CN101284856A - Puerarin extractive technique and kudzuvine root beverage process - Google Patents
Puerarin extractive technique and kudzuvine root beverage process Download PDFInfo
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- CN101284856A CN101284856A CNA2008100711582A CN200810071158A CN101284856A CN 101284856 A CN101284856 A CN 101284856A CN A2008100711582 A CNA2008100711582 A CN A2008100711582A CN 200810071158 A CN200810071158 A CN 200810071158A CN 101284856 A CN101284856 A CN 101284856A
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- kudzu root
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Abstract
The invention provides a technology for extracting puerarin and a process for making kudzu root beverage. The technology for extracting puerarin adopts an ultrasonic multistage advection contact process to carry out extraction, wherein the contact process is as follows: the second stage and the third stage of a three-stage advection contact process for extracting kudzu root adopt ultrasonic wave to assist the extraction; the process for making kudzu root beverage comprises material selection, pretreatment and precooking; during extraction, the ultrasonic multistage advection contact process is adopted to extract kudzu root; finally, the extract is made into kudzu root beverage after centrifugation. The extracting technology is scientific and reasonable and has short extraction time, good effect and strong operability; when the technology is adopted to make kudzu root beverage, the process of the technology has low requirement on equipment and is easy to control along with strong operability, less energy consumption and low production cost; therefore, the technology is suitable for the large-scale production of kudzu root beverage; moreover, manufactured kudzu root beverage has abundant nutrition, convenient eating and delicious and various tastes; therefore, the technology has tremendous economic benefit.
Description
Technical field
The invention belongs to the beverage processing field, more specifically relate to a kind of puerarin extractive technique and kudzu root beverage technology.
Background technology
The root of kudzu vine (Radix Puerariae) is the root of legume pueraria lobata, is rich in isoflavones components puerarin, puerarin xyloside, daizeol, daidzin and β-Gu Zaichun, eicosanoic acid, contains volume starch again, and its pharmaceutical use and edibleness are high.It is cool in nature, and it is sweet, hot to distinguish the flavor of, and goes into lung, stomach, the spleen channel, lightly floats rise to loose, and the effect that have expelling pathogenic factors from muscles for reducing heat, promotes the production of body fluid to quench thirst have the good reputation of " Asia genseng ".The root of kudzu vine in Hunan of China, that output is economized in Guangdong, Fujian, Yunnan, Guizhou, Sichuan, Anhui etc. is bigger, can be for development and use.Tradition generally is directly edible or medicinal to the utilization of the root of kudzu vine, and its beneficiating ingredient puerarin etc. can not effectively utilize, and edible also inconvenient, taste is single; And now the extracting method of puerarin is generally decocting, alcohol extracting method, microwave-assisted extraction etc., but these technology exist extraction efficiency limited, extract shortcomings such as incomplete, be applied to kudzu root beverage process in effect also undesirable.
Summary of the invention
The purpose of this invention is to provide a kind of puerarin extractive technique and adopt this technology to prepare the technology of kudzu root beverage; This extractive technique is scientific and reasonable, and extraction time is short, effective, workable; Use this technology to produce kudzu root beverage, its technology is less demanding to equipment, is easy to control, and is workable, and power consumption is few, and production cost is low, is applicable to the scale operation of kudzu root beverage, and the kudzu root beverage of producing is nutritious, instant, features good taste has remarkable economic efficiency.
Puerarin extractive technique of the present invention is characterized in that: adopt the multistage advection contact process of ultrasonic wave to extract, the multistage advection contact process of described ultrasonic wave is: the second stage and the third stage of extracting puerarin three grades of advection contact processs are adopted ultrasonic-assisted extraction.
Employing puerarin extractive technique of the present invention prepares kudzu root beverage technology, comprise and select materials, pre-treatment, precook, it is characterized in that: adopt the multistage advection contact process of described ultrasonic wave that the root of kudzu vine is extracted at leaching process, after extracting solution is centrifugal, make kudzu root beverage through allotment.
Remarkable advantage of the present invention is:
(1) the present invention applies to ultrasonic wave in the multistage advection contact process extractive technique root of kudzu vine to be extracted, carry on the basis of touching the method extraction at three grades of advections, two-stage adopts ultrasonic-assisted extraction in the back, and the oscillating action that utilizes ultrasonic wave to produce is strengthened release, diffusion and the dissolving of puerarin in the root of kudzu vine cell; Extract the puerarin in the root of kudzu vine fully, extraction time is short, effective, simple to operate, and equipment requirements is low.
(2) this technology is applied to produce kudzu root beverage in the processing of kudzu root beverage, the production efficiency height, less demanding to equipment is easy to control, and be workable, and power consumption is few, is applicable to the scale operation of kudzu root beverage; Help comprehensive development and utilization root of kudzu vine resource, have remarkable economic efficiency and social benefit.
(3) the kudzu root beverage nutritive ingredient height that adopts the technology of the present invention to prepare, instant, taste is beautiful and various, and is beneficial to transportation and storage.
Description of drawings
Fig. 1 is the schema of multistage advection contact process extractive technique.
Fig. 2 is the schema of the multistage advection contact process of ultrasonic wave of the present invention extractive technique.
Wherein, L
0Be initial material (the 1st grade of charging); L
1It is the 2nd grade charging; L
2Charging for 3rd level; L
3It is the 4th grade charging; L
N-1It is the charging of n level; L
nFor having extracted discharging; S
1, S
2, S
3S
nBe respectively the 1st, 2,3 ... the n level is extracted the solvent that adds; V
1, V
2, V
3V
nBe respectively the 1st, 2,3 ... the extracting solution that the n level is extracted.
Fig. 3 is a kudzu root beverage preparation technology schema of the present invention.
Embodiment
Multistage advection contact process of the present invention is 3 grades, and the mass ratio of every grade of root of kudzu vine that extract to adopt and water is 1: 8～and 10, three grades extraction temperature is 60～70 ℃, and extraction time is 5～8min, and total time is 15～24min.
On the basis that three grades of advection contact processs are extracted, increase ultrasonic-assisted extraction, described partial hyperacoustic output specific power 0.02～0.022kw/kg water, hyperacoustic output specific power 0.02～0.025kw/kg water of the third stage in second and third two-stage; Three grades extraction temperature is 60～70 ℃, and extraction time is 5～8min.Total extraction time is 15～24min.
The kudzu root beverage preparation technology of the employing puerarin extractive technique of invention, concrete steps are:
(1) select materials: selecting the fresh root of kudzu vine is raw material;
(2) pre-treatment: comprise cleaning, section, oven dry; Wherein, slice thickness is 0.5～1.0cm; Smoke 14～18h in 55～65 ℃, make dry product water ratio≤15%;
(3) precook: the raw material of handling well is precooked, when making surface temperature reach 70 ℃ till;
(4) extract: adopt the auxiliary 3 grades of advection contact processs of ultrasonic wave to extract, and carry out centrifugal extracting solution;
(5) centrifugal: it is centrifugal to remove impurity to adopt supercentrifuge that the root of kudzu vine is extracted, and the rotating speed of whizzer is 8000rpm;
(6) allotment:, make kudzu root beverage with adding food flavouring in the root of kudzu vine filtrate.
Beverage according to required different taste in the allotment adds food flavouring, makes kudzu root beverage.
Described being allocated as: according to 8～9.5 parts of mass fraction root of kudzu vine filtrates, 0.08～0.12 part of licorice extract, 0.03～0.05 part of white sugar.
With described kudzu root beverage carry out tinning, seal, sterilization; The described mode of sealing behind 20～50kPa that is evacuated to that adopts of sealing; It is 10min that the heating-up time is adopted in described sterilization, and 116～121 ℃ of constant temperature sterilization 25～50min are cooled to below 40 ℃ through 20min.
Following embodiment further sets forth the present invention, but the present invention is not limited only to this:
Embodiment 1
Puerarin extracts
Multistage advection contact process is 3 grades, and the root of kudzu vine of every grade of extraction employing and the mass ratio of water are 1: 8, and three grades extraction temperature is 60 ℃, and extraction time is 5min, and total time is 15min.
On the basis that three grades of advection contact processs are extracted, increase ultrasonic-assisted extraction, described partial hyperacoustic output specific power 0.02kw/kg water, hyperacoustic output specific power 0.02kw/kg water of the third stage in second and third two-stage; Three grades extraction temperature is 60 ℃, and extraction time is 5min, and total extraction time is 15min.
Embodiment 2
Puerarin extracts
Multistage advection contact process is 3 grades, and the root of kudzu vine of every grade of extraction employing and the mass ratio of water are 1: 10, and three grades extraction temperature is 65 ℃, and extraction time is 7min, and total time is 21min.
On the basis that three grades of advection contact processs are extracted, increase ultrasonic-assisted extraction, described partial hyperacoustic output specific power 0.022kw/kg water, hyperacoustic output specific power 0.025kw/kg water of the third stage in second and third two-stage; Three grades extraction temperature is 65 ℃, and extraction time is 7min.Total extraction time is 21min.
Embodiment 3
Puerarin extracts
Multistage advection contact process is 3 grades, and the root of kudzu vine of every grade of extraction employing and the mass ratio of water are 1: 9, and three grades extraction temperature is 70 ℃, and extraction time is 8min, and total time is 24min.
On the basis that three grades of advection contact processs are extracted, increase ultrasonic-assisted extraction, described partial hyperacoustic output specific power 0.021kw/kg water, hyperacoustic output specific power 0.023kw/kg water of the third stage in second and third two-stage; Three grades extraction temperature is 65 ℃, and extraction time is 8min.Total extraction time is 24min.
Embodiment 4
Kudzu root beverage
(1) select materials: selecting the fresh root of kudzu vine is raw material;
(2) pre-treatment: comprise cleaning, section, oven dry; Wherein, slice thickness is 0.5～1.0cm; Smoke 18h in 65 ℃, make dry product water ratio≤15%;
(3) precook: the raw material of handling well is precooked, when making surface temperature reach 70 ℃ till;
(4) extract: adopt the auxiliary 3 grades of advection contact processs of ultrasonic wave to extract, and carry out centrifugal extracting solution;
(5) centrifugal: it is centrifugal to remove impurity to adopt supercentrifuge that the root of kudzu vine is extracted, and the rotating speed of whizzer is 8000rpm;
(6) allotment:, make kudzu root beverage with adding food flavouring in the root of kudzu vine filtrate.
Beverage according to required different taste in the described allotment adds food flavouring, makes kudzu root beverage.
Described being allocated as: according to 8 parts of massfraction root of kudzu vine filtrates, 0.08 part of licorice extract, 0.03 part of white sugar.
With described kudzu root beverage carry out tinning, seal, sterilization; The described mode of sealing behind the 50kPa that is evacuated to that adopts of sealing; It is 10min that the heating-up time is adopted in described sterilization, and 121 ℃ of constant temperature sterilization 50min are cooled to below 40 ℃ through 20min.
Embodiment 5
Kudzu root beverage
(1) select materials: selecting the fresh root of kudzu vine is raw material;
(2) pre-treatment: comprise cleaning, section, oven dry; Wherein, slice thickness is 1.0cm; Smoke 14～18h in 55 ℃, make dry product water ratio≤15%;
(3) precook: the raw material of handling well is precooked, when making surface temperature reach 70 ℃ till;
(4) extract: adopt the auxiliary 3 grades of advection contact processs of ultrasonic wave to extract, and carry out centrifugal extracting solution;
(5) centrifugal: it is centrifugal to remove impurity to adopt supercentrifuge that the root of kudzu vine is extracted, and the rotating speed of whizzer is 8000rpm;
(6) allotment:, make kudzu root beverage with adding food flavouring in the root of kudzu vine filtrate.
Beverage according to required different taste in the described allotment adds food flavouring, makes kudzu root beverage.
Described being allocated as: according to 8 parts of massfraction root of kudzu vine filtrates, 0.082 part of licorice extract, 0.05 part of white sugar.
With described kudzu root beverage carry out tinning, seal, sterilization; The described mode of sealing behind the 20kPa that is evacuated to that adopts of sealing; It is 10min that the heating-up time is adopted in described sterilization, and 116 ℃ of constant temperature sterilization 25min are cooled to below 40 ℃ through 20min.
Claims (8)
1. puerarin extractive technique is characterized in that: adopt the multistage advection contact process of ultrasonic wave to extract, the multistage advection contact process of described ultrasonic wave is: extract in the process of puerarin in multistage advection contact process, add ultrasonic-assisted extraction.
2. puerarin extractive technique according to claim 1, it is characterized in that: described multistage advection contact process is 3 grades, the mass ratio of every grade of root of kudzu vine that extract to adopt and water is 1: 8～and 10, three grades extraction temperature is 60～70 ℃, extraction time is 5～8min, and total time is 15～24min.
3. puerarin extractive technique according to claim 2, it is characterized in that: on the basis that three grades of advection contact processs are extracted, increase ultrasonic-assisted extraction in second and third two-stage, described partial hyperacoustic output specific power 0.02～0.022kw/kg water, hyperacoustic output specific power 0.02～0.025kw/kg water of the third stage; Three grades extraction temperature is 60～70 ℃, and extraction time is 5～8min.Total extraction time is 15～24min.
4. the kudzu root beverage preparation technology of employing such as claim 1,2 or 3 described puerarin extractive techniques, comprise and select materials, pre-treatment, precook, it is characterized in that: adopt the multistage advection contact process of described ultrasonic wave that the root of kudzu vine is extracted at leaching process, after extracting solution is centrifugal, make kudzu root beverage through allotment.
5. kudzu root beverage preparation technology according to claim 4 is characterized in that: the concrete steps of described technology are:
(1) select materials: selecting the fresh root of kudzu vine is raw material;
(2) pre-treatment: comprise cleaning, section, oven dry; Wherein, slice thickness is 0.5～1.0cm; Smoke 14～18h in 55～65 ℃, make dry product water ratio≤15%;
(3) precook: the raw material of handling well is precooked, when making surface temperature reach 70 ℃ till;
(4) extract: adopt the auxiliary 3 grades of advection contact processs of ultrasonic wave to extract, and carry out centrifugal extracting solution;
(5) centrifugal: it is centrifugal to remove impurity to adopt supercentrifuge that the root of kudzu vine is extracted, and the rotating speed of whizzer is 8000rpm;
(6) allotment:, make kudzu root beverage with adding food flavouring in the root of kudzu vine filtrate.
6. according to claim 4 or 5 described kudzu root beverage preparation technologies, it is characterized in that: the beverage according to required different taste in the described allotment adds food flavouring, makes kudzu root beverage.
7. kudzu root beverage preparation technology according to claim 6 is characterized in that: described being allocated as: according to 8～9.5 parts of mass fraction root of kudzu vine filtrates, and 0.08～0.12 part of licorice extract, 0.03～0.05 part of white sugar.
8. kudzu root beverage preparation technology according to claim 5 is characterized in that: with described kudzu root beverage carry out tinning, seal, sterilization; The described mode of sealing behind 20～50kPa that is evacuated to that adopts of sealing; It is 10min that the heating-up time is adopted in described sterilization, and 116～121 ℃ of constant temperature sterilization 25～50min are cooled to below 40 ℃ through 20min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2008100711582A CN101284856B (en) | 2008-06-02 | 2008-06-02 | Puerarin extractive technique and kudzuvine root beverage process |
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| CN2008100711582A CN101284856B (en) | 2008-06-02 | 2008-06-02 | Puerarin extractive technique and kudzuvine root beverage process |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102178306A (en) * | 2011-06-08 | 2011-09-14 | 许江林 | Method for producing kudzuvine root plant drink |
| CN103141905A (en) * | 2013-04-03 | 2013-06-12 | 重庆市万州区食品工业研究所 | Kudzuvine root nutritive drinks and manufacture method thereof |
| CN103204848A (en) * | 2012-01-11 | 2013-07-17 | 随州市康汇保健品有限公司 | Method for extracting puerarin |
| CN103444964A (en) * | 2013-10-01 | 2013-12-18 | 汪盛明 | Kudzu root bao beverage |
| CN103494287A (en) * | 2013-10-18 | 2014-01-08 | 重庆市万州区食品工业研究所 | Kudzuvine root week-base water and preparation method thereof |
| CN104757679A (en) * | 2015-04-14 | 2015-07-08 | 宁波可口生物工程有限公司 | Kudzuvine root beverage containing nicotinic acid |
| CN109315657A (en) * | 2018-09-29 | 2019-02-12 | 广州天天有财付网络科技有限公司 | A kind of pueraria lobata mulse and preparation method thereof |
| CN114097967A (en) * | 2021-10-22 | 2022-03-01 | 湖南张家界九天生物科技有限责任公司 | Kudzu vine root beverage |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1186636A (en) * | 1996-12-30 | 1998-07-08 | 湖南张家界市食品厂 | Kudzuvine root drink and its producing method |
| CN1927230B (en) * | 2006-09-06 | 2010-05-12 | 成都信息工程学院 | Process for extracting and purifying resin from traditional Chinese medicine by ultrasonic |
-
2008
- 2008-06-02 CN CN2008100711582A patent/CN101284856B/en not_active Expired - Fee Related
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102178306A (en) * | 2011-06-08 | 2011-09-14 | 许江林 | Method for producing kudzuvine root plant drink |
| CN103204848A (en) * | 2012-01-11 | 2013-07-17 | 随州市康汇保健品有限公司 | Method for extracting puerarin |
| CN103141905A (en) * | 2013-04-03 | 2013-06-12 | 重庆市万州区食品工业研究所 | Kudzuvine root nutritive drinks and manufacture method thereof |
| CN103444964A (en) * | 2013-10-01 | 2013-12-18 | 汪盛明 | Kudzu root bao beverage |
| CN103494287A (en) * | 2013-10-18 | 2014-01-08 | 重庆市万州区食品工业研究所 | Kudzuvine root week-base water and preparation method thereof |
| CN104757679A (en) * | 2015-04-14 | 2015-07-08 | 宁波可口生物工程有限公司 | Kudzuvine root beverage containing nicotinic acid |
| CN109315657A (en) * | 2018-09-29 | 2019-02-12 | 广州天天有财付网络科技有限公司 | A kind of pueraria lobata mulse and preparation method thereof |
| CN114097967A (en) * | 2021-10-22 | 2022-03-01 | 湖南张家界九天生物科技有限责任公司 | Kudzu vine root beverage |
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| CN101284856B (en) | 2012-03-21 |
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