CN101473926B - Method for preparing response type peanut essence - Google Patents
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- CN101473926B CN101473926B CN2009100956955A CN200910095695A CN101473926B CN 101473926 B CN101473926 B CN 101473926B CN 2009100956955 A CN2009100956955 A CN 2009100956955A CN 200910095695 A CN200910095695 A CN 200910095695A CN 101473926 B CN101473926 B CN 101473926B
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Abstract
The invention discloses a method for preparing response type peanut essence, comprising the following steps: peanut meal is ground and the ground peanut meal is hydrolyzed by alkali protease after being screened; then the peanut meal is hydrolyzed again by protamex, and the supernate is filtered to obtain peanut meal hydrolyzate; other material is added for thermal reaction and stabilizing agent and substances for blending flavour are added after the heating is stopped, thereby obtaining the response type peanut essence. In the method, the peanut essence is produced by the thermal reaction, so that the problems of weak fragrance and poor taste of the essence with the products produced by chemical synthetic perfume are solved; in addition, as the raw material is natural, the product is harmless and nutritious with genuine and strong peanut fragrance and nutrition.
Description
Technical field
The present invention relates to a kind of food additive field, particularly a kind of method of utilizing the peanut pool to prepare peanut essence.
Background technology
Peanut (Arachis hypogaea L.) has another name called peanut, peanut, papaw, is pulse family butterfly suborder (Papilonaceae) annual herb self-pollinated plant, has nearly 500 years plantation historical in China.Peanut has very high medical medical value, and it is malnutritive to can be used for treatment, taste imbalance, various anaemias, cough asthma due to excessive phlegm, the dry constipation of intestines, diseases such as agalactosis.Supplementary Amplifications of the Compendium of Materia Medica carries: peanut is pleased spleen and stomach, moistening lung for removing phlegm, nourish tonifying Qi, clearing is antipruritic.Carry " the southern regions of the Yunnan Province book on Chinese herbal medicine ": peanut salt solution is cooked and is controlled the lung pain, fries and use the dryness-heat promoting circulation of blood, controls that cold long-pending tripe aches in the abdomen." property of medicine is examined " carries: these article fry edible clearing stomach and are amusing, and laxation is moisturized.Contain multiple anti-ageing composition in the peanut, especially in the majority with monounsaturated fatty acids, resveratrol, β-phytosterol, folic acid and trace element zinc.
Peanut is one of the world five big oil crops, and it produces each continent all over the world, and whole world cultivated area is 2173.9 ten thousand hectares, and wherein the Asia accounts for more than 56%.China is peanut big producing country, China's peanut cultivation area cumulative year after year in recent years, and to 2005, annual production reached 1,500 ten thousand tons, occupies the No. 1 in the world.
China is the largest production state and the country of consumption of peanut in the world, and except that few part ate as dry fruit, major part was used to squeeze edible oil and fat as oil resource.Peanut has surpassed other oil plant (vegetable seed, sunflower seeds and cottonseed etc.) as its output of a kind of oil crops, accounts for 40% of domestic oil plant gross output.
Peanut meal is the accessory substance after shelled peanut extracts oil, is a kind of plant protein resource of high nutrition, and wherein protein content is up to 50%～70% (butt); Be rich in multiple human body essential amino acid; Do not contain cholesterol, its nutritive value and animal protein are close, and digestibility is high.
China has extremely abundant peanut protein resource, and annual have the peanut meal more than 3,000,000 tons to demand development and use urgently approximately, and it is mainly as feed or fertilizer at present, and cheap.China has a large amount of peanut protein like this well not develop and useedd, even certain exploitation is arranged, does not also form large-scale production, causes the huge waste of peanut protein resource.
Food flavor is the important source of modern processed food fragrance, and beautiful pursuit has important function to food flavor for satisfying people, can roughly be divided into two big types of natural perfume material and chemically composite perfumes.The raw material of chemically composite perfume is easy to get, and cost price is extremely cheap, and fragrance is thin, mouthfeel is relatively poor, simultaneously synthetic perfume its insecurity that comes to light gradually; Natural perfume material fragrance pure, strong with and security and the synthetic perfume olfactory that is difficult to substitute and the organoleptic attribute strong preference that receives consumers in general.
Hot reaction essence (Process Flavor or Heat-Reaction Flavor) be a kind of by raw-food material with (or) raw material that allows in food or reaction essence, to add adds the product of hot preparation.At present, the hot reaction essence of development mainly is a meat flavor both at home and abroad, and nut fruits essence does not almost have.
Nineteen fifty-one, Unilever adopts the method for precursor substances such as heating amino acid and reduced sugar to prepare beef flavor.Nineteen sixty, people such as Morton can obtain having the material of meat giving off a strong fragrance flavor from pentose, hexose and cysteine reaction system.Since the seventies in 20th century; Meat essence has obtained extensive studies and application abroad, and the Takasago company of the Qi Huadun company of the IFF company of the many in the world essence corporations such as the U.S., the BBA company of Britain, Switzerland, Japan etc. all produces meat essence in a large number.
At present, the peanut essence of selling on the domestic and international market all forms with the chemically composite perfume allotment.
Summary of the invention
The objective of the invention is to overcome deficiency of the prior art, providing a kind of is raw material with the peanut meal, through the method for reaction for preparation peanut essence.
A kind of preparing response type peanut essence of the present invention may further comprise the steps: peanut meal is pulverized, and the peanut meal powder screening after the pulverizing is after hydrolysis by novo; Through the compound protein enzyme hydrolysis, cross the leaching supernatant again, obtain the peanut meal hydrolyzate; Add other material thermal response; After stopping heating, add stabilizing agent and blending thing, obtain response type peanut essence.
Described peanut meal powder was the choosings of 200 mesh sieves.
Described other material is: amino acid A, amino acid B, amino acid C, amino acid D, thiamine, wood sugar, peanut oil.
Described stabilizing agent is a monoglyceride.
The composition of the blending thing of described peanut essence is by volume part: 1.2～1.8 parts of 40～42 parts of N-methylpyrroles, 0.8～1.2 part of methylpyrazine, 1.2～1.8 parts in 2-methoxyl group furans, hexanal, 2; 0.4～0.6 part of 5-dimethyl pyrazine, 2; 2～4 parts of 6-dimethyl pyrazines, 2; 0.4～0.6 part of 3-dimethyl pyrazine, 2,3,0.8～1.2 part of 5-trimethylpyrazine, 1.2～1.8 parts of n-hexyl alcohols, 0.4～0.6 part of ethyl pyrazine, 2～3 parts of furfuryl alcohols.
The composition of the blending thing of described peanut essence is by volume part: 1.5 parts of 41 parts of N-methylpyrroles, 1.0 parts of methylpyrazines, 1.5 parts in 2-methoxyl group furans, hexanal, 2; 0.5 part of 5-dimethyl pyrazine, 2; 3 parts of 6-dimethyl pyrazines, 2; 0.5 part of 3-dimethyl pyrazine, 2,3,1 part of 5-trimethylpyrazine, 1.5 parts of n-hexyl alcohols, 0.5 part of ethyl pyrazine, 2.5 parts of furfuryl alcohols;
As preparing response type peanut essence of the present invention further, may further comprise the steps:
(1) will moor the phosphate buffer solution that powder adds the amount adding pH9.0 of 8～12ml by every gram peanut through pulverizing 8～12 parts in 200 purpose peanut meal powder, add 1～2 part in alkali protease powder; Electric blender 100rpm rotating speed stirs in 50 ℃ of water-baths, behind hydrolysis 1～3h, adds 1～2 part of compound protease; After continuing hydrolysis 1～3h; Take out beaker and in 100 ℃ of boiling water baths, heat 8～20min, make enzyme deactivation, cross the leaching supernatant; Hydrolyzate is concentrated into 1/7th to 1/4th volumes through rotary evaporation, obtains the peanut meal hydrolyzate;
(2) add other material thermal response
Get 100 parts of peanut meal hydrolyzates, add 1.2～2 parts of amino acid A, 1～2 part of amino acid B, 1.2～2 parts of amino acid C, 1～2 part of amino acid D, 0.3～0.8 part of thiamine, 1～2 part of wood sugar, 7～12 parts of peanut oil; Stirring makes the heating and refluxing in 120 ℃～140 ℃ oil bath pans of abundant dissolving back, behind 50～70min, stops heating, obtains the peanut essence base-material after the thermal response.
(3) preparation of response type peanut essence
Get 200 parts of peanut essence base-material and 3～5 parts of monoglycerides after the thermal response, stir, in 90 ℃ of oil bath pans behind reflux 8～12min; Stop heating; Add 8～12 parts of blending things after cooling to 50～70 ℃, continue to stir 3～6min, obtain response type peanut essence.
The present invention has following beneficial effect:
The present invention is raw material with the peanut meal; Through reaction for preparation peanut spices; Can solve problems such as the essence fragrance that product brought that forms with the chemically composite perfume allotment is thin, mouthfeel is relatively poor; And because employed raw material is taken from naturally, product nutrition is harmless, has pure, the strong peanut fragrance and the function of nutrition concurrently.
Simultaneously, prepare peanut spices, not only can solve the handling problem of discarded object, and have an economic benefit, reduce the production cost of enterprise greatly, open up a new approach for the value added applications of peanut meal simultaneously with peanut meal.
The specific embodiment
Through the specific embodiment the present invention is described in further detail below:
Embodiment 1, preparing response type peanut essence
(1) in the 1000mL beaker, adds through pulverizing 200 purpose peanut meal powder 50g, add the phosphate buffer solution 500ml of pH9.0, add the alkali protease powder and (believe available from Novi; Alkali protease Alcalase 2.4L) 5g, electric blender 100rpm rotating speed stirs in 50 ℃ of water-baths, behind the hydrolysis 2h; Add compound protease (available from Novi's letter, compound protease Protamex) 5g, behind the continuation hydrolysis 2h; Take out beaker and in 100 ℃ of boiling water baths, heat 10min, make enzyme deactivation, double gauze filters; Hydrolyzate is concentrated to 100mL through rotary evaporation in vacuo, promptly obtains the peanut meal hydrolyzate;
(2) reaction for preparation peanut essence base-material
In the 1000mL there-necked flask, add peanut meal hydrolyzate 100mL, add amino acid A (alanine Ala) 1.6g; Amino acid B (aspartic acid, asparagine Asx) 1.4g, amino acid C (cysteine Cys) 1.6g; Amino acid D (asparatate Asp) 1.3g; Thiamine 0.5g, wood sugar 1.25g, peanut oil 10g.Electronic stirring makes solid dissolving back heating and backflow in 135 ℃ of oil bath pans, behind the 60min, stops heating.Obtain frying the peanut essence base-material of peanut fragrance.
(3) preparation of the blending thing of peanut essence
In the 500mL beaker; Add N-methylpyrrole 41ml, methylpyrazine 1.0ml, 2-methoxyl group furans 1.5ml, hexanal 1.5ml, 2 respectively; 5-dimethyl pyrazine 0.5ml, 2,6-dimethyl pyrazine 3ml, 2,3-dimethyl pyrazine 0.5ml, 2; 3,5-trimethylpyrazine 1ml, n-hexyl alcohol 1.5ml, ethyl pyrazine 0.5ml, furfuryl alcohol 2.5ml.Behind the mixing, obtain the blending thing.
(4) preparation of paste peanut essence
In the 500mL there-necked flask, essence base-material and 4g stabilizing agent (monoglyceride) after the adding 200g thermal response behind the reflux 10min, stop heating under the electronic stirring in 90 ℃ of oil bath pans.Add 10mL blending thing after cooling to 60 ℃, continue to stir 5min, obtain frying the peanut essence of peanut fragrance.
The examining report of the peanut essence that table 1 the present invention obtains, report number 20088099:
| Sequence number | Test item | Unit | Standard value | Result data | Individual event is judged |
| 1 | Fragrance | The standard sample that meets same model | Meet | Meet | |
| 2 | Fragrance | The standard sample that meets same model | Meet | Meet | |
| 3 | The look shape | The standard sample that meets same model | Meet | Meet | |
| 4 | Heavy metal (in pb) | mg/kg | ≤10 | ＜10 | Meet |
| 5 | Arsenic (in As) | mg/kg | ≤3 | ＜3 | Meet |
| 6 | Total number of bacteria | Individual/g | ≤10000 | 20 | Meet |
| 7 | Coliform | MPN/100g | ≤30 | ＜30 | Meet |
| 8 | Lead content | mg/kg | ≤10 | 0.9 | Meet |
| 9 | Mercury content | mg/kg | ≤1 | ＜0.1 | Meet |
| 10 | Cadmium content | mg/kg | ≤1 | 0.1 | Meet |
Embodiment 2, preparing response type peanut essence
(1) in the 1000mL beaker, adds through pulverizing 200 purpose peanut meal powder 60g, add the phosphate buffer solution 480ml of pH9.0, add the alkali protease powder and (believe available from Novi; Alkali protease Alcalase 2.4L) 8g, electric blender 100rpm rotating speed stirs in 50 ℃ of water-baths, behind the hydrolysis 2h; Add compound protease (available from Novi's letter, compound protease Protamex) 10g, behind the continuation hydrolysis 2h; Take out beaker and in 100 ℃ of boiling water baths, heat 20min, make enzyme deactivation, double gauze filters; Hydrolyzate is concentrated to 100mL through rotary evaporation in vacuo, promptly obtains the peanut meal hydrolyzate;
(2) reaction for preparation peanut essence base-material
In the 1000mL there-necked flask, add peanut meal hydrolyzate 100mL, add amino acid A (alanine Ala) 2g, amino acid B (aspartic acid; Asparagine Asx) 1.8g, amino acid C (cysteine Cys) 2g, amino acid D (asparatate Asp) 1.8g; Thiamine 1g, wood sugar 1.5g, peanut oil 12g.Electronic stirring makes solid dissolving back heating and backflow in 140 ℃ of oil bath pans, behind the 70min, stops heating.Obtain frying the peanut essence base-material of peanut fragrance.
(3) preparation of the blending thing of peanut essence
In the 500mL beaker; Add N-methylpyrrole 42ml, methylpyrazine 1.0ml, 2-methoxyl group furans 1.6ml, hexanal 1.5ml, 2 respectively; 5-dimethyl pyrazine 0.6ml, 2,6-dimethyl pyrazine 3ml, 2,3-dimethyl pyrazine 0.5ml, 2; 3,5-trimethylpyrazine 1ml, n-hexyl alcohol 1.5ml, ethyl pyrazine 0.6ml, furfuryl alcohol 2.8ml.Behind the mixing, obtain the blending thing.
(4) preparation of paste peanut essence
In the 500mL there-necked flask, essence base-material and 4g stabilizing agent (monoglyceride) after the adding 200g thermal response behind the reflux 10min, stop heating under the electronic stirring in 90 ℃ of oil bath pans.Add 10mL blending thing after cooling to 60 ℃, continue to stir 5min, obtain frying the peanut essence of peanut fragrance.Fragrance, fragrance, look shape all meet standard
At last, it is also to be noted that what more than enumerate only is practical implementation example of the present invention.Obviously, the invention is not restricted to above examples of implementation, many distortion can also be arranged.All distortion that those of ordinary skill in the art can directly derive or associate from content disclosed by the invention all should be thought protection scope of the present invention.
Claims (3)
1. preparing response type peanut essence is characterized in that may further comprise the steps: peanut meal is pulverized, and the peanut meal powder screening after the pulverizing is after hydrolysis by novo; Through the compound protein enzyme hydrolysis, cross the leaching supernatant again, obtain the peanut meal hydrolyzate; Add other material thermal response; After stopping heating, add stabilizing agent and blending thing, obtain response type peanut essence; Described peanut meal powder was the choosings of 200 mesh sieves; Described other material is: amino acid A, amino acid B, amino acid C, amino acid D, thiamine, wood sugar, peanut oil; Described stabilizing agent is a monoglyceride; The composition of the blending thing of described peanut essence is by volume part: 1.2～1.8 parts of 40～42 parts of N-methylpyrroles, 0.8～1.2 part of methylpyrazine, 1.2～1.8 parts in 2-methoxyl group furans, hexanal, 2; 0.4～0.6 part of 5-dimethyl pyrazine, 2; 2～4 parts of 6-dimethyl pyrazines, 2; 0.4～0.6 part of 3-dimethyl pyrazine, 2,3,0.8～1.2 part of 5-trimethylpyrazine, 1.2～1.8 parts of n-hexyl alcohols, 0.4～0.6 part of ethyl pyrazine, 2～3 parts of furfuryl alcohols.
2. preparing response type peanut essence according to claim 1; It is characterized in that described peanut essence the blending thing composition by volume part: 1.5 parts of 41 parts of N-methylpyrroles, 1.0 parts of methylpyrazines, 1.5 parts in 2-methoxyl group furans, hexanal, 2; 0.5 part of 5-dimethyl pyrazine, 2,3 parts of 6-dimethyl pyrazines, 2,0.5 part of 3-dimethyl pyrazine, 2; 3,1 part of 5-trimethylpyrazine, 1.5 parts of n-hexyl alcohols, 0.5 part of ethyl pyrazine, 2.5 parts of furfuryl alcohols.
3. according to the described preparing response type peanut essence of claim 1～2, it is characterized in that may further comprise the steps:
(1) will moor the phosphate buffer solution that powder adds the amount adding pH9.0 of 8～12ml by every gram peanut through pulverizing 8～12 parts in 200 purpose peanut meal powder, add 1～2 part in alkali protease powder; Electric blender 100rpm rotating speed stirs in 50 ℃ of water-baths, behind hydrolysis 1～3h, adds 1～2 part of compound protease; After continuing hydrolysis 1～3h; Take out beaker and in 100 ℃ of boiling water baths, heat 8～20min, make enzyme deactivation, cross the leaching supernatant; Hydrolyzate is concentrated into 1/7th to 1/4th volumes through rotary evaporation, obtains the peanut meal hydrolyzate;
(2) add other material thermal response
Get 100 parts of peanut meal hydrolyzates, add 1.2～2 parts of amino acid A, 1～2 part of amino acid B, 1.2～2 parts of amino acid C, 1～2 part of amino acid D, 0.3～0.8 part of thiamine, 1～2 part of wood sugar, 7～12 parts of peanut oil; Stirring makes the heating and refluxing in 120 ℃～140 ℃ oil bath pans of abundant dissolving back, behind 50～70min, stops heating, obtains the peanut essence base-material after the thermal response;
(3) preparation of response type peanut essence
Get 200 parts of peanut essence base-material and 3～5 parts of monoglycerides after the thermal response, stir, in 90 ℃ of oil bath pans behind reflux 8～12min; Stop heating; Add 8～12 parts of blending things after cooling to 50～70 ℃, continue to stir 3～6min, obtain response type peanut essence.
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| CN2009100956955A CN101473926B (en) | 2009-01-19 | 2009-01-19 | Method for preparing response type peanut essence |
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| CN101473926B true CN101473926B (en) | 2012-07-18 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102551009B (en) * | 2010-12-17 | 2013-07-31 | 上海爱普植物科技有限公司 | Method for preparing natural dried fruit essence by utilizing dried fruit raw materials |
| CN103110083A (en) * | 2013-02-22 | 2013-05-22 | 广州联丰香料科技有限公司 | Preparation method of nut essence |
| CN104207090B (en) * | 2014-09-09 | 2015-09-30 | 王婧婧 | A kind of preparation method of walnut essence |
| CN104256494B (en) * | 2014-09-14 | 2016-09-07 | 王婧婧 | A kind of preparation method of fibert essence |
| CN104621523B (en) * | 2015-03-18 | 2016-09-07 | 王婧婧 | A kind of preparation method of salted dried mustard cabbage taste essence |
| CN105062657A (en) * | 2015-08-04 | 2015-11-18 | 西宁科进工业设计有限公司 | Almond processing apparatus and processing method |
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Address after: 311121, Yuhang District, Zhejiang province Hangzhou former industrial park Patentee after: Zhejiang Lvjing Biotechnology Co., Ltd Address before: 311121 No. 2 Dragon Boat Road, Cang Qian Industrial Park, Yuhang District, Zhejiang, Hangzhou Patentee before: Zhejiang Green Crystal Flavor Co., Ltd. |