CN 2009100089141 A CN2009100089141 A CN 2009100089141A CN 200910008914 A CN200910008914 A CN 200910008914A CN 101485392 B CN101485392 B CN 101485392B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
The invention relates to a method for processing a compound amino acid small peptide chelate trace element feed additive, which comprises the following steps: taking 10 portions of fresh and alive earthworms, flushing the earthworms by water, standing over night, and putting the cleaned earthworms into a container; capping and sealing the container, putting the container into a thermostatic tank, and carrying out enzymolysis for the earthworms for 5 to 12 hours at a temperature of between 30 and 65 DEG C to prepare earthworm enzymolysis solution; taking 1 to 12 portions of trace element inorganic acid, dissolving the trace element inorganic acid by warm water at a temperature of between 20 and 70 DEG C, pouring the solution into the earthworm enzymolysis solution to prepare mixed solution, and putting the mixed solution into the thermostatic tank to react for 1 to 3 hours; taking 2 to 6 portions of plant proteinoid feed, crushing the feed, sieving the crushed feed by a sieve of 60 to 80 meshes, adding the sieved feed into the mixed solution, stirring the solution, and then putting the solution into a dryer for drying at a temperature of between 100 and 120 DEG C, wherein the water content of the dried product is lower than 12 percent; and crushing the solid product, wherein the crushed product is a finished product of the compound amino acid small peptide chelate trace element feed additive.
Description
Technical field
The present invention relates to a kind of processing method of feed addictive, specifically a kind of processing method of composite aminoacid small peptide chelated microelement feed addictive.
Background technology
Trace element participates in various physiology, the biochemical process of animal body, it is one of essential nutritional factors of animal body, in livestock and poultry breeding industry, though the consumption of microelement feed addictive seldom, bringing into play important role with the aspects such as resistance against diseases of reproductive performance, enhancing body in the production of growing, improve that promotes animal.Microelement feed addictive has experienced three developing stage substantially, i.e. inorganic salts, simple organic compound and aminoacid chelating microelement.Inorganic salts and simple organic compound class trace mineral supplement exist that absorption rate is low, addition greatly, easily causes shortcomings such as environmental pollution.Though and aminoacid chelating microelement has higher bioavailability, and have special trophism,, limited its extensive use in Production of Livestock and Poultry because its cost is higher at disease resistance, anti-aspects such as reproductive performance that stress and improve livestock and poultry.
Summary of the invention
Goal of the invention of the present invention is in order to overcome deficiency of the prior art, and after providing a kind of protease with earthworm self that earthworm is hydrolyzed into several amino acids and little peptide, with micro-inorganic salts generation chelatropic reaction, thus the processing method of producing composite aminoacid small peptide chelated microelement feed addictive.
Realize the foregoing invention purpose by the following technical solutions: a kind of processing method of composite aminoacid small peptide chelated microelement feed addictive, it processes raw material and mainly is made of earthworm, micro-inorganic salts, plant albuminoid feed, and the processing method of this additive is carried out according to following steps:
A, get 10 parts of fresh and alive earthworms by weight, be placed in the pond, water flushing back standing over night is discharged the residue in its alimentary canal, takes out then and puts into container after earthworm is cleaned with distilled water, treats materials as earthworm;
B, the container that earthworm treats materials will be housed seal, put into insulating box, under 30-65 ℃ temperature conditions enzymolysis 5-12 hour, obtain the earthworm enzymolysis liquid;
C, get micro-inorganic salts 1-12 part by weight again, pour in the earthworm enzymolysis liquid after its warm water with 20-70 ℃ dissolved fully, make mixed liquor after stirring, again mixed liquor put into insulating box reaction 1-3 hour, during stirred once every 20-30 minute;
D, mixed liquor is taken out from insulating box, get plant albuminoid feed 2-6 part in addition by weight, pulverize the back and cross the 60-80 mesh sieve, screenings is joined in the mixed liquor, put into dryer after fully stirring, with its oven dry, the solid product internal moisture content after the oven dry is lower than 12% under 100-120 ℃ temperature conditions;
E, solid product is pulverized, its grinding particle size is the 60-120 order, and the product after the pulverizing is the composite aminoacid small peptide chelated microelement feed addictive finished product.
Compared with prior art, beneficial effect of the present invention is: contain several amino acids and little peptide components in the earthworm enzymolysis liquid, can be respectively and the ion generation chelatropic reaction of micro-inorganic salts, form composite aminoacid small peptide chelated microelement, and contain multiple bioactive ingredients, this product has higher bioavailability, nutrition is comprehensive and reasonable more, production and processing is simple and convenient, low production cost, and the systematization production of factory suits to carry out.
The specific embodiment
Below in conjunction with embodiment in detail the present invention is described in detail.
Step is made composite aminoacid small peptide chelated microelement feed addictive as follows, and micro-inorganic salts of the present invention comprise copper sulphate, ferrous sulfate, zinc sulfate, zinc oxide, manganese sulfate etc.; Plant albuminoid feed comprises corn protein powder, dregs of beans (cake), the cottonseed dregs of rice (cake), rapeseed dregs (cake), peanut meal (cake) etc.
Embodiment one: the micro-inorganic salts in the present embodiment adopt copper sulphate, and plant albuminoid feed adopts corn protein powder, and its preparation method is as follows:
A. get fresh and alive earthworm and place the pond for 100 kilograms, water flushing, and standing over night to be to discharge the residue in the earthworm alimentary canal is rinsed it well with distilled water after taking out earthworm, puts into container, treats materials as earthworm;
B., after container that earthworm treats materials will be housed seal, put into insulating box, enzymolysis is 7 hours under 50 ℃ temperature conditions, obtains the earthworm enzymolysis liquid, and the protease of earthworm self can be hydrolyzed into earthworm several amino acids and little peptide;
C. take by weighing 5 kilograms in copper sulphate, warm water with 35 ℃ dissolves it fully, be poured in the molten device that the earthworm enzymolysis liquid is housed, obtain mixed liquor after stirring, this mixed liquor is put into insulating box, under 50 ℃ temperature conditions, reacted 2 hours, this secondary response is the ion generation chelatropic reaction of amino acid, little peptide and micro-inorganic salts, between this stage of reaction, every 30 minutes mixed liquor is stirred once;
D. container is taken out from insulating box, other gets 50 kilograms of corn protein powders, after crossing 80 mesh sieves, its screenings is joined in the container that mixed liquor is housed, fully stir, mix, then container is put into dryer, dry under 100-120 ℃ temperature conditions, the solid product internal moisture content after its oven dry is controlled at below 12%;
E. solid product is pulverized, its grinding particle size is controlled at about 80 orders, and the finished product after the pulverizing is the finished product of the feed addictive of composite aminoacid small peptide chelated copper.
Embodiment two: the micro-inorganic salts in the present embodiment adopt zinc sulfate, and plant albuminoid feed adopts peanut meal, and its preparation method is as follows:
A. get dried earthworms by weight and place container for 10 kilograms, add 30 kilograms of distilled water, soaked 12 hours, treat materials as earthworm;
B., after container that earthworm treats materials will be housed seal, put into insulating box, enzymolysis is 10 hours under 40 ℃ temperature conditions, obtains the earthworm enzymolysis liquid, and the protease of earthworm self can be hydrolyzed into earthworm several amino acids and little peptide;
C. take by weighing 2 kilograms in zinc sulfate, with 40 ℃ of warm water it is dissolved fully, be poured in the molten device that the earthworm enzymolysis liquid is housed, obtain mixed liquor after stirring, this mixed liquor is put into insulating box, under 40 ℃ temperature conditions, reacted 2.5 hours, this secondary response is the ion generation chelatropic reaction of amino acid, little peptide and micro-inorganic salts, between this stage of reaction, every 20 minutes mixed liquor is stirred once;
D. container is taken out from insulating box, other gets 20 kilograms of pulverizing of peanut meal, after crossing 80 mesh sieves, its screenings is joined in the container that mixed liquor is housed, fully stir, mix, then container is put into dryer, dry under 100-120 ℃ temperature conditions, the solid product internal moisture content after its oven dry is controlled at below 12%;
E. solid product is pulverized, its grinding particle size is controlled at about 100 orders, and the finished product after the pulverizing is the finished product of the feed addictive of composite aminoacid small peptide chelated zinc.
More than disclosed only be of the present invention two each and every one embodiment, but the present invention is not limited thereto, any those skilled in the art can think variation, all should drop within protection scope of the present invention.
Claims (2)
1. the processing method of a composite aminoacid small peptide chelated microelement feed addictive, it processes raw material and mainly is made of earthworm, micro-inorganic salts, plant albuminoid feed, it is characterized in that the processing method of this additive is carried out according to following steps:
A, get 10 parts of fresh and alive earthworms by weight, be placed in the pond, water flushing back standing over night is discharged the residue in its alimentary canal, takes out then and puts into container after earthworm is cleaned with distilled water, treats materials as earthworm;
B, the container that earthworm treats materials will be housed seal, put into insulating box, under 30-65 ℃ temperature conditions enzymolysis 5-12 hour, obtain the earthworm enzymolysis liquid;
C, get micro-inorganic salts 1-12 part by weight again, pour in the earthworm enzymolysis liquid after its warm water with 20-70 ℃ dissolved fully, make mixed liquor after stirring, again mixed liquor put into insulating box reaction 1-3 hour, during stirred once every 20-30 minute;
D, mixed liquor is taken out from insulating box, get plant albuminoid feed 2-6 part in addition by weight, pulverize the back and cross the 60-80 mesh sieve, screenings is joined in the mixed liquor, put into dryer after fully stirring, with its oven dry, the solid product internal moisture content after the oven dry is lower than 12% under 100-120 ℃ temperature conditions;
E, solid product is pulverized, its grinding particle size is the 60-120 order, and the product after the pulverizing is the composite aminoacid small peptide chelated microelement feed addictive finished product.
2. the processing method of composite aminoacid small peptide chelated microelement feed addictive according to claim 1, it is characterized in that, earthworm in the raw material is selected dried earthworms for use, its method for preparing that earthworm treats materials is: get dried earthworms by weight and place container for 2 parts, add distilled water 5-10 part, soaked 10-15 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2009100089141A CN101485392B (en) | 2009-02-13 | 2009-02-13 | Method for processing composite aminoacid small peptide chelated microelement feed addictive |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2009100089141A CN101485392B (en) | 2009-02-13 | 2009-02-13 | Method for processing composite aminoacid small peptide chelated microelement feed addictive |
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| CN101485392A CN101485392A (en) | 2009-07-22 |
| CN101485392B true CN101485392B (en) | 2011-08-31 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101849615A (en) * | 2010-06-08 | 2010-10-06 | 丁积平 | Preparation and application for feed additive |
| CN103005228B (en) * | 2013-01-15 | 2013-10-23 | 唐山师范学院 | Preparation method and application of additive for preventing diarrhea of piglet and promoting growth |
| CN103508779B (en) * | 2013-09-29 | 2015-07-08 | 苏州农业职业技术学院 | Organic selenium nutrient solution as well as preparation method and application thereof |
| CN103621790A (en) * | 2013-11-29 | 2014-03-12 | 南宁市百济生物工程有限公司 | Composite earthworm enzymatic hydrolysate feed additive and preparation method thereof |
| CN107176865A (en) * | 2017-06-30 | 2017-09-19 | 宁波费尔诺生物科技有限公司 | The sweetened liquid fertilizer method of preparation and use of marine alga earthworm hydrolyzate efficient bio-active |
| CN109331044A (en) * | 2018-11-20 | 2019-02-15 | 成都市农林科学院 | A kind of earth-worm extractive as raw material and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1334090A (en) * | 2000-07-19 | 2002-02-06 | 云南爱地生物技术研究所 | Earthworm-amino acid zinc for feed and its preparing process |
| CN1566356A (en) * | 2003-06-20 | 2005-01-19 | 陈训高 | Method for preparing earthworm bioactive peptide and earthworm biological micro-fertilizer and use thereof |
| CN1568750A (en) * | 2004-04-29 | 2005-01-26 | 雷金丰 | Production method of rainworm amino acid composite animal nutrient solution |
| CN101002598A (en) * | 2007-01-19 | 2007-07-25 | 唐山师范学院 | Art for producing milk production increasing agent by utilizing earth-worm extractive as raw material |
| CN101243832A (en) * | 2008-03-21 | 2008-08-20 | 唐山师范学院 | Process technique of ecological nutrition feedstuff additive |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1334090A (en) * | 2000-07-19 | 2002-02-06 | 云南爱地生物技术研究所 | Earthworm-amino acid zinc for feed and its preparing process |
| CN1566356A (en) * | 2003-06-20 | 2005-01-19 | 陈训高 | Method for preparing earthworm bioactive peptide and earthworm biological micro-fertilizer and use thereof |
| CN1568750A (en) * | 2004-04-29 | 2005-01-26 | 雷金丰 | Production method of rainworm amino acid composite animal nutrient solution |
| CN101002598A (en) * | 2007-01-19 | 2007-07-25 | 唐山师范学院 | Art for producing milk production increasing agent by utilizing earth-worm extractive as raw material |
| CN101243832A (en) * | 2008-03-21 | 2008-08-20 | 唐山师范学院 | Process technique of ecological nutrition feedstuff additive |
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