CN101444211A - Synergy desinsection composite containing anabasine compound and application thereof - Google Patents
Synergy desinsection composite containing anabasine compound and application thereof Download PDFInfo
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- CN101444211A CN101444211A CNA2008101907400A CN200810190740A CN101444211A CN 101444211 A CN101444211 A CN 101444211A CN A2008101907400 A CNA2008101907400 A CN A2008101907400A CN 200810190740 A CN200810190740 A CN 200810190740A CN 101444211 A CN101444211 A CN 101444211A
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Abstract
The invention relates to a desinsection composite and applications thereof. The effective components are Nitenpyram and carbamate pesticides; the desinsection composite is used for controlling pests on plants. The desinsection composite can be processed into any preparation formulation acceptable to pesticide application; the preferable preparation formulation is a wettable powder, aqueous emulsion, missible oil, microemulsion, water dispersible granule or troche, and a suspending agent.
Description
Technical field
The present invention relates to composition pesticide and application thereof, being specially with Nitenpyram and carbamate insecticide is the Pesticidal combination of active ingredient, and the insect on the control plant especially is suitable for preventing and treating plant hopper, leafhopper and thrips.
Background technology
Insects such as plant hopper, aleyrodid, aphid, thrips, diamond-back moth are the important pests on the crops such as paddy rice, cotton, fruit tree, vegetables, not only have a strong impact on the growing way of plant, and breeding is fast, and it is many that algebraically takes place, and generation overlap is serious, therefore control is relatively more difficult, and forms pesticide resistance easily.
Rice fulgorid is one of paddy rice three major pests, can migrate at a distance, and can propagate the paddy rice virus disease.The rice fulgorid breeding amount is big, and every mu of insect population number can reach heads up to a million when serious, can cause crushing harm to paddy rice.In China South China and Central China, the rice fulgorid pesticide resistance is obvious, and some areas brown planthopper is to the resistant multiple of Imidacloprid even up to 250-400 times.And the conventional pesticide composition, as the sumicidin in the pyrethroid, the phoxim in the organic phosphor, the Mobucin of carbamates etc., control has not almost had any effect separately.So develop the antagonism insect as early as possible, especially the resistant rice plant hopper is effective, and the good medicament that can be accepted by numerous growers on price, has become the urgent need in the production.
Nitenpyram, English general nitenpyram by name is a kind of efficient, wide spectrum, novel nicotinamide insecticide.Mainly act on the nerve of insect, the aixs cylinder of insect is touched acceptor have the nerve block effect.Nitenpyram has remarkable interior suction and osmosis, and consumption is few, and toxicity is low, to crop safety, no poisoning.Nitenpyram can be widely used in paddy rice, fruit tree, vegetables and tea, control rice fulgorid, aphid, thrips, trialeurodes vaporariorum, Bemisia tabaci, leafhopper etc.Its structure and Imidacloprid belong to anabasine, and the pesticide resistance risk is higher, must take preventive measures.
Go up the insect that produces resistance for control agricultural, a kind of way is to release the new component that new and existing kind do not have cross resistance.But, the development cost height of new active ingredient, the construction cycle is long, and development rate produces the speed of resistance less than insect.The composition of different cultivars carries out composite, is control resistant insect or the very common way of evil mite.If synergy mutually between each component of evidence composition, said composition promptly can be used for further development and utilization.
At present, the composite and application of Nitenpyram and carbamate insecticide occurs as yet, does not at home and abroad also appear in the newspapers in the document.
Summary of the invention
Based on above statement, the purpose of this invention is to provide a kind of Pesticidal combination, quick-acting is good, and the lasting period is long, can reduce the usage amount of agricultural chemicals, and the control efficiency of its antagonism property of medicine insect is good especially, helps to overcome and delay pest resistance to insecticide.
Another object of the present invention provides the application of Pesticidal combination.
The objective of the invention is to be achieved through the following technical solutions:
The agricultural chemicals of different cultivars shows three kinds of type of action: summation action, synergistic effect and antagonism after mixing usually.But be specially which kind of effect, can't do not determine by a large amount of tests.
Patent applicant of the present invention is surprised to find that the mixed use of Nitenpyram and carbamate insecticide by indoor biological activity determination test, and insect is had the notable synergistic effect, after further study, has finished the present invention.
The carbamate insecticide that the present invention relates to comprises:
1, Mobucin has another name called isoprocarb, English general isoprocarb by name, and the CA registration number is 2631-40-5.Mobucin has stronger action of contace poison, and the power of knocking down is strong, and drug effect is rapid, but the longevity of residure is shorter, generally has only 3-5 days.Rice fulgorid, Cicadellidae insect are had special efficacy, and can doublely control thrips and leech, to natural enemy, Araneae safety.
2, meta-tolyl-N-methylcarbamate (MTMC), English general metolcarb by name, the CA registration number is 1129-41-5.Meta-tolyl-N-methylcarbamate (MTMC) has tags and fumigation action, rice fulgorid, rice leafhopper and rice thrips and tea lesser leafhopper there are special efficacy, also can be used for preventing and treating rice leaf roller, tea tree aphid, smaller green leaf hopper, long white scale insect and tortoise plastron scale insect, black aleyrodid, citrus goitre mite, cotton aphid, cotton bollworm etc.
3, Bassa has another name called bufencarb, English general fenobucarb by name, and the CA registration number is 3766-81-2.Bassa has strong action of contace poison, and has certain stomach toxicity, stifling and ovicidal action.Can prevent and treat the insects such as leafhopper, plant hopper, aphid and weevil on paddy rice, tealeaves, sugarcane, wheat, pumpkin, the purple eggplant, also can prevent and treat sanitary insect pests such as the cotton bollworm of cotton and cotton aphid and mosquito, fly.
4, dimethyl phenyl carbamate is Cosban again, restrains dead prestige, and English general dimethacarb by name is the insecticide that is mixed by two kinds of isomers.Dimethyl phenyl carbamate has strong action of contace poison to insect, and is all effective to Lepidoptera and homoptera pest.
5, Aphox, English general pirimicarb by name has another name called and wards off the aphid mist, and is medium to higher mammal toxicity, to fish, honeybee and birds low toxicity, to natural enemy of aphid safety.Having and tag, fumigate and the blade face osmosis, is the strong aphicide of selectivity, is applicable to the aphid on control vegetables, tobacco, the cereal crops.Desinsection is rapid, but the longevity of residure is short, can not effectively prevent and treat cotten aphid.
The present composition is first active component (A) with Nitenpyram, with carbamate insecticide is second active component (B), B comprises at least a in Mobucin, meta-tolyl-N-methylcarbamate (MTMC), Bassa, dimethyl phenyl carbamate, the Aphox, the ratio of quality and the number of copies of A and B is 1:1-1:20 at 1:1-1:50 preferably.
Pesticidal combination provided by the invention, can be according to crop, the environmental condition of living in of required control, prevent and treat all kinds of factors such as method, control cost, cooperate with the auxiliary material that allows in the agricultural chemicals to use, make acceptable any one formulation in the agricultural chemicals application, the total content of active ingredient is 5-80% in the preparation; Preferred formulation is wetting powder, aqueous emulsion, missible oil, microemulsion, water dispersible granules or tablet.
Auxiliary material in the present composition comprises that solvent, dispersant, wetting agent, emulsifier, stabilizing agent, thickener, pH regulator agent, antifreezing agent, excipient, filler, carrier, synergist, bleeding agent and other are of value to the known substance of active ingredient stable and drug effect performance in preparation, all be the various compositions that permission commonly used in the pesticidal preparations is used, be not particularly limited.
The processing technology of the various preparations of the present composition adopts known method preparation, is method commonly used in the pesticidal preparations processing technology.
Product described in the invention can the finished product preparation form provide, and promptly each material mixes in the composition, and the composition of composition also can provide with single agent form, directly directly mixes in bucket or jar before the use, is diluted to required concentration then.
The present invention is in conjunction with test and embodiment, and composition has obvious synergistic effect as can be seen, and has produced following beneficial effect:
1. the present composition shows fabulous synergistic effect in certain ratio range, the insecticidal effect of composition is significantly improved than single agent, using dosage, dispenser recruitment and the cost of agricultural chemicals have been reduced, also reduced harmful effect and residue of pesticide, had remarkable economic efficiency and social benefit environment.
2. the active ingredient mechanism of action difference in the present composition, the application of composition can delay or overcome the pesticide resistance of insect, prolongs the service life of single agent.
3. the present composition combines the advantage of two kinds of active ingredient insecticidal actions well, has remedied shortcoming separately, and promptly suction is effective in the Nitenpyram, and the lasting period is long, but quick-acting is poor; Carbamate insecticide quick-acting is good, and knockdown effect is strong, but systemic action is relatively poor.
Embodiment
When the present patent application people finds Nitenpyram and some carbamate insecticide applied in any combination unexpectedly, plant hopper there is significant synergistic effect; Nitenpyram and carbamate insecticide are that 1:1-1:50 is composite by ratio of quality and the number of copies, can adopt prior art will contain the former medicine of these active ingredients and suitable assistant agent and make agricultural and go up available any formulation, the total content of two kinds of active ingredients in preparation is 5-80%; The present composition can be used for preventing and treating insect, the especially homoptera pest on the various plants, more particularly water rice hopper, leafhopper and thrips.
In order to make purpose of the present invention, technical scheme and advantage clearer, summary of the invention is described in further detail below in conjunction with embodiment.Should be appreciated that specific embodiment described herein only in order to explanation the present invention, and be not used in qualification the present invention.All any modifications of being made within the spirit and principles in the present invention, be equal to and replace and improvement etc., all should be included within protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
In the embodiment of the invention in the proportioning of all preparations percentage be mass percent, the treatment dosage of the biologicall test part and the test of pesticide effectiveness is effective content.
Embodiment 1:20% Nitenpyram Mobucin suspending agent (1: 1)
Nitenpyram 10%
Mobucin 10%
Poly-naphthaldehyde sulfonate sodium 3%
Alkylaryl polyoxyethylene polyoxypropylene ether 2%
Silicon oil foam killer 0.1%
Xanthans 0.2%
Propane diols 4%
Water is mended to 100%
Mentioned component is added in the mixing kettle in proportion,, be mixed with 20% Nitenpyram Mobucin suspending agent through abundant agitation grinding.
This prescription control rice-leaf hopper test, the contrast medicament is 20% Mobucin missible oil (Shilou County, Fanyu, Guangdong Province Fine Chemical Works) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spray-on process to handle.
This prescription dosage is 30 gram/hectares, and contrast medicament 20% Mobucin missible oil dosage is 600 gram/hectares, and 10% Nitenpyram aqua dosage is 30 gram/hectares, and 5 days control efficiency is respectively 92.8%, 83.6% and 78.3% behind the medicine; 30 days control efficiency is respectively 93.8%, 60.6% and 81.5% behind the medicine.
The control efficiency of this prescription is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 2:25% Nitenpyram Mobucin aqueous emulsion (1: 4)
Nitenpyram 5%
Mobucin 20%
Polyoxyethylene nonylphenol ether 4%
Emulsifier 500# 2%
Polyvinyl alcohol 0.2%
Acetone 3%
Silicone defoaming agent 0.4%
Water is mended to 100%
Above components in certain proportion is added in the mixing kettle, shear, be mixed with 25% Nitenpyram Mobucin aqueous emulsion through fully stirring.
This prescription control water rice hopper test, the contrast medicament is 20% Mobucin missible oil (Shilou County, Fanyu, Guangdong Province Fine Chemical Works) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spray-on process to handle.
This prescription dosage is 135 gram/hectares, and contrast medicament 20% Mobucin missible oil dosage is 600 gram/hectares, and 10% Nitenpyram aqua dosage is 30 gram/hectares, and 5 days preventive effect is respectively 95.3%, 82.6% and 77.8% behind the medicine; 5 days preventive effect is respectively 95.3%, 82.6% and 77.8% behind the medicine.
The control efficiency of this prescription is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 3:22% Nitenpyram Mobucin meta-tolyl-N-methylcarbamate (MTMC) wetting powder (1:
5+5)
Nitenpyram 2%
Mobucin 10%
Meta-tolyl-N-methylcarbamate (MTMC) 10%
Sodium lignin sulfonate 3%
PO-EO block polyether 2%
Lauryl sodium sulfate 5%
Sodium carboxymethyl starch 3%
White carbon is mended to 100%
Mentioned component is through coarse crushing, and after mixing, comminution by gas stream is mixed with 22% Nitenpyram Mobucin meta-tolyl-N-methylcarbamate (MTMC) wetting powder.
This prescription control rice fulgorid test, the contrast medicament is 25% meta-tolyl-N-methylcarbamate (MTMC) wetting powder (Chengdu Huangpai Cropscience Science Co., Ltd.), 40% Mobucin wetting powder (Shenzhen Nuopuxin Agricultural Chemical Co., Ltd) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spraying to handle.
The dosage of this prescription is 30 gram/hectares, the dosage of contrast medicament 25% meta-tolyl-N-methylcarbamate (MTMC) wetting powder is 750 gram/hectares, the dosage of 40% Mobucin wetting powder is 600 gram/hectares, the dosage of 10% Nitenpyram aqua is 30 gram/hectares, and 5 days preventive effect is respectively 94.7%, 85.1%, 84.6% and 80.2% behind the medicine; 30 days preventive effect is respectively 93.8%, 70.4%, 69.5% and 86.9% behind the medicine.
The control efficiency of this prescription all is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 4:55% Nitenpyram meta-tolyl-N-methylcarbamate (MTMC) water-dispersible granules (1: 10)
Nitenpyram 5%
Meta-tolyl-N-methylcarbamate (MTMC) 50%
Sodium lignin sulfonate 3%
PO-EO block polyether 2%
Lauryl sodium sulfate 5%
Sodium carboxymethyl starch 3%
White carbon is mended to 100%
Mentioned component is through coarse crushing, and after mixing, comminution by gas stream becomes wetting powder, adds certain water again, fully mix, and extruder grain, the drying screening is mixed with 55% Nitenpyram meta-tolyl-N-methylcarbamate (MTMC) water-dispersible granules.
This prescription control vegetable aphid test, the contrast medicament is 25% meta-tolyl-N-methylcarbamate (MTMC) wetting powder (Chengdu Huangpai Cropscience Science Co., Ltd.) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spraying to handle.
This prescription dosage is 247.5 gram/hectares, and contrast medicament 25% meta-tolyl-N-methylcarbamate (MTMC) wetting powder dosage is 750 gram/hectares, and 10% Nitenpyram aqua dosage is 30 gram/hectares, and 5 days preventive effect is respectively 93.5%, 84.6% and 83.2% behind the medicine; 30 days preventive effect is respectively 94.1%, 70.6% and 83.8% behind the medicine.
The control efficiency of this prescription is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 5:21.5% Nitenpyram meta-tolyl-N-methylcarbamate (MTMC) missible oil (1: 13.3)
Nitenpyram 1.5%
Meta-tolyl-N-methylcarbamate (MTMC) 20%
N-Methyl pyrrolidone 3%
The newborn 600# 2% of farming
Nongru-700 # 2%
Acetone is mended to 100%
Mentioned component is added in the mixing kettle, after mixing, make 21.5% Nitenpyram meta-tolyl-N-methylcarbamate (MTMC) missible oil.
This prescription control cotton aphid test, the contrast medicament is 20% meta-tolyl-N-methylcarbamate (MTMC) missible oil (Dongguan City, Guangdong Province Rui Defeng bio tech ltd) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spraying to handle.
This prescription dosage is 258 gram/hectares, and contrast medicament 20% meta-tolyl-N-methylcarbamate (MTMC) missible oil dosage is 630 gram/hectares, and 10% Nitenpyram aqua dosage is 30 gram/hectares, and 5 days preventive effect is respectively 95.3%, 82.6% and 77.8% behind the medicine; 30 days control efficiency is respectively 90.8%, 68.2% and 85.4% behind the medicine.
The control efficiency of this prescription is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 6:25% Nitenpyram Mobucin Bassa microemulsion (1:
1+3)
Nitenpyram 5%
Mobucin 5%
Bassa 15%
Emulsifier 1602# 4%
Emulsifier 500# 2%
N-Methyl pyrrolidone 4%
Isopropyl alcohol 6%
Dimethylbenzene 3%
Water is mended to 100%
Mentioned component is added in the mixing kettle, shear, be mixed with 25% Nitenpyram Mobucin Bassa microemulsion through fully stirring.
This prescription control paddy rice thrips test, the contrast medicament is 20% Mobucin missible oil (Shilou County, Fanyu, Guangdong Province Fine Chemical Works), 20% Bassa microemulsion (Shenzhen Nuopuxin Agricultural Chemical Co., Ltd) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spraying to handle.
The dosage of this prescription is 120 gram/hectares, the dosage of contrast medicament 20% Mobucin missible oil is 600 gram/hectares, the dosage of 20% Bassa microemulsion is 600 gram/hectares, the dosage of 10% Nitenpyram aqua is 30 gram/hectares, and 5 days preventive effect is respectively 95.3%, 84.2%, 82.6% and 77.8% behind the medicine; 30 days control efficiency is respectively 96.3%, 71.0%, 69.2% and 84.2% behind the medicine.
The control efficiency of this prescription is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 7:52.5% Nitenpyram Bassa missible oil (1: 20)
Nitenpyram 2.5%
Bassa 50%
N-Methyl pyrrolidone 3%
The newborn 600# 2% of farming
Nongru-700 # 2%
Dimethylbenzene is mended to 100%
Mentioned component is added in the mixing kettle, after mixing, make 52.5% Nitenpyram Bassa missible oil.
This prescription control rice fulgorid test, the contrast medicament is 80% Bassa missible oil (Shenzhen Nuopuxin Agricultural Chemical Co., Ltd) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spraying to handle.
This prescription dosage is 394 gram/hectares, and contrast medicament 80% Bassa missible oil dosage is 600 gram/hectares, and 10% Nitenpyram aqua dosage is 30 gram/hectares, and 5 days preventive effect is respectively 94.0%, 82.1% and 80.8% behind the medicine; 30 days control efficiency is respectively 93.6%, 68.0% and 83.9% behind the medicine.
The control efficiency of this prescription is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 8:45% Nitenpyram dimethyl phenyl carbamate missible oil (1: 8)
Nitenpyram 5%
Dimethyl phenyl carbamate 40%
N-Methyl pyrrolidone 3%
Castor oil polyoxyethylene ether 2%
Nongru-700 # 2%
Dimethylbenzene is mended to 100%
Mentioned component is added in the mixing kettle, after fully mixing, make 45% Nitenpyram dimethyl phenyl carbamate missible oil.
This prescription control Chinese cabbage flea beetle test, contrast medicament are 50% dimethyl phenyl carbamate missible oil (the many and chemical industry Co., Ltd in Jiangxi) and 10% Nitenpyram aqua (Jiangsu Lianyungang Liben Agro-chemical Co., Ltd.).Test adopts spraying to handle.
This prescription dosage is 202.5 gram/hectares, and contrast medicament 50% dimethyl phenyl carbamate missible oil dosage is 750 gram/hectares, and 10% Nitenpyram aqua dosage is 30 gram/hectares, and 5 days preventive effect is respectively 95.0%, 85.6% and 82.8% behind the medicine; 30 days control efficiency is respectively 94.7%, 70.5% and 84.3% behind the medicine.
The control efficiency of this prescription is better than single agent kind, and dosage reduces, and synergistic effect is obvious, and quick-acting is good, and the lasting period is long.
Embodiment 9:51% Nitenpyram Bassa dimethyl phenyl carbamate missible oil (1:
25+25)
Nitenpyram 1%
Bassa 25%
Dimethyl phenyl carbamate 25%
N-Methyl pyrrolidone 3%
Castor oil polyoxyethylene ether 2%
Nongru-700 # 2%
Dimethylbenzene is mended to 100%
Mentioned component is added in the mixing kettle, after fully mixing, make 51% Nitenpyram Bassa dimethyl phenyl carbamate missible oil.
Claims (6)
1, a kind of Pesticidal combination is characterized in that active component is made up of Nitenpyram and carbamate insecticide, and the ratio of quality and the number of copies of Nitenpyram and carbamate insecticide is at 1:1-1:50.
2, according to claim 1, the ratio of quality and the number of copies of Nitenpyram and carbamate insecticide is 1:1-1:20.
3, the carbamate insecticide of mentioning in the claim 1 comprises at least a in Mobucin, meta-tolyl-N-methylcarbamate (MTMC), Bassa, dimethyl phenyl carbamate and the Aphox.
4, according to claim 1 or 2, the total content that it is characterized in that active ingredient in the composition is 5-80%.
5, according to claim 1 or 2, it is characterized in that Nitenpyram and carbamate insecticide are composite, be processed into acceptable any one formulation in the agricultural chemicals application, preferred formulation is wetting powder, aqueous emulsion, missible oil, microemulsion, water dispersible granules or tablet, suspending agent.
6, a kind of Pesticidal combination is used to prevent and treat the insect on the plant, especially is suitable for preventing and treating insects such as plant hopper, leafhopper and thrips, more specifically is suitable for preventing and treating the insects such as water rice hopper, leafhopper and thrips that produced resistance.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2008101907400A CN101444211A (en) | 2008-12-27 | 2008-12-27 | Synergy desinsection composite containing anabasine compound and application thereof |
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| CNA2008101907400A CN101444211A (en) | 2008-12-27 | 2008-12-27 | Synergy desinsection composite containing anabasine compound and application thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102197807A (en) * | 2011-03-31 | 2011-09-28 | 上海生农生化制品有限公司 | Cycloxaprid wettable powder and preparation method thereof |
| CN103250742A (en) * | 2013-05-23 | 2013-08-21 | 苏州谷力生物科技有限公司 | Pesticide composition |
| CN106818757A (en) * | 2017-02-15 | 2017-06-13 | 江苏克胜集团股份有限公司 | Mechanization preventing and treating auxiliary agent and its production method of a kind of anabasine agricultural chemical insecticide |
-
2008
- 2008-12-27 CN CNA2008101907400A patent/CN101444211A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102197807A (en) * | 2011-03-31 | 2011-09-28 | 上海生农生化制品有限公司 | Cycloxaprid wettable powder and preparation method thereof |
| CN103250742A (en) * | 2013-05-23 | 2013-08-21 | 苏州谷力生物科技有限公司 | Pesticide composition |
| CN103250742B (en) * | 2013-05-23 | 2014-08-06 | 苏州谷力生物科技有限公司 | Pesticide composition |
| CN106818757A (en) * | 2017-02-15 | 2017-06-13 | 江苏克胜集团股份有限公司 | Mechanization preventing and treating auxiliary agent and its production method of a kind of anabasine agricultural chemical insecticide |
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Open date: 20090603 |