CN101435155B - Nano silver antibacterial health care canton gaze gambiered silk and finishing method thereof - Google Patents
Nano silver antibacterial health care canton gaze gambiered silk and finishing method thereof Download PDFInfo
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- CN101435155B CN101435155B CN2007101245720A CN200710124572A CN101435155B CN 101435155 B CN101435155 B CN 101435155B CN 2007101245720 A CN2007101245720 A CN 2007101245720A CN 200710124572 A CN200710124572 A CN 200710124572A CN 101435155 B CN101435155 B CN 101435155B
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Abstract
The invention belongs to the technical field of fabric dyeing and finishing and provides nano-silver antibacterial health-care Canton gauze gambiered silk and a finishing method thereof. The nano-silver antibacterial health-care Canton gauze gambiered silk is made by the following steps: greig is repeatedly dipped with Dioscorea cirrhosa juice for a plurality of times, and is aired, treated by mud, washed and dried by fog-spreading, the Dioscorea cirrhosa juice is added with nano-silver, and silver content in the finished product, silk, is 70 to 100mg/kg. The Canton gauze gambiered silk has antibacterial performance with broad spectrum, can kill more than 650 types of noxious bacteria within a few minutes, has lasting antibacterial performance, can promote the healing of wound of the skin, the growth of cells and the repair of damaged cells, and has the health-care function.
Description
Technical field
The present invention relates to yarn silk fabric fabric and dyeing and finishing method thereof, relate in particular to a kind of nano silver antibacterial health care Canton gauze gambiered silk fabric and method for sorting thereof.
Background technology
The Canton gauze gambiered silk fabric, have another name called gambiered Guangdong gauze, it is Guangdong traditional handicraft famous-object, it is to contaminate greig by dye yam juice, is coated with envelope by the river bed mineral mud that is rich in iron ion then, treats that iron ion in the shale and the tannic acid in other biochemistry composition and the dye yam juice fully react, generated the tannic acid of black ferrous after, tremble and take off pond sludge, clean up, just become that face is yellow in black, the gambiered Guangdong gauze of glossy flicker.The production procedure of traditional gambiered Guangdong gauze is: greig → concise → soak dye yam juice → airing → repeat is above-mentioned soaks solarization process multipass → kiering → repeatedly wash and shines Liang juice → kiering again → repeatedly wash again and shine Liang juice → boil → dry → cross mud → wash → dry → spread out mist → tentering → self-contained.It is about 30% that fabric thickness after treatment increases, and weight increases about 40%.
The antibacterial and mouldproof finishing technique of textiles is very important and the textile finishing content of development prospect is arranged that along with the raising of social civilization degree, people require to have the weaving new product of antibacterial deodourizing health care function day by day.Traditional gambiered Guangdong gauze is as a kind of famous and precious garment material, and is inadequate at aspects such as antibiotic, mildew-resistant, health cares, can not satisfy the needs of high-end consumers.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, a kind of Canton gauze gambiered silk fabric with antibiotic, mildew-resistant, health care function and preparation method thereof is provided.
The technical scheme that realizes the object of the invention is:
A kind of nano silver antibacterial health care Canton gauze gambiered silk fabric, by greig through repeatedly flood dye yam juice and airing repeatedly, cross mud, washing and stand mist dry and make, it is characterized in that: be added with Nano Silver in the dye yam juice, silver content is 70～100mg/kg in the finished product yarn silk fabric.
In a kind of optimized technical scheme, silver content is 80～85mg/kg in the finished product yarn silk fabric.
As the present invention on the other hand, provide a kind of method for sorting of nano silver antibacterial health care Canton gauze gambiered silk fabric, comprise the steps:
(1) the dye yam stem tuber is pulverized, the water extraction and the filtration that add 1～5 times of its quality obtain dye yam Normal juice;
(2) add Nano Silver 1% aqueous solution of 0.3～0.8kg in every 100kg dye yam Normal juice, mix, obtain Nano Silver dye yam juice;
(3) greig was flooded 3～5 minutes in Nano Silver dye yam juice, greig fully, evenly absorbs Nano Silver potato gelsemium juice;
(4) the silk tentering after contaminating is tiled on the meadow with 25～40 ℃ of daylight airings, floods by (3) after drying again, and dries again, 30～40 times so repeatedly, obtains the semi-finished product of pale brown look;
(5) mix and be polished into mud by mixing sander with being rich in high price iron ion mineral mud, the semi-finished product front evenly is coated with the mud of the thick 0.5～1.5mm of last layer, and will be coated with mud in the face of the folding divide, make tannic acid and high price iron ion reaction 0.5～1.5 hour in the dye yam juice on the silk, yellow Canton gauze gambiered silk fabric in formation face is black;
(6) with cold water the Canton gauze gambiered silk fabric is cleaned up, spread out on the meadow in mist, even up, behind fog, dry by daylight again and get product.
Beneficial effect of the present invention: have the broad-spectrum sterilization performance, can kill more than 650 kind of harmful bacteria in several minutes, anti-microbial property is lasting; Can promote the healing of skin wound, the growth of cell and the reparation of damaged cell, have health care.
The specific embodiment
Employed dye yam is the stem tuber of Dioscoreaceae plant dye yam (Dioscorea cirrhosaLour.) among the present invention, and it contains polyphenol and the tannin that is easy to oxidative deformation generation freezing action in a large number.
Preferred use particle diameter is antibiotic raw material at the water white transparency Nano silver solution of 0.2～0.4nm among the present invention, and this class nano-silver water solution can be bought by market, as buying from the positive nanometer in Shanghai, Shanghai Co., Ltd.
Describe the present invention below in conjunction with embodiment, but embodiment does not constitute any limitation of the invention.
Embodiment 1
The preparation of dye yam Normal juice: get the dye yam of 100kg, peeling is ground into particle about particle diameter 1mm with pulverizer, the clear water that adds 300kg with pulverize after the dye yam particle fully mix, filter and obtain dye yam Normal juice 347kg.
The preparation of Nano Silver dye yam juice: 100 kilograms of dye yam Normal juice are blended into 0.5 kilogram of particle diameter at 0.2～0.4nm Nano Silver, 1% aqueous solution, mix standby.
Contaminate: place Nano Silver dye yam juice dye vat to flood 3-5 minute the silk grey cloth, constantly stir in the process, greig is fully contaminated.
Airing: dye behind the gelsemium lining tentering is tiled in and use the natural daylight airing on the meadow, the front of lining is towards sun direct irradiation face, solar temperature is between 25-45 ℃, treat to use again after the cloth that dyes first dries with the quadrat method dipping, dry 30-40 time repeatedly, hold the 5-7 days time of continuing, average dyeing every day, airing 4-6 time.The openpore silk fabric promptly becomes the semi-finished product of pale brown look after potato gelsemium juice repeated multiple times is contaminated.
Cross mud:, be not subjected to carry out before the sun direct irradiation at 3-6 point in morning.To be rich in iron mineral mud and mix polishing formation slurry by mixing sander.With sweeping son (contact-making surface: diameter 25-50cm, wide 3-6cm, sweep the long 20-35cm of sub-hair) be stained with behind the mud oar in the front of semi-finished product lining of dying behind the gelsemium that tiling is evened up and carry out fast once or repeat to be coated with and sweep, allow the mud oar be conformable to fully, equably lining wait be coated with the mud face, thickness is about 1mm.
Color development: divide on sand ground after will being coated with the front doubling inwardly behind the mud, allow in the mud iron ion fully and the tannic acid in the potato gelsemium juice in lining front fully react, after about 1 hour of the course of reaction, the lining that has been coated with mud has been looked unfamiliar ferrous into the tannic acid of black, the tannic acid that brown composition is an oxidative deformation, like this, yellow gelsemium yarn silk shell fabric had just formed in a face was deceived.
Canton gauze gambiered silk fabric behind the color development is cleaned in cold water, the reacted mud of lining is cleaned up.Then having under the weather condition of mist, the finished product lining after cleaning up is being placed dry after evening up on the outdoor meadow, getting product.
Finished product gambiered Guangdong silk is compared weightening finish about 38% with greig.Physico-chemical analysis method with routine detects, and the content of silver is 82mg/kg in gambiered Guangdong silk silk fabric.Finished product Canton gauze gambiered silk fabric is through 50 washings, and anti-microbial property still keeps more than 99.9%.
Embodiment 2
Preparation process is identical with embodiment's 1, and wherein every 100kg dye yam is extracted dye yam juice with the 500kg clear water, and the content of silver is 70mg/kg in finished product gambiered Guangdong silk silk fabric.
Embodiment 3
Preparation process is identical with embodiment's 1, and wherein every 100kg dye yam is extracted dye yam juice with the 100kg clear water, and the content of silver is 98mg/kg in finished product gambiered Guangdong silk silk fabric.
Claims (4)
1. nano silver antibacterial health care Canton gauze gambiered silk fabric, is crossed mud, washing and stand mist then and is dried and make through repeatedly flooding dye yam juice and airing repeatedly by greig, and it is characterized in that: be added with Nano Silver in the dye yam juice, silver content is 70～100mg/kg in the finished product yarn silk fabric.
2. nano silver antibacterial health care Canton gauze gambiered silk fabric according to claim 1 is characterized in that: silver content is 80～85mg/kg in the finished product yarn silk fabric.
3. the method for sorting of a nano silver antibacterial health care Canton gauze gambiered silk fabric comprises the steps:
(1) the dye yam stem tuber is pulverized, the water extraction and the filtration that add 1～5 times of its quality obtain dye yam Normal juice;
(2) in every 100kg dye yam Normal juice, add 0.3～0.8kg Nano Silver, 1% aqueous solution, mix, obtain Nano Silver dye yam juice;
(3) greig was flooded 3～5 minutes in Nano Silver dye yam juice, greig fully, evenly absorbs Nano Silver potato gelsemium juice;
(4) the silk tentering after contaminating is tiled on the meadow with 25～40 ℃ of daylight airings, floods by (3) after drying again, and dries again, 30～40 times so repeatedly, obtains the semi-finished product of pale brown look;
(5) mix and be polished into mud by mixing sander with being rich in the iron ion mineral mud, the semi-finished product front evenly is coated with the mud of the thick 0.5～1.5mm of last layer, and will be coated with mud in the face of the folding divide, make tannic acid and high price iron ion reaction 0.5～1.5 hour in the dye yam juice on the silk, yellow Canton gauze gambiered silk fabric in formation face is black;
(6) with cold water the Canton gauze gambiered silk fabric is cleaned up, spread out on the meadow in mist, even up, behind fog, dry by daylight again and get product.
4. the method for sorting of nano silver antibacterial health care Canton gauze gambiered silk fabric according to claim 1 is characterized in that: adding be the nano-silver water solution of particle diameter at 0.2～0.4nm.
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| CN2007101245720A CN101435155B (en) | 2007-11-16 | 2007-11-16 | Nano silver antibacterial health care canton gaze gambiered silk and finishing method thereof |
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| CN2007101245720A CN101435155B (en) | 2007-11-16 | 2007-11-16 | Nano silver antibacterial health care canton gaze gambiered silk and finishing method thereof |
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| CN101435155A CN101435155A (en) | 2009-05-20 |
| CN101435155B true CN101435155B (en) | 2011-04-13 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8920850B2 (en) | 2010-06-02 | 2014-12-30 | Eco Product Group LLC | Antimicrobial colloidal silver products and method of making same |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2654431B1 (en) * | 2010-12-23 | 2019-10-02 | Eco Product Group LLC | Antimicrobial colloidal silver and gold products |
| CN102433736A (en) * | 2011-08-28 | 2012-05-02 | 佛山市中国地质大学研究院 | Environmentally friendly anti-bacterial fabric |
| CN103422363B (en) * | 2012-05-21 | 2015-09-02 | 深圳市梁子时装实业有限公司 | A kind of silk dyeing technique |
| CN106592213A (en) * | 2016-12-08 | 2017-04-26 | 佛山市中国地质大学研究院 | Modified tannin antibacterial finishing agent prepared from diosorea cirrhosa extract solution |
| CN107022909A (en) * | 2017-05-17 | 2017-08-08 | 万秦君 | A kind of colouring method of dye yam fabric |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1558016A (en) * | 2004-02-13 | 2004-12-29 | 黄德欢 | Preparation method of antibiotic textile carrying nano silver |
| CN101046067A (en) * | 2007-04-12 | 2007-10-03 | 苏州大学 | Process of dyeing silk with dye yam extract |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1558016A (en) * | 2004-02-13 | 2004-12-29 | 黄德欢 | Preparation method of antibiotic textile carrying nano silver |
| CN101046067A (en) * | 2007-04-12 | 2007-10-03 | 苏州大学 | Process of dyeing silk with dye yam extract |
Non-Patent Citations (1)
| Title |
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| 吴浩亮.漫话莨纱绸.《丝绸》.1999,(第7期),41－42. * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8920850B2 (en) | 2010-06-02 | 2014-12-30 | Eco Product Group LLC | Antimicrobial colloidal silver products and method of making same |
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