CN101297680B - Composite vitamin emulsion and preparation thereof - Google Patents
Composite vitamin emulsion and preparation thereof Download PDFInfo
- Publication number
- CN101297680B CN101297680B CN2008100528943A CN200810052894A CN101297680B CN 101297680 B CN101297680 B CN 101297680B CN 2008100528943 A CN2008100528943 A CN 2008100528943A CN 200810052894 A CN200810052894 A CN 200810052894A CN 101297680 B CN101297680 B CN 101297680B
- Authority
- CN
- China
- Prior art keywords
- vitamin
- water
- emulsion
- cobastab
- composite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Abstract
The invention discloses a compound vitamin emulsion and a preparation method thereof, aiming at providing a compound vitamin emulsion which can dissolve in water and is convenient for use and the preparation method thereof. The method includes the following steps: cooking oil is taken to dissolve fat-soluble vitamin A, vitamin D [3], and vitamin E in water bath which is at 70 DEG C, and then agitated and ground with Twain-80, span-85, and water into emulsion stroma; in addition, water is taken to dissolve vitamin C, vitamin K [3], vitamin B [1], vitamin B [2], folic acid, and pantothenic acidsodium; liquid prepared in the two steps is merged and agitated evenly, and then the compound vitamin emulsion of the invention is obtained. The compound vitamin emulsion prepared by the method of the invention can be mixed with water according to arbitrary proportion without lamination or precipitate, has simple operation and can be used industrially and automatically in batch in using process by users.
Description
Technical field
The present invention relates to a kind of composite vitamin emulsion and preparation method thereof.
Background technology
Vitamin is poultry one of the necessary micronutrient element of growing, and has important effect, and being deficient in vitamin to cause nutritive disease, and degradation under decreased growth, the resistance, vitamin play important effect in poultry farming, be widely used.
The vitamins product that uses all is solid product mostly now, occurs easily mixing uneven phenomenon when batch mixing, causes the vitamin supplement deficiency, and, use inconvenient.And liquid vitamin generally is divided into fat-soluble oily liquids and water miscible vitamin liquid, because fat-soluble liquid vitamin is water insoluble, and it is immiscible with water miscible vitamin liquid, come-up or sinkage are arranged in the time of in adding entry, make the vitamin supplement deficiency that causes in when drinking-water, and have excessive and cause the poisoning by vitamin phenomenon influences the growth of poultry.
Summary of the invention
The present invention is in order to overcome weak point of the prior art, provide a kind of can be molten with water, composite vitamin emulsion easy to use and preparation method thereof.
The present invention is achieved through the following technical solutions:
A kind of composite vitamin emulsion is characterized in that, the consisting of of every 100L composite vitamin emulsion: vitamin A 10000～2,000,000,000 IU, vitamin D
31000～30,000 ten thousand IU, vitamin E 10～400,000 IU, vitamin C 100～1000g, vitamin K
3100～500g, Cobastab
120～100g, Cobastab
250～400g, folic acid 5～50g, sodium pantothenate 100～1000g, edible oil 100～2000ml, Tween-80 500～5000ml, Arlacel-85 100～1500ml, the water of surplus.
A kind of method of utilizing emulsifying technology to prepare above-mentioned composite vitamin emulsion is characterized in that, comprises the steps:
(1) get edible oil and dissolve fat-soluble vitamin 70 ℃ of water-baths, become creamy base with Tween-80, Arlacel-85, water agitation grinding again, described fat-soluble vitamin is vitamin A, vitamin D
3, vitamin E;
(2) vitamin C, vitamin K are dissolved in water intaking in addition
3, Cobastab
1, Cobastab
2, folic acid, sodium pantothenate;
(3) liquid of combining step (1) and step (2) preparation stirs, and promptly gets composite vitamin emulsion of the present invention.
The preferable of every 100L composite vitamin emulsion consists of: vitamin A 20000～1,800,000,000 IU, vitamin D
31500～25,000 ten thousand IU, vitamin E 15～350,000 IU, vitamin C 150～900g, vitamin K
3150～450g, Cobastab
125～90g, Cobastab
280～350g, folic acid 10～40g, sodium pantothenate 150～900g, edible oil 150～1800ml, Tween-80 600～4000ml, Arlacel-85 150～1300ml, the water of surplus.
The best group of every 100L composite vitamin emulsion becomes: vitamin A 1,000,000,000 IU, vitamin D
316,500 ten thousand IU, vitamin E 26.5 ten thousand IU, vitamin C 500g, vitamin K
3280g, Cobastab
155g, Cobastab
2200g, folic acid 27.6g, sodium pantothenate 440g, edible oil 1000ml, Tween-80 2000ml, Arlacel-85 700ml, the water of surplus.
The water that uses in the above-mentioned composite vitamin emulsion preferably adopts purified water.Edible oil preferably liquid vegetable oil such as soya-bean oil, peanut oil, palm wet goods.
The present invention has following technique effect:
Production method of the present invention is utilized emulsifying technology, with fat-soluble vitamin and water miscible vitamin is rationally organically tied and, utilize fat-soluble vitamin to adopt oil-in-water mode to be blended in the water uniformly with oil dissolving back, the characteristic of utilizing water soluble vitamin in water, to dissolve again, both are organically tied and, reach with water can be arbitrarily than the purpose of mixing, this product is evenly disperseed in water simultaneously, not stratified, mix easily, and, the vitamin A wide selection of colours and designs, nutritious, consumption is suitable.In user's use, simple to operate, industrialization in batches, automation are used.Can use to poultry by automatic drinking bowl, alleviate labour intensity greatly, the harmful effect of having avoided mixing inequality or layering and precipitating to bring simultaneously helps the growth of poultry.
The specific embodiment
Below in conjunction with specific embodiment to the detailed description of the invention.
Embodiment 1
1. get soya-bean oil 100ml at 70 ℃ of water-bath dissolving vitamin A 10,000 ten thousand IU, vitamin D
31,000 ten thousand IU, vitamin E 100,000 IU become creamy base with Tween-80 500ml, Arlacel-85 100ml, purified water 5000ml agitation grinding again.
2. get purified water 50L dissolving vitamin C 100g, vitamin K in addition
3100g, Cobastab
120g, Cobastab
250g, folic acid 5g, sodium pantothenate 100g.
3. the liquid of combining step 1 and step 2 preparation stirs, and mends purified water and promptly gets composite vitamin emulsion of the present invention to 100L.
Embodiment 2
1. get palm oil 2000ml at 70 ℃ of water-bath dissolving vitamin A 2,000,000,000 IU, vitamin D
330,000 ten thousand IU, vitamin E 400,000 IU, again with Tween-80 5000ml, Arlacel-85 1500ml, purified water 1 0000ml agitation grinding becomes creamy base.
2. the 50L that fetches water in addition dissolving vitamin C 1000g, vitamin K
3500g, Cobastab
1100g, Cobastab
2400g, folic acid 50g, sodium pantothenate 1000g.
3. the liquid of combining step 1 and step 2 preparation stirs, and moisturizing promptly gets composite vitamin emulsion of the present invention to 100L.
Embodiment 3
1. get soya-bean oil 150ml at 70 ℃ of water-bath dissolving vitamin A 20,000 ten thousand IU, vitamin D
31,500 ten thousand IU, vitamin E 150,000 IU, with Tween-80 600ml, Arlacel-85 150ml, purified water 5000ml agitation grinding becomes creamy base again.
2. get purified water 50L dissolving vitamin C 150g, vitamin K in addition
3150g, Cobastab
125g, Cobastab
280g, folic acid 10g, sodium pantothenate 150g.
3. the liquid of combining step 1 and step 2 preparation stirs, and mends purified water and promptly gets composite vitamin emulsion of the present invention to 100L.
Embodiment 4
1. get peanut oil 1800ml at 70 ℃ of water-bath dissolving vitamin A 1,800,000,000 IU, vitamin D
325,000 ten thousand IU, vitamin E 350,000 IU become creamy base with Tween-80 4000ml, Arlacel-85 1300ml, purified water 5000ml agitation grinding again.
2. get purified water 50L dissolving vitamin C 900g, vitamin K in addition
3450g, Cobastab
190g, Cobastab
2350g, folic acid 40g, sodium pantothenate 900g.
3. the liquid of combining step 1 and step 2 preparation stirs, and mends purified water and promptly gets composite vitamin emulsion of the present invention to 100L.
Embodiment 5
1. get soya-bean oil 1200ml at 70 ℃ of water-bath dissolving vitamin A 1,200,000,000 IU, vitamin D
318,000 ten thousand IU, vitamin E 250,000 IU become creamy base with Tween-80 2500ml, Arlacel-85 900ml, purified water 5000ml agitation grinding again.
2. get purified water 50L dissolving vitamin C 400g, vitamin K in addition
3300g, Cobastab
160g, Cobastab
2250g, folic acid 30g, sodium pantothenate 600g.
3. the liquid of combining step 1 and step 2 preparation stirs, and mends purified water and promptly gets composite vitamin emulsion of the present invention to 100L.
Embodiment 6
1. get palm oil 1000ml at 70 ℃ of water-bath dissolving vitamin A 1,000,000,000 IU, vitamin D
316,500 ten thousand IU, vitamin E 26.5 ten thousand IU become creamy base with Tween-80 2000ml, Arlacel-85 700ml, purified water 5000ml agitation grinding again.
2. get purified water 50L in addition, dissolve vitamin C 500g, vitamin K successively
3280g, Cobastab
155g, Cobastab
2200g, folic acid 27.6g, sodium pantothenate 440g.
3. the liquid of combining step 1 and step 2 preparation stirs, and mends purified water and promptly gets composite vitamin emulsion of the present invention to 100L.
Using method:
Can use to poultry by automatic drinking bowl, the ratio that adds vitamin emulsion in the water is 5/10000ths.
Prior art and preparation technology's of the present invention comparative result is as shown in table 1.
Table 1
| The compound multivitamin emulsion of liquid of the present invention | Conventional solid vitamin | Traditional liquid vitamin | |
| Kind | Composite vitamin emulsion is a kind of liquid | It is a kind of solid | Be generally two kinds of liquid, a kind of is the Water Soluble Compound multidimensional, and a kind of is oil-soluble AD oil |
| Mix with water | Can not precipitate than mixing by any, not stratified | Precipitation or layering take place in water insoluble or half molten water | A kind of is the Water Soluble Compound multidimensional, and oil-soluble AD oil is not dissolved in water, on the upper strata |
| The compound multivitamin emulsion of liquid of the present invention | Conventional solid vitamin | Traditional liquid vitamin | |
| Water fountain drinking-water | Do not fill in water pipe | Fill in water pipe easily | Do not fill in water pipe |
| General using method | Drinking-water | Spice | Drinking-water and spice combine |
| Different labour intensity by using method | Low | High | High |
| Mix uneven danger | Extremely low | High (pressing traditional-handwork mixes) | High |
Conclusion:
See in the use by table 1 that the B B-complex series products that the present invention is more traditional has remarkable advantages.
Claims (4)
1. a composite vitamin emulsion is characterized in that, the consisting of of every 100L composite vitamin emulsion: vitamin A 10000～2,000,000,000 IU, vitamin D
31000～30,000 ten thousand IU, vitamin E 10～400,000 IU, vitamin C 100～1000g, vitamin K
3100～500g, Cobastab
120～100g, Cobastab
250～400g, folic acid 5～50g, sodium pantothenate 100～1000g, edible oil 100～2000ml, Tween-80 500～5000ml, Arlacel-85 100～1500ml, the water of surplus; This composite vitamin emulsion adopts following preparation method to obtain:
(1) get edible oil and dissolve fat-soluble vitamin 70 ℃ of water-baths, become creamy base with Tween-80, Arlacel-85, water agitation grinding again, described fat-soluble vitamin is vitamin A, vitamin D
3, vitamin E;
(2) vitamin C, vitamin K are dissolved in water intaking in addition
3, Cobastab
1, Cobastab
2, folic acid, sodium pantothenate;
(3) liquid of combining step (1) and step (2) preparation stirs, and promptly gets composite vitamin emulsion of the present invention.
2. composite vitamin emulsion according to claim 1 is characterized in that, the consisting of of every 100L composite vitamin emulsion: vitamin A 20000～1,800,000,000 IU, vitamin D
31500～25,000 ten thousand IU, vitamin E 15～350,000 IU, vitamin C 150～900g, vitamin K
3150～450g, Cobastab
125～90g, Cobastab
280～350g, folic acid 10～40g, sodium pantothenate 150～900g, edible oil 150～1800ml, Tween-80 600～4000ml, Arlacel-85 150～1300ml, the water of surplus.
3. composite vitamin emulsion according to claim 2 is characterized in that, the consisting of of every 100L composite vitamin emulsion: vitamin A 1,000,000,000 IU, vitamin D
316,500 ten thousand IU, vitamin E 26.5 ten thousand IU, vitamin C 500g, vitamin K
3280g, Cobastab
155g, Cobastab
2200g, folic acid 27.6g, sodium pantothenate 440g, edible oil 1000ml, Tween-80 2000ml, Arlacel-85 700ml, the water of surplus.
4. composite vitamin emulsion according to claim 1 is characterized in that, used edible oil is a liquid vegetable oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100528943A CN101297680B (en) | 2008-04-25 | 2008-04-25 | Composite vitamin emulsion and preparation thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100528943A CN101297680B (en) | 2008-04-25 | 2008-04-25 | Composite vitamin emulsion and preparation thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101297680A CN101297680A (en) | 2008-11-05 |
| CN101297680B true CN101297680B (en) | 2010-11-03 |
Family
ID=40077738
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100528943A Expired - Fee Related CN101297680B (en) | 2008-04-25 | 2008-04-25 | Composite vitamin emulsion and preparation thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101297680B (en) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101874571B (en) * | 2009-11-20 | 2012-07-11 | 天津集合科技有限公司 | Vitamin composition sprayed on surface of pet cat food and spraying method thereof |
| CN101766261B (en) * | 2010-01-11 | 2011-09-28 | 广东大华农动物保健品股份有限公司 | Nano nutrient microemulsion and preparation method thereof |
| CN101797276B (en) * | 2010-03-15 | 2012-03-21 | 河南农业大学 | Compound vitamin nanoemulsion |
| CN101897386A (en) * | 2010-08-14 | 2010-12-01 | 施瑞客（天津）生物技术有限公司 | Fat-soluble liquid functional feed |
| CN102138638B (en) * | 2010-11-29 | 2013-03-13 | 北京永业民丰农业科技有限公司 | Animal nutrient solution and preparation method thereof |
| CN102100304B (en) * | 2011-01-12 | 2013-01-30 | 山东信得科技股份有限公司 | Fat-soluble vitamin nano microemulsion oral liquid and preparation method thereof |
| CN102552058B (en) * | 2011-12-27 | 2013-05-01 | 东南大学 | Compound vitamin lipid nanoparticle and preparation method thereof |
| CN102919547B (en) * | 2012-11-16 | 2013-12-18 | 石家庄市光华药业有限公司 | Traditional Chinese medicine liquid multivitamins and preparation process thereof |
| CN104224713A (en) * | 2014-09-17 | 2014-12-24 | 句容亿格纳米材料厂 | Vitamin B and vitamin K composite nanoemulsion as well as preparation method thereof |
| CN104304797B (en) * | 2014-10-30 | 2017-10-13 | 四川中农致远生物科技有限公司 | A kind of manufacturing process of livestock and poultry B B-complex nano-emulsion |
| CN105746929A (en) * | 2016-03-15 | 2016-07-13 | 济南大东农生物技术有限公司 | Poultry ultrafine molecular oil-emulsion vitamin complex and preparation method thereof |
| CN108391748A (en) * | 2018-02-07 | 2018-08-14 | 于长青 | A kind of liquid feed additive and preparation method thereof improving poultry intestinal health |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1175407A (en) * | 1996-07-31 | 1998-03-11 | 巴斯福股份公司 | Clear hydroalcoholic multivitamin solution containing physiologically effective amounts of beta-carotene |
| CN1179913A (en) * | 1996-10-14 | 1998-04-29 | 巴斯福股份公司 | Stable emulsions and dry powders of mixtures of fat-soluble vitamins, their preparation and use |
| CN1561967A (en) * | 2004-03-23 | 2005-01-12 | 毛一鹏 | Nano grade vitamin micro emulsion and its preparing method |
| CN1620278A (en) * | 2001-12-19 | 2005-05-25 | 陶氏康宁公司 | Stabilization of vitamins in water-in-silicone oil (W/O) emulsions |
| CN1875965A (en) * | 2006-06-29 | 2006-12-13 | 西北农林科技大学 | A micro-emulsion containing Vitamin C and Vitamin E and preparation method thereof |
| CN101095954A (en) * | 2006-06-30 | 2008-01-02 | 西北农林科技大学 | Transparent water oil-packaging type micro-emulsion stroma and method for preparing the same |
-
2008
- 2008-04-25 CN CN2008100528943A patent/CN101297680B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1175407A (en) * | 1996-07-31 | 1998-03-11 | 巴斯福股份公司 | Clear hydroalcoholic multivitamin solution containing physiologically effective amounts of beta-carotene |
| CN1179913A (en) * | 1996-10-14 | 1998-04-29 | 巴斯福股份公司 | Stable emulsions and dry powders of mixtures of fat-soluble vitamins, their preparation and use |
| CN1620278A (en) * | 2001-12-19 | 2005-05-25 | 陶氏康宁公司 | Stabilization of vitamins in water-in-silicone oil (W/O) emulsions |
| CN1561967A (en) * | 2004-03-23 | 2005-01-12 | 毛一鹏 | Nano grade vitamin micro emulsion and its preparing method |
| CN1875965A (en) * | 2006-06-29 | 2006-12-13 | 西北农林科技大学 | A micro-emulsion containing Vitamin C and Vitamin E and preparation method thereof |
| CN101095954A (en) * | 2006-06-30 | 2008-01-02 | 西北农林科技大学 | Transparent water oil-packaging type micro-emulsion stroma and method for preparing the same |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101297680A (en) | 2008-11-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101297680B (en) | Composite vitamin emulsion and preparation thereof | |
| CN101411410B (en) | Feedstuff additive for fattening river crab with red oil | |
| CN103271406B (en) | Compound amphiphilic core microcapsule electuary and preparation method thereof | |
| CN105580948A (en) | Instant coffee beverage and preparation method thereof | |
| CN106213004A (en) | A kind of egg duck feed and preparation method thereof | |
| CN105325749A (en) | Partridge shank chicken compound feed for preventing coccidiosis | |
| CN101336678A (en) | Premixing feeder capable of increasing pig growth rate and improving meat quality | |
| CN106071366A (en) | A kind of herb fermenting multienzyme somatotrophic Siniperca chuatsi feedstuff | |
| CN103622091B (en) | A kind of method utilizing hot pressed peanut meal to prepare peanut butter | |
| CN105941833A (en) | Feed capable of improving immunity of eleutheronema tetradactylum and preparation method of feed | |
| CN102511664B (en) | Fish oil feed additive and production method thereof | |
| CN104905012A (en) | Macrobrachium nipponensis disease-resistant Chinese herbal medicine fodder and processing method thereof | |
| CN104642817A (en) | Murray cod fish larvae compound feed and preparation method thereof | |
| CN105454733A (en) | Rainbow trout nutrition enhancer and application thereof | |
| CN101731562A (en) | Salt containing carotene and iodine and processing method thereof | |
| CN104224713A (en) | Vitamin B and vitamin K composite nanoemulsion as well as preparation method thereof | |
| CN108566987A (en) | It is a kind of to be conducive to protein solid beverage of the human body to calcium iron zinc-iron alloy solution | |
| CN105961914A (en) | Eleutheronema tetradactylum low fish meal environment-friendly feed, and preparation and application method thereof | |
| CN107494746A (en) | A kind of functional food for promoting skeleton development and preparation method thereof | |
| CN104642791A (en) | Penaeus vannamei boone formula feed suitable for freshwater aquaculture and preparation method thereof | |
| CN107183332A (en) | A kind of mutton sheep tea feed and preparation method thereof | |
| CN104839460A (en) | Beinong 1# laying hen feed preparation method | |
| CN101849670A (en) | Composite balancing nutritional agent | |
| CN102885232B (en) | The Chinese medicine additive of one boar food | |
| CN105341512A (en) | Feed enhancing disease resistance for pufferfish |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Composite vitamin emulsion and preparation thereof Effective date of registration: 20120925 Granted publication date: 20101103 Pledgee: Bank of Shanghai Limited by Share Ltd Tianjin branch Pledgor: Tianjin Shengji Group Co., Ltd. Registration number: 2012990000565 |
|
| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20131202 Granted publication date: 20101103 Pledgee: Bank of Shanghai Limited by Share Ltd Tianjin branch Pledgor: Tianjin Shengji Group Co., Ltd. Registration number: 2012990000565 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Composite vitamin emulsion and preparation thereof Effective date of registration: 20131202 Granted publication date: 20101103 Pledgee: Bank of Shanghai Limited by Share Ltd Tianjin branch Pledgor: Tianjin Shengji Group Co., Ltd. Registration number: 2013990000919 |
|
| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20151019 Granted publication date: 20101103 Pledgee: Bank of Shanghai Limited by Share Ltd Tianjin branch Pledgor: Tianjin Shengji Group Co., Ltd. Registration number: 2013990000919 |
|
| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20101103 Termination date: 20150425 |
|
| EXPY | Termination of patent right or utility model |