CN101258907B - Barley green formula and preparation technique thereof - Google Patents
Barley green formula and preparation technique thereof Download PDFInfo
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- CN101258907B CN101258907B CN2008100608806A CN200810060880A CN101258907B CN 101258907 B CN101258907 B CN 101258907B CN 2008100608806 A CN2008100608806 A CN 2008100608806A CN 200810060880 A CN200810060880 A CN 200810060880A CN 101258907 B CN101258907 B CN 101258907B
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Abstract
The present invention relates to a barley greeg composition and a preparation process thereof. The barley barley greeg composition comprises the raw materials by weight percentage as follows: 82-95 percent of barley green powder and 5-18 percent of extract of edible cactus; wherein, the barley green powder is the extract of tender leaves of the fresh barley; and the extract of the edible cactus is the extract of opuntia milpa alta, the extracting proportion of the extract of opuntia milpa alta and the fresh cactus by weight ratio is 1:20 to 1:40. The preparation process comprises the following steps: the barley green powder and the extract of the edible cactus are weighted according to the weight ratio, then the two extracts are well mixed and stirred by adopting the method of equal quantity increasing and infiltration stirring; the obtained mixture is granulated and then placed in an oven to be dried for 3.5-5 hours and the moisture content is controlled in 3-4 percent; then the dried mixture passes through the steps of inspecting, screening, tabletting, sterilizing, thus the product is obtained after encapsulation. The barley green prescription of the invention has the advantages of no chemical composition, obviously improved oxidation resistance and stability, more complete and richer nutrition and inhibition of reproduction of bacteria.
Description
Technical field
The present invention relates to a kind of Barley Greeg, especially a kind of Barley Greeg composition and preparation process thereof.
Background technology
At present, but the relevant product of domestic and Barley Greeg invention mainly contains rich board Barley Greeg and green fingers board Barley Greeg.The former patent No. is ZL95117689.7, and patent name is " wheat seedling powder preparation technology ", and the latter's the patent No. is " ZL99126689.7 ", patent name be a kind of Barley Greeg the preparation method ".
Need to prove, wheat seedling powder and Barley Greeg powder are two title notions in the sector, wheat seedling powder is barley seedling to be cleaned the direct oven dry in back grind the pulvis that forms, this pulvis contains a large amount of celluloses and thick polysaccharide, but hyperthermia drying process (more than 100 ℃) can cause its active nutrient component by heavy damage (as SOD, chlorophyll, Vc etc.); And Barley Greeg is after fresh barley seedling is squeezed out juice and filters out slag, carry out vacuum drying (or spraying) powder delivery under normal temperature or cryogenic conditions, the nutritional labeling of Barley Greeg powder is very abundant, but its proterties is extremely unstable, be easy to oxidized or make moist, it is bigger to store difficulty.
The Barley Greeg raw material that above-mentioned binomial patented technology is produced very has competitiveness in the international market, outstanding " sample " that can domestic at last Barley Greeg raw material.But also exist following defective with the Barley Greeg finished product (being mainly tablet) that this raw material preparation forms:
1, very easily become damp and rotten: owing to be rich in chlorophyll in the Barley Greeg, plant flavone, phytoprotein more than 30%, more than 20 kind of vitamin, kind of mineral matter and trace element surplus in the of 70, over two hundred kind of active nutrient components such as hundreds of enzyme, what take is the dehydration extraction process in addition, so extremely unstable (SOD especially wherein of its proterties, chlorophyll, Vc, compositions such as the sodium of free state), usually at the bigger China's southern area of humidity, take under the normal storage condition back, finished product Barley Greeg Kaifeng, often (needless to say whole bottle has been taken) color relation is obviously deepened green or blackish green in the two weeks by emerald green, as plum rain season, color relation blackening in ten days especially, Here it is makes moist and has absorbed the performance of excess moisture.The national standard of Barley Greeg moisture is≤6%, as long as moisture is controlled in 6%, its color relation can not deepen or turn black.In case make moist, will cause the quick breeding of bacterium, cause the total plate count of product to exceed standard.At present, under the prerequisite of not adding any chemical composition (as stabilizing agent and afterbirth), stability how to improve the Barley Greeg product has become the problem that the industry peer will face jointly.
Experiment shows: in the normal humidity environment about 70%, a 300mg Barley Greeg is placed desktop, examine and to find, its color just began to change gradually after 90 seconds, significant change promptly took place after 3 minutes, blackish green with regard to having become basically after 6～8 minutes, the complete blackening of color began to be clamminess after 25 minutes after 15 minutes.
2, the nutritional labeling ratio is easier to run off and is oxidized: the Barley Greeg that one bottle of harsh output is come carries out sealing after nutrition detects preservation (normally 24 months shelf-life of Barley Greeg in the industry), Kaifeng detection again after 7-8 month, can find that its main nutrient composition content has nearly lacked 1/4 when dispatching from the factory than just, especially the content of compositions such as Vc, Ve, SOD has almost reduced 1/3, and color is dark much when also dispatching from the factory than just.This is because itself just there is air to exist in the Packaging Bottle, there is the invisible slit of a large amount of naked eyes (because of vial is unfavorable for transportation and frangible) in the plastic bottle molecular structure medical in addition, that health products are special-purpose, make Barley Greeg can see through bottle and receive a spot of air, so as long as the holding time is long slightly, oxidative phenomena will take place in the unsettled active component of some in the Barley Greeg in this a spot of air, its part component content will be gradually by " sacrifice " in oxidized process,! When the phytoprotein in the Barley Greeg during, can produce adverse influence to human body because of severe oxidation generation sex change.
Summary of the invention
Technical problem to be solved by this invention provides does not a kind ofly add any chemical composition, significantly improves oxidation resistance and stability, makes nutrition abundanter more comprehensively and can suppress vegetative Barley Greeg composition and preparation process thereof.
The present invention addresses the above problem the technical scheme that is adopted: this Barley Greeg composition is formed by following raw materials by weight percent proportioning: Barley Greeg powder 82%～95%, cardoncillo extract 5～18%.
Barley Greeg powder of the present invention is fresh barley tender leaf extract.
Cardoncillo extract of the present invention is the Mibangta cactus extract, and the withdrawal ratio of itself and fresh cactus is weight ratio 1: 30.
The procedure of processing of the preparation process of this Barley Greeg composition is:
(1) weighs Barley Greeg powder and cardoncillo extract by weight percentage, take equivalent to increase progressively the infiltration paddling process both mixing and stirring;
(2) mixture of step (1) gained is granulated after, put into 51～55 ℃ drying in oven 3.5～5 hours, its moisture is controlled at 3～4%;
(3) test, sieve, compressing tablet, sterilization and encapsulation.
Equivalent of the present invention increase progressively the infiltration paddling process for the cardoncillo extract total amount of getting required adding earlier with after the Barley Greeg powder of equivalent mixes, evenly stirred 5～8 minutes, drop into again with the Barley Greeg powder of mixture equivalent is even and stirred 10～15 minutes, drop into even the stirring 15～20 minutes of Barley Greeg powder again with the mixture equivalent second time, increase by this times amount, until all mixing.
Barley Greeg powder of the present invention is fresh barley tender leaf extract.
Cardoncillo extract of the present invention is the Mibangta cactus extract, and the withdrawal ratio of itself and fresh cactus is weight ratio 1: 30.
The present invention compared with prior art has following beneficial effect:
(1) raw material of this Barley Greeg is Barley Greeg powder (fresh barley tender leaf extract) and cardoncillo extract, the inventor has successively selected over one hundred kind of (as aloe, pollen pini, spirulina, mulberry leaf etc.) plant material to carry out the test of proportioning preparation with Barley Greeg respectively, find opuntia milpa alta haw extract and the most suitable compatibility of Barley Greeg at last, and can reach thundering effect.
Cactus and barley seedling belong to thing cold in nature together, the risk that does not have restriction or checking relation in five elements, and fresh cactus withdrawal ratio is between weight ratio 1: 20～1: 40, optimum weight ratio is 1: 20～1: 30, the proportion of Radix et Caulis Opuntiae Dillenii extract and Barley Greeg is very approaching, and both have complementarity again in existing homogeney aspect nutritional labeling and the content.Cactus has extremely strong cold-resistant heat, anti-ability of invading and harassing, its molecular structure closely and very stable, the expert assert that all cactus has good moisture-resistant, antibacterial, radioresistance, anti-oxidant, the tonifying spleen of being good for the stomach, antifatigue effect both at home and abroad.These characteristics of cactus have just greatly strengthened the stability of Barley Greeg active component, help the nutrition of having pinned Barley Greeg, protect it oxidized no longer easily and cause the sex change of nutrient.Therefore this Barley Greeg composition has improved the Barley Greeg trophic structure and has formed the stable inadequately scarce property of proterties by adding the cardoncillo extract, has strengthened the humidity resistance and the oxidation resistance of Barley Greeg, makes it more relievedly to store.
(2) the cardoncillo extract weight percentage that is added is 5～18%, suitable cactus proportioning makes the nutritional labeling of this Barley Greeg product more reasonable than the Barley Greeg of single raw material, more comprehensively, more balanced, its Protein content and stability obviously promote, vitamin C, citrin, carrotene, calcium, iron, zinc, SOD, component contents such as flavones slightly increase, and newly-increased cactus saponin, Baobi lotus, cholla stem, compositions such as Kok Beattie cents, the Radix et Caulis Opuntiae Dillenii extract of low sodium has also suitably reduced the sodium content of Barley Greeg product simultaneously, more helps the health to human body.
The percentage by weight of cardoncillo extract is selected meticulously through the inventor, if the blanking ratio of cactus too high (as surpassing 18%), can obviously have influence on the content of composition such as chlorophyll in the Barley Greeg, destroy the property balanced in nutrition of Barley Greeg itself on the contrary, if the blanking ratio of cactus is on the low side (as being lower than 5%), that stability action that plays will be not enough.Confirm that by experiment the best blanking of cardoncillo extract is than between 8%-15%.This content value can fully guarantee the raising of Barley Greeg stability, can further improve the comprehensive and harmonious of Barley Greeg nutrition again.
(3) Radix et Caulis Opuntiae Dillenii extract self has antibiotic and the self-protection effect, can help to suppress the bacterial reproduction of Barley Greeg in storage, strengthens the Barley Greeg security of products.
(4) the maximum difference of this Barley Greeg manufacturing process and conventional Barley Greeg production is the drying time that has shortened in original technology.Conventional Barley Greeg needs 5 hours drying course approximately at 51-55 ℃ baking oven, be controlled at about 3-3.5% with the moisture with Barley Greeg, moisture in 24 months shelf-life does not finally exceed 6% because moisture only in this way just can be guaranteed Barley Greeg.After adding percentage by weight and be 5～18% Radix et Caulis Opuntiae Dillenii extract, whole drying course obviously shortens, and as adding the Radix et Caulis Opuntiae Dillenii extract of percentage by weight 10%, can shorten nearly 1 hour.This is because cactus has superpower stability and humidity-proof ability, the colloid molecular structure of cactus is more tight than Barley Greeg, its sequestering power can seal or dwindle the slit of tablet surface, stop the infiltration of moisture, Barley Greeg can easily be stored, and the shortening of drying time can reduce the loss of Barley Greeg nutritional labeling to a certain extent.
Stability experiment shows:
Be in about 75% the environment in air humidity, with cardoncillo extract weight percentage is that 10% Barley Greeg tablet (hereinafter to be referred as A) and 100% pure Barley Greeg tablet (hereinafter to be referred as B) are respectively got 2 and be exposed in the air, can find by observing, after about 90 seconds, the color of B begins to change gradually, and A does not observe change color under naked eyes, significant change has taken place in B after 3 minutes, B has just become blackish green basically after 6 minutes, and the color of A just slightly changes at this moment, the color of B is blackening fully after 13 minutes, and A rigidly connects and is bordering on blackish greenly, all deepen black after 23 minutes inside and outside the B and begin to be clamminess, and A surface deflection black just, and after pulling open tablet, significant change does not take place in the color of its interior profile basically.
The disintegration experiment shows:
Be in about 75% the environment in air humidity, with cardoncillo extract weight percentage is that 10% Barley Greeg tablet (hereinafter to be referred as A) and 100% pure Barley Greeg tablet (hereinafter to be referred as B) are respectively got 6 and inserted two respectively and simulated gastric fluid is housed (promptly gets watery hydrochloric acid 16.4ml, add about 800ml of water and pepsin 10g, after shaking up, thin up becomes 1000m1) container in (water temperature is 37 ℃ ± 1), evenly shake or rock.Make discovery from observation, A in 40 minutes all disintegrations be scattered in the solution, B then after 55 minutes the time just whole disintegrations be scattered in the solution.This experimental results show that human body has better assimilation effect for A.
The specific embodiment
Embodiment 1: the Barley Greeg preparation in the present embodiment is respectively 92% and 8% Barley Greeg powder and cardoncillo extract by percentage by weight and forms.
Procedure of processing is as follows: weigh 46 kilograms of Barley Greeg powder and 4 kilograms of cardoncillo extracts, the withdrawal ratio of cardoncillo extract and fresh cactus is 1: 40, increasing progressively the infiltration paddling process by equivalent stirs, equivalent increase progressively the infiltration paddling process for the cardoncillo extract total amount of getting required adding earlier with after the Barley Greeg powder of equivalent mixes, evenly stirred 5～8 minutes, drop into again with the Barley Greeg powder of mixture equivalent is even and stirred 10～15 minutes, last input more evenly stirred 15～20 minutes with the Barley Greeg powder of the mixture equivalent second time, increase by this times amount, until all mixing.Because both proportion is more approaching, therefore interpenetrate very easy.
Concrete whipping process mixes with 4 kilograms of Barley Greeg powder for getting 4 kilograms of cardoncillo extracts earlier, evenly stirred 5～8 minutes, obtain 8 kilograms of mixtures, dropping into 8 kilograms of Barley Greeg powder more evenly stirred 10～15 minutes, obtain 16 kilograms of mixtures, drop into again with 16 kilograms of Barley Greeg powder and evenly stirred 15～20 minutes, at last remaining 18 kilograms of Barley Greeg powder are all poured into, evenly stir.After mixture granulated according to a conventional method, put into 51-53 ℃ baking oven, drying time is 4 hours 20 minutes, and its moisture is controlled in 3～4%, test then, sieve, compressing tablet, sterilization and encapsulation, can get specification and be about 166666 of the emerald green Barley Greeg tablet of 300mg/ grain.
Barley Greeg powder in the present embodiment is fresh barley tender leaf extract, and the Radix et Caulis Opuntiae Dillenii extract is the Mibangta cactus extract.
This finished product is encapsulated into bottle two days later, open and seal aluminium foil, get in the environment that 2 Barley Greeg tablets are exposed to air humidity about 75%, examine, its color began to deepen gradually after 260 seconds, had become blackish greenly after 8 minutes, and the rear surface became black in 16 minutes, but pull open tablet, significant change does not take place in the color of its interior profile basically.
Embodiment 2: the Barley Greeg preparation in the present embodiment is respectively 90% and 10% Barley Greeg powder and cardoncillo extract by percentage by weight and forms.
Procedure of processing is as follows: weigh 45 kilograms of Barley Greeg powder and 5 kilograms of cardoncillo extracts, the withdrawal ratio of cardoncillo extract and fresh cactus is 1: 30, increasing progressively the infiltration paddling process by equivalent stirs, both proportion is more approaching, therefore interpenetrate very easy, equivalent increases progressively the detailed process of infiltration paddling process in embodiment 1 existing detailed description, no longer explanation herein.After mixture granulated according to a conventional method, put into 51-53 ℃ baking oven, drying time is 4 hours, its moisture is controlled in 3～4%, test then, sieve, compressing tablet, sterilization and encapsulation, can get specification is about 166666 of the emerald green Barley Greeg tablet (surface presents the variegated of a small amount of cactus) of 300mg/ grain.
Barley Greeg powder in the present embodiment is fresh barley tender leaf extract, and the Radix et Caulis Opuntiae Dillenii extract is the Mibangta cactus extract.
This finished product is encapsulated into bottle two days later, open and seal aluminium foil, getting 2 Barley Greeg tablets, to be exposed to air humidity be in about 75% the environment, examine, its color begins to deepen gradually near 300 seconds the time, has become blackish greenly behind 9 fens halfs, and the rear surface became black in 18 minutes, but pull open tablet, significant change does not take place in the color of its interior profile basically.
Embodiment 3: the Barley Greeg preparation in the present embodiment is respectively 88% and 12% Barley Greeg powder and cardoncillo extract by percentage by weight and forms.
Procedure of processing is as follows: weigh 44 kilograms of Barley Greeg powder and 6 kilograms of cardoncillo extracts, the withdrawal ratio of cardoncillo extract and fresh cactus is 1: 30, increasing progressively the infiltration paddling process by equivalent stirs, both proportion is more approaching, therefore interpenetrate very easy, equivalent increases progressively the detailed process of infiltration paddling process in embodiment 1 existing detailed description, no longer explanation herein.After mixture granulated according to a conventional method, put into 51-53 ℃ baking oven, drying time is 3 hours 45 minutes, its moisture is controlled in 3～4%, test then, sieve, compressing tablet, sterilization and encapsulation, can get specification is about 166666 of the emerald green Barley Greeg tablet (surface presents the variegated of tangible cactus) of 300mg/ grain.
Barley Greeg powder in the present embodiment is fresh barley tender leaf extract, and the Radix et Caulis Opuntiae Dillenii extract is the Mibangta cactus extract.
This finished product is encapsulated into bottle two days later, open and seal aluminium foil, getting 2 Barley Greeg tablets, to be exposed to air humidity be in about 75% the environment, examine, its color begins to deepen gradually after near 340 seconds, has become blackish greenly behind 11 fens halfs, and the rear surface became black in 21 minutes, but pull open tablet, significant change does not take place in the color of its interior profile basically.
Embodiment 4: the Barley Greeg preparation in the present embodiment is respectively 85% and 15% Barley Greeg powder and cardoncillo extract by percentage by weight and forms.
Procedure of processing is as follows: weigh 42.5 kilograms of Barley Greeg powder and 7.5 kilograms of cardoncillo extracts, the withdrawal ratio of cardoncillo extract and fresh cactus is 1: 20, increasing progressively the infiltration paddling process by equivalent stirs, both proportion is more approaching, therefore interpenetrate very easy, equivalent increases progressively the detailed process of infiltration paddling process in embodiment 1 existing detailed description, no longer explanation herein.After mixture granulated according to a conventional method, put into 51-53 ℃ baking oven, drying time is 3 hours 30 minutes, its moisture is controlled in 3～3.5%, test then, sieve, compressing tablet, sterilization and encapsulation, can get specification is about 166666 of the emerald green Barley Greeg tablet (surface presents the variegated of fairly obvious and uniform cactus) of 300mg/ grain.
Barley Greeg powder in the present embodiment is fresh barley tender leaf extract, and the Radix et Caulis Opuntiae Dillenii extract is the Mibangta cactus extract.
This finished product is encapsulated into bottle two days later, open and seal aluminium foil, getting 2 Barley Greeg tablets, to be exposed to air humidity be in about 75% the environment, examine, its color began to deepen gradually after 6 minutes, had become blackish greenly behind 13 fens halfs, and the rear surface became black in 24 minutes, but pull open tablet, significant change does not take place in the color of its interior profile basically.
Claims (7)
1. a Barley Greeg composition is characterized in that: formed by following raw materials by weight percent proportioning: Barley Greeg powder 82%～95%, cardoncillo extract 5～18%.
2. Barley Greeg composition according to claim 1 is characterized in that: described Barley Greeg powder is fresh barley tender leaf extract.
3. Barley Greeg composition according to claim 1 is characterized in that: described cardoncillo extract is the Mibangta cactus extract, and the withdrawal ratio of itself and fresh cactus is weight ratio 1: 30.
4. preparation process of Barley Greeg composition according to claim 1, it is characterized in that: procedure of processing is:
(1) weighs Barley Greeg powder and cardoncillo extract by weight percentage, take equivalent to increase progressively the infiltration paddling process both mixing and stirring;
(2) mixture of step (1) gained is granulated after, put into 51～55 ℃ drying in oven 3.5～5 hours, its moisture is controlled at 3～4%;
(3) test, sieve, compressing tablet, sterilization and encapsulation.
5. according to the preparation process of the described Barley Greeg composition of claim 4, it is characterized in that: described equivalent increase progressively the infiltration paddling process for the cardoncillo extract total amount of getting required adding earlier with after the Barley Greeg powder of equivalent mixes, evenly stirred 5～8 minutes, drop into again with the Barley Greeg powder of mixture equivalent is even and stirred 10～15 minutes, drop into even the stirring 15～20 minutes of Barley Greeg powder again with the mixture equivalent second time, increase by this times amount, until all mixing.
6. according to the preparation process of claim 4 or 5 described Barley Greeg compositions, it is characterized in that: described Barley Greeg powder is fresh barley tender leaf extract.
7. according to the preparation process of claim 4 or 5 described Barley Greeg compositions, it is characterized in that: described cardoncillo extract is the Mibangta cactus extract, and the withdrawal ratio of itself and fresh cactus is weight ratio 1: 30.
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| CN1208620A (en) * | 1997-08-15 | 1999-02-24 | 陈秀枢 | Composite contg. bacterium bifidum and lactobacillus |
| CN1225801A (en) * | 1998-02-09 | 1999-08-18 | 山东省生物药物研究所 | Compounded Mailusuo and preparation process thereof |
| CN1243747A (en) * | 1997-08-15 | 2000-02-09 | 北京建昊高科技股份有限公司 | Growth-promoting composition for bacteria useful to microecology of intestine |
| CN1372843A (en) * | 2002-03-21 | 2002-10-09 | 李华堂 | Synthetic organic nutrient |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1208620A (en) * | 1997-08-15 | 1999-02-24 | 陈秀枢 | Composite contg. bacterium bifidum and lactobacillus |
| CN1243747A (en) * | 1997-08-15 | 2000-02-09 | 北京建昊高科技股份有限公司 | Growth-promoting composition for bacteria useful to microecology of intestine |
| CN1225801A (en) * | 1998-02-09 | 1999-08-18 | 山东省生物药物研究所 | Compounded Mailusuo and preparation process thereof |
| CN1372843A (en) * | 2002-03-21 | 2002-10-09 | 李华堂 | Synthetic organic nutrient |
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Effective date of registration: 20170605 Address after: 448000, beside the village committee of four ridge village, Jingshan County, Jingmen, Hubei Patentee after: Hubei Liwei Honest biological science and Technology Co Ltd Address before: 310005, New River, Hangzhou, Zhejiang province 288 Gongshu District Road, apartment 4-802 Co-patentee before: Dong Guoren Patentee before: Gu Shouzhi Co-patentee before: Hao Weijiang |