CN101250343A - Polymer microsphere insulation heat-proof dry-powder paint - Google Patents
Polymer microsphere insulation heat-proof dry-powder paint Download PDFInfo
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- CN101250343A CN101250343A CNA2008100472435A CN200810047243A CN101250343A CN 101250343 A CN101250343 A CN 101250343A CN A2008100472435 A CNA2008100472435 A CN A2008100472435A CN 200810047243 A CN200810047243 A CN 200810047243A CN 101250343 A CN101250343 A CN 101250343A
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- 229920000642 polymer Polymers 0.000 title claims abstract description 63
- 239000004005 microsphere Substances 0.000 title claims abstract description 47
- 239000000843 powder Substances 0.000 title claims abstract description 40
- 238000009413 insulation Methods 0.000 title claims abstract description 25
- 239000003973 paint Substances 0.000 title claims abstract description 13
- 239000002245 particle Substances 0.000 claims abstract description 44
- 239000011521 glass Substances 0.000 claims abstract description 20
- 239000012510 hollow fiber Substances 0.000 claims abstract description 18
- 239000000919 ceramic Substances 0.000 claims abstract description 16
- 239000010451 perlite Substances 0.000 claims abstract description 16
- 235000019362 perlite Nutrition 0.000 claims abstract description 16
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 13
- 235000019353 potassium silicate Nutrition 0.000 claims abstract description 13
- 239000011734 sodium Substances 0.000 claims abstract description 13
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 13
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 239000000835 fiber Substances 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 14
- 239000000654 additive Substances 0.000 claims description 12
- 239000004816 latex Substances 0.000 claims description 12
- 229920000126 latex Polymers 0.000 claims description 12
- 239000011324 bead Substances 0.000 claims description 10
- 230000000996 additive effect Effects 0.000 claims description 6
- 239000005995 Aluminium silicate Substances 0.000 claims description 5
- 235000012211 aluminium silicate Nutrition 0.000 claims description 5
- 239000004743 Polypropylene Substances 0.000 claims description 4
- PZZYQPZGQPZBDN-UHFFFAOYSA-N aluminium silicate Chemical compound O=[Al]O[Si](=O)O[Al]=O PZZYQPZGQPZBDN-UHFFFAOYSA-N 0.000 claims description 4
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 4
- -1 polypropylene Polymers 0.000 claims description 4
- 229920001155 polypropylene Polymers 0.000 claims description 4
- 230000004888 barrier function Effects 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 5
- 238000010276 construction Methods 0.000 abstract description 2
- 238000005336 cracking Methods 0.000 abstract description 2
- 239000000839 emulsion Substances 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 239000011325 microbead Substances 0.000 abstract 2
- 230000003487 anti-permeability effect Effects 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000011148 porous material Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 description 21
- 239000011248 coating agent Substances 0.000 description 19
- 230000000694 effects Effects 0.000 description 9
- 229910000838 Al alloy Inorganic materials 0.000 description 6
- 230000001680 brushing effect Effects 0.000 description 6
- 238000007599 discharging Methods 0.000 description 6
- 238000012856 packing Methods 0.000 description 6
- 238000011109 contamination Methods 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 238000003776 cleavage reaction Methods 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 230000007017 scission Effects 0.000 description 2
- 239000004593 Epoxy Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 238000007720 emulsion polymerization reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012767 functional filler Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 239000012782 phase change material Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000010557 suspension polymerization reaction Methods 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Polymer microsphere thermal insulation dry powder paint is formed by raw material with following parts by weight of 20-40 water glass powder, 8-15 pore closed expansive perlite, 3-15 hollow glass or ceramic micro-bead, 10-30 polymer phase-change microsphere, 2-5 hollow fiber, 3-5 sodium fluosilicate, 5-10 emulsion powder and 5-10 water-proof anti-permeability addition agent, which shares the common characteristics of thermal resistance type and thermal capacity type materials, and has prominent weatherability and extremely excellent strain resistance. Hollow fiber provides excellent thermal insulation property, and largely increases the properties of pull-resistance, cracking resistance and breaking resistance at large amplitude. An excellent barrier layer is formed through the mutual gradation of hollow glass or ceramic micro-bead, hollow fiber and polymer microsphere and the like according to particle size, thereby largely increasing thermal insulating property. Dry powder supply is employed, which largely reduce transportation cost and storage cost, and is convenient for storing and transporting and construction.
Description
Technical field
The present invention relates to a kind of architectural decoration external and internal wall coating, especially a kind of polymer microsphere insulation heat-proof dry-powder paint.
Background technology
The heat preservation energy-saving of buildings receives publicity day by day in recent years, has wherein emerged a large amount of outstanding heat insulating products, and wherein major part is the product that belongs to the mortar class, excellent thermal insulation performance, with low cost and coating series products can widespread use is less.Chinese patent publication number: 101108930A, open day: on January 23rd, 2008, denomination of invention " a kind of aquosity heat insulating heat preserving paint and production method " has proposed employing elastomeric propylene acid modified emulsion, Resins, epoxy, ethylene glycol, hollow glass micropearl, functional filler, kaolin, talcum powder and other auxiliary agents are formulated and heat insulating coatings.Heat reflection and hollow insulating heat-blocking action that it utilizes hollow glass micropearl improve heat insulating effect, and the toxicity of coating is less, and energy saving is higher.But above-mentioned coating belongs to simple heat resistance type coating, and used heat preserving and insulating material is more single, and filming of hollow glass micropearl periphery is difficult to form the insulation barrier layer, and heat insulation effect is desirable not to the utmost; The weathering resistance and the contamination resistance of coating are relatively poor, and the tension resistance to cleavage also has much room for improvement.
Summary of the invention
It is perfect inadequately to the objective of the invention is to overcome existing thermal insulation coatings insulation barrier layer, weathering resistance and contamination resistance are relatively poor, defective that the tension splitting resistance is lower and deficiency, provide a kind of its to film and be easy to form good insulation barrier layer, weathering resistance, contamination resistance and tension resistance to cleavage are better, use and allocate polymer microsphere insulation heat-proof dry-powder paint easily.
Technical solution of the present invention is: a kind of polymer microsphere insulation heat-proof dry-powder paint, raw material by following weight part is formed: water glass powder 20-40, closed-cell expanded perlite 8-15, hollow glass or ceramic fine bead 3-15, polymer microballoon 10-30, tubular fibre 2-5, Sodium Silicofluoride 3-5, latex powder 5-10, water proof anti-seepage additive 5-10;
After water glass powder and hollow glass or ceramic fine bead and closed perlite mixed, adding polymer microballoon and latex powder mixes, join after water proof anti-seepage additive and Sodium Silicofluoride are pre-mixed in the above-mentioned miscellany and to continue to mix, sneak into tubular fibre at last and mix the back.
The particle diameter of closed-cell expanded perlite of the present invention is the 150-200 micron, the particle diameter of hollow glass or ceramic fine bead is the 50-100 micron, the particle diameter of polymer microballoon is the 10-40 micron, tubular fibre is PET Hollow fiber or polypropylene hollow fiber or pure aluminium silicate tubular fibre, its diameter is the 20-40 micron, and length is the 0.5-2 millimeter.
Polymer hollow microsphere of the present invention preferably adopts the applicant to be " a kind of polymer hollow microsphere and preparation method thereof " prepared polymer hollow microsphere in the denomination of invention of application on the same day, and described polymer phase-change microsphere preferably adopts the applicant to be " a kind of polymer phase-change microsphere and preparation method thereof " prepared polymer phase-change microsphere in the denomination of invention of application on the same day.
Polymer microballoon of the present invention is formed by polymer hollow microsphere and the polymer phase-change microsphere mixed by weight 0-1: 0-1.
The particle diameter of polymer hollow microsphere of the present invention is the 20-40 micron, and the particle diameter of polymer phase-change microsphere is the 10-20 micron.
The invention has the beneficial effects as follows: at first the present invention has adopted double glazing or ceramic microsphere and polymer microballoon, because the structure of phase change material or hollow negative pressure in the polymer microballoon, make coating have the common feature of heat resistance type and thermal capacitance section bar material concurrently, comparing the simple heat resistance type of existing insulating mold coating is a progress and innovation; Secondly, lower at existing insulating mold coating weather resistance, the defective that contamination resistance is relatively poor, inorganic-organic compound form that the present invention adopts has outstanding weather resistance and good especially contamination resistance; The 3rd, used tubular fibre to strengthen in the coating of the present invention, increased substantially tension cracking resistance fracture resistance, tubular fibre also provides good heat insulating effect simultaneously, thereby has improved the thermal and insulating performance of coating; The 4th, coating of the present invention is pressed the mutual grating of particle diameter by hollow glass or materials such as ceramic microsphere, tubular fibre and polymer microballoon, make and the good barrier layer of having filmed intermediate formation to have reduced the cold and hot bridge of the intermediary of filming, further improved thermal and insulating performance.At last, compare the form of existing insulating mold coating with the liquid supply, the present invention adopts the dry powder material supply, greatly reduces transportation cost and storage cost, is convenient to accumulating and construction.
Embodiment
The present invention is described in further detail below in conjunction with embodiment.
A kind of polymer microsphere insulation heat-proof dry-powder paint, raw material by following weight part is formed: water glass powder 20-40, closed-cell expanded perlite 8-15, hollow glass or ceramic fine bead 3-15, polymer microballoon 10-30, tubular fibre 2-5, Sodium Silicofluoride 3-5, latex powder 5-10, water proof anti-seepage additive 5-10;
After water glass powder and hollow glass or ceramic fine bead and closed perlite mixed, adding polymer microballoon and latex powder mixes, join after water proof anti-seepage additive and Sodium Silicofluoride are pre-mixed in the above-mentioned miscellany and to continue to mix, sneak into tubular fibre at last and mix the back.
The particle diameter of described closed-cell expanded perlite is the 150-200 micron, the particle diameter of hollow glass or ceramic fine bead is the 50-100 micron, the particle diameter of polymer microballoon is the 10-40 micron, tubular fibre is PET Hollow fiber or polypropylene hollow fiber or pure aluminium silicate tubular fibre, its diameter is the 20-40 micron, and length is the 0.5-2 millimeter.
Described polymer microballoon can use the polymer microballoon of making by existing emulsion polymerization or suspension polymerization, but preferably adopt by the applicant on the same day the application, denomination of invention is that " a kind of polymer hollow microsphere and preparation method thereof " prepared polymer hollow microsphere and/or denomination of invention are " a kind of polymer phase-change microsphere and preparation method thereof " prepared polymer phase-change microsphere, and promptly described polymer microballoon is formed by polymer hollow microsphere and the polymer phase-change microsphere mixed by weight 0-1: 0-1.With the size grading of materials such as hollow glass or ceramic fine bead on, the particle diameter that preferably makes described polymer hollow microsphere is the 20-40 micron, the particle diameter of polymer phase-change microsphere is the 10-20 micron.
Embodiment 1
Add 100 parts of water glass powder by weight, 75 parts of particle diameters are 200 microns closed-cell expanded perlite, 75 parts of particle diameters are that 100 microns hollow glass micropearl is in Agravicmixer, start and mixed 10 minutes, with 75 parts particle diameters is that the mixed back of polymer phase-change microsphere that 40 microns polymer hollow microsphere and 75 parts of particle diameters are 20 microns adds in the Agravicmixer with 50 parts of latex powder in the lump, mix after 10 minutes, added 50 parts of water proof anti-seepage additives (SEAL-80) and 25 parts of Sodium Silicofluorides and thorough mixing again 15 minutes, adding 25 parts of diameters at last is 40 microns, and length is 2 millimeters PET Hollow fiber thorough mixing discharging packing after 20-30 minute.Mixed finished product and water can be constructed after being in harmonious proportion.The ratio that product and water are in harmonious proportion is 1: 1 (weight ratio).Be brushed on the flat aluminium alloy plate after the product for preparing and water is in harmonious proportion, brushing thickness is 2 millimeters, the temperature head that adds heat determination surface and hot face in the back of flat board is about 80 ℃, and (temperature of hot face is 140 ℃, the coating surface temperature is 58 ℃) and temperature to reach balance time be 8 hours, average effect of heat insulation is near 40 ℃/millimeter.
Embodiment 2
Add 200 parts of water glass powder by weight, 60 parts of particle diameters are 150 microns closed-cell expanded perlite, 15 parts of particle diameters are that 50 microns hollow ceramic microspheres is in Agravicmixer, start and mixed 10 minutes, with 50 parts of particle diameters is that the mixed back of polymer phase-change microsphere that 20 microns polymer hollow particles and 50 parts of particle diameters are 10 microns adds in the Agravicmixer with 25 parts of latex powder in the lump, mix after 10 minutes, added 25 parts of water proof anti-seepage additives (SAMTAK-3498) and 15 parts of Sodium Silicofluorides and thorough mixing again 15 minutes, adding 10 parts of diameters at last is 20 microns, and length is 0.5 millimeter pure aluminium silicate tubular fibre thorough mixing discharging packing after 20-30 minute.Mixed finished product and water can be constructed after being in harmonious proportion.The ratio that product and water are in harmonious proportion is 1: 1 (weight ratio).Be brushed on the flat aluminium alloy plate after the product for preparing and water is in harmonious proportion, brushing thickness is 2 millimeters, the temperature head that adds heat determination surface and hot face in the back of flat board is 45 ℃, and (temperature of hot face is 100 ℃, the coating surface temperature is 55 ℃) and temperature to reach balance time be 3 hours, average effect of heat insulation is near 23 ℃/millimeter.
Embodiment 3
Add 1000 parts of water glass powder by weight, 400 parts of particle diameters are 180 microns closed-cell expanded perlite, 200 parts of particle diameters are that 80 microns hollow glass micropearl is in Agravicmixer, start and mix after 10 minutes, add 300 parts of particle diameters and be polymer hollow particles and 300 parts of miscellany and 400 parts of latex powder that particle diameter is 15 microns a polymer phase-change microsphere of 30 microns, mix after 10 minutes, added 300 parts of water proof anti-seepage additives (ONTAMR-6) and 200 parts of Sodium Silicofluorides and thorough mixing again 15 minutes, adding 250 parts of diameters at last is 30 microns, and length is 1 millimeter polypropylene hollow fiber thorough mixing discharging packing after 20-30 minute.Mixed finished product and water can be constructed after being in harmonious proportion.The ratio that product and water are in harmonious proportion is 1: 1 (weight ratio).Be brushed on the flat aluminium alloy plate after the product for preparing and water is in harmonious proportion, brushing thickness is 2 millimeters, (temperature of hot face is 120 ℃ to the temperature head that adds heat determination surface and hot face in the back of flat board near 60 ℃, the coating surface temperature is 61 ℃) and temperature to reach balance time be 6 hours, average effect of heat insulation is near 30 ℃/millimeter.
Embodiment 4
Add 1000 parts of water glass powder by weight, 400 parts of particle diameters are 180 microns closed-cell expanded perlite, 150 parts of particle diameters are that 80 microns hollow glass micropearl is in Agravicmixer, start and mix after 10 minutes, add 500 parts of particle diameters and be polymer hollow microsphere and 250 parts of latex powder of 30 microns, mix after 10 minutes, added 250 parts of water proof anti-seepage additives (ONTAMR-6) and 150 parts of Sodium Silicofluorides and thorough mixing again 15 minutes, adding 100 parts of diameters at last is 40 microns, and length is 1 millimeter PET Hollow fiber thorough mixing discharging packing after 20-30 minute.Mixed finished product and water can be constructed after being in harmonious proportion.The ratio that product and water are in harmonious proportion is 1: 1 (weight ratio).Be brushed on the flat aluminium alloy plate after the product for preparing and water is in harmonious proportion, brushing thickness is 2 millimeters, (temperature of hot face is 120 ℃ to the temperature head that adds heat determination surface and hot face in the back of flat board near 62 ℃, the coating surface temperature is 58 ℃) and temperature to reach balance time be 4.5 hours, average effect of heat insulation is near 31 ℃/millimeter.
Embodiment 5
Add 1000 parts of water glass powder by weight, 375 parts of particle diameters are 150 microns closed-cell expanded perlite, 375 parts of particle diameters are that 50 microns hollow ceramic microspheres is in Agravicmixer, start and mix after 10 minutes, add 750 parts of particle diameters and be polymer phase-change microsphere and 250 parts of latex powder of 20 microns, mix after 10 minutes, added 250 parts of water proof anti-seepage additives (ONTAMR-6) and 125 parts of Sodium Silicofluorides and thorough mixing again 15 minutes, adding 75 parts of diameters at last is 20 microns, and length is 1 millimeter PET Hollow fiber thorough mixing discharging packing after 20-30 minute.Mixed finished product and water can be constructed after being in harmonious proportion.The ratio that product and water are in harmonious proportion is 1: 1 (weight ratio).Be brushed on the flat aluminium alloy plate after the product for preparing and water is in harmonious proportion, brushing thickness is 2 millimeters, (temperature of hot face is 120 ℃ to the temperature head that adds heat determination surface and hot face in the back of flat board near 56 ℃, the coating surface temperature is 64 ℃) and temperature to reach balance time be 12 hours, average effect of heat insulation is near 28 ℃/millimeter.
Embodiment 6
Add 900 parts of water glass powder by weight, 360 parts of particle diameters are 200 microns closed-cell expanded perlite, 270 parts of particle diameters are that 80 microns hollow glass micropearl is in Agravicmixer, start and mix after 10 minutes, add 200 parts of particle diameters and be polymer hollow microsphere and 400 parts of mixture and 240 parts of latex powder that particle diameter is 15 microns a polymer phase-change microsphere of 30 microns, mix after 10 minutes, added 240 parts of water proof anti-seepage additives (ONTAMR-6) and 120 parts of Sodium Silicofluorides and thorough mixing again 15 minutes, adding 120 parts of particle diameters at last is 30 microns, and length is 1 millimeter PET Hollow fiber thorough mixing discharging packing after 20-30 minute.Mixed finished product and water can be constructed after being in harmonious proportion.The ratio that product and water are in harmonious proportion is 1: 1 (weight ratio).Be brushed on the flat aluminium alloy plate after the product for preparing and water is in harmonious proportion, brushing thickness is 2 millimeters, (temperature of hot face is 120 ℃ to the temperature head that adds heat determination surface and hot face in the back of flat board near 64 ℃, the coating surface temperature is 56 ℃) and temperature to reach balance time be 8 hours, average effect of heat insulation is near 32 ℃/millimeter.
Claims (5)
1. polymer microsphere insulation heat-proof dry-powder paint, it is characterized in that forming: water glass powder 20-40 by the raw material of following weight part, closed-cell expanded perlite 8-15, hollow glass or ceramic fine bead 3-15, polymer phase-change microsphere 10-30, tubular fibre 2-5, Sodium Silicofluoride 3-5, latex powder 5-10, water proof anti-seepage additive 5-10;
After water glass powder and hollow glass or ceramic fine bead and closed perlite mixed, adding polymer microballoon and latex powder mixes, join after water proof anti-seepage additive and Sodium Silicofluoride are pre-mixed in the above-mentioned miscellany and to continue to mix, sneak into tubular fibre at last and mix the back.
2. a kind of polymer microsphere insulation heat-proof dry-powder paint according to claim 1, it is characterized in that: the particle diameter of described closed-cell expanded perlite is the 150-200 micron, the particle diameter of hollow glass or ceramic fine bead is the 50-100 micron, the particle diameter of polymer microballoon is the 10-40 micron, described tubular fibre is inorganic hollow fibers and/or organic hollow fiber, its diameter is the 20-40 micron, and length is the 0.5-2 millimeter.
3. a kind of polymer microsphere insulation heat-proof dry-powder paint according to claim 2 is characterized in that: described inorganic hollow fibers is the pure aluminium silicate tubular fibre, and described organic hollow fiber is PET Hollow fiber or polypropylene hollow fiber.
4. a kind of polymer microsphere insulation heat-proof dry-powder paint according to claim 1 is characterized in that: described polymer microballoon is formed by polymer hollow particles and the polymer phase-change microsphere mixed by weight 0-1: 0-1.
5. a kind of polymer microsphere insulation heat-proof dry-powder paint according to claim 4 is characterized in that: the particle diameter of described polymer hollow particles is the 20-40 micron, and the particle diameter of polymer phase-change microsphere is the 10-20 micron.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2008100472435A CN101250343B (en) | 2008-04-03 | 2008-04-03 | Polymer microsphere insulation heat-proof dry-powder paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100472435A CN101250343B (en) | 2008-04-03 | 2008-04-03 | Polymer microsphere insulation heat-proof dry-powder paint |
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| CN101250343A true CN101250343A (en) | 2008-08-27 |
| CN101250343B CN101250343B (en) | 2010-06-02 |
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| CN102093788A (en) * | 2010-12-15 | 2011-06-15 | 谢刚 | Industrial thermal insulation coating and preparation method thereof |
| CN102617102A (en) * | 2011-12-28 | 2012-08-01 | 上海墙特节能材料有限公司 | Inorganic dry powder architectural coating and production method thereof |
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