CN101205603A - Ceramic vacuum coating technique - Google Patents
Ceramic vacuum coating technique Download PDFInfo
- Publication number
- CN101205603A CN101205603A CNA2006101579623A CN200610157962A CN101205603A CN 101205603 A CN101205603 A CN 101205603A CN A2006101579623 A CNA2006101579623 A CN A2006101579623A CN 200610157962 A CN200610157962 A CN 200610157962A CN 101205603 A CN101205603 A CN 101205603A
- Authority
- CN
- China
- Prior art keywords
- vacuum
- produce
- vacuum chamber
- gas
- current
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Physical Vapour Deposition (AREA)
Abstract
A ceramic vacuum film coating technological method belongs to the vacuum film coating technical field, comprising the following process steps: A. a domestic ceramic device is put into a vacuum chamber hanging part of a vacuum multi-arc ion film coating machine having magnetic control function, and positive ion magnetic deposited particles are generated when the current is 40-48 ampere and the voltage is 450-490 voltampere; B. a vacuum chamber is heated to ensure the temperature of the vacuum chamber reaches the range between 200 and 350 DEG C, and when the gas in the vacuum chamber is pumped and the vacuum reaches 3x10-2Pa-5x10-3Pa, 450 ml-980ml of argon gas or nitrogen gas with the gas pressure between 1Mpa and 1.2MPa is injected; C. a multi-arc titanium target is opened; when the DC current is 70-90 ampere and the DC voltage is 450-490 voltampere, ion electrode current is generated to impact titanium target phase pulse, and reacts with argon gas or the nitrogen gas in the vacuum chamber to produce imitatively golden or imitatively silvery color deposited on the surface of the device. The present invention is simple in process, favorable for environmental protection, nontoxic and suitable for processing domestic ceramic or glass products.
Description
Technical field:
The present invention relates to a kind of ceramic vacuum coating technique, it belongs to technical field of vacuum plating.
Background technology:
In the prior art, the vacuum plating of pottery is technological difficulties, needs to adopt special equipment just can finish.But therefore the equipment price costliness that this class is special, makes that the price of ceramic vacuum plating product is very expensive night.And, in the existing processes, all be to adopt the metal bullion and silver to carry out plated film as raw material, on technology, this class coating technique needs earlier with printing, artificial coating again with in warm kiln burn till, produce obnoxious flavour and endanger surrounding enviroment.This type coating comes off night easily, and luminance brightness is poor, and coated membrane contain harmful HUMAN HEALTH elements such as plumbous cadmium, can not guarantee the security of using; Use the metal bullion and silver as coating raw material in addition, its cost is also than higher.
Summary of the invention:
The object of the present invention is to provide a kind of technology simple, tooling cost is low, and coating quality is good, ceramic vacuum coating technique.
The object of the present invention is achieved like this:
A kind of ceramic vacuum coating technique, it comprises following processing step:
A: the vacuum chamber suspension member of at first the domestic ceramics device being put into vacuum arc deposition film machine with magnetic control function, make magnetic titanium rod produce bias current by magnetic control means earlier, in electric current 40～48 peaces doubly, voltage 450～490 volt-ampere hours generation positive ion magnetic substance deposited particles makes domestic ceramics device top layer have the magnetosphere body;
B: when the titanium rod produced bias current, hot donut made the temperature of vacuum chamber reach between 200～350 ℃, extracted the vacuum indoor gas out and reached vacuum tightness 3 * 10
-2Pa～5 * 10
-3During Pa, put into argon gas or the nitrogen gas 450ml～980ml of air pressure at 1Mpa～1.2MPa;
C: open multi sphere titanium target doubly in galvanic current 70～95 peaces, volts DS 450～490 volt-ampere hours produce ion electrode electric current and titanium target mutually pulse impinge upon in the vacuum chamber to produce and imitate the gold color with the nitrogen gas phase reaction, produce silver color deposited particles with the argon gas phase reaction and produce rete, decontrol gas and can take out product in ceramic surface.
Described selection process step is:
A: the vacuum chamber suspension member of at first the domestic ceramics device being put into vacuum arc deposition film machine with magnetic control function, by magnetic control means carrying magnetic titanium rod will be housed earlier and produce bias current, in electric current 45 peaces doubly, voltage 480 volt-ampere hours generation positive ion magnetic substance deposited particles makes product subsurface have the magnetosphere body;
B: when the titanium rod produced bias current, hot donut made the temperature of vacuum chamber reach between room temperature 280 degree, extracts the vacuum indoor gas out and reaches vacuum tightness 4 * 10
-2During Pa, put into argon gas or the nitrogen gas 450ml～980ml of air pressure at 1Mpa～1.2MPa;
C: open multi sphere titanium target doubly in galvanic current 80 peaces, volts DS 470 volt-ampere hours produce ion electrode electric current and titanium target mutually pulse impinge upon nitrogen gas in the vacuum chamber and produce imitative gold or silver color deposited particles produces rete in ceramic surface, relieving gas can take out product.
The present invention does not use the metal bullion and silver as coating raw material, does not have any public hazards, and can make ceramic surface more wear-resisting, light, and protection against corrosion, acidproof alkali salt, chroma-luminance is smooth, is not easy to come off, and human body is not had any public hazards, and is pollution-free; Process period of the present invention is short, and easy to operate, tooling cost is low; Can disposal molding, need not other and protect assistant engineer's tool, can not produce obnoxious flavour harm surrounding enviroment.
Embodiment:
Below in conjunction with embodiment the present invention is further detailed:
Embodiment 1
In the present embodiment, process silver-plated domestic ceramics device, the present invention includes following processing step:
A: at first the domestic ceramics device is put into the vacuum chamber suspension member of the vacuum arc deposition film machine with magnetic control function, described vacuum arc deposition film machine with magnetic control function is a prior art.Make the carrying magnetic titanium rod in the vacuum arc deposition film machine produce bias current by magnetic control means earlier, in electric current 45 peaces doubly, voltage 480 volt-ampere hours produce positive ion magnetic substance deposited particles makes the top layer of domestic ceramics device have the magnetosphere body;
B: when titanium rod produced bias current, hot donut when making the temperature of vacuum chamber reach 280 ℃, was extracted the vacuum indoor gas out, makes that the vacuum tightness in the vacuum chamber reaches 4 * 10
-2During Pa, put into the argon gas 450ml～980ml of air pressure at 1Mpa～1.2MPa;
C: open multi sphere titanium target, galvanic current in the multi sphere titanium target be 80 peaces doubly, volts DS is 470 volt-ampere hours, produce the ion electrode electric current, this ion electrode electric current and titanium target pulse mutually impinge upon the argon gas in the vacuum chamber and produce imitative silver color deposited particles and produce rete in ceramic surface, decontrol gas and can take out product.
The domestic ceramics device Production Flow Chart each time that has plated film according to processing method process for processing of the present invention only needs 15～20 minutes.
Embodiment 2
In the present embodiment, process gold-plated domestic glass device, the present invention includes following processing step:
A: at first the domestic glass device is put into the vacuum chamber suspension member of the vacuum arc deposition film machine with magnetic control function, described vacuum arc deposition film machine with magnetic control function is a prior art.Make the carrying magnetic titanium rod in the vacuum arc deposition film machine produce bias current by magnetic control means earlier, in electric current 40 peaces doubly, voltage 450 volt-ampere hours produce positive ion magnetic substance deposited particles makes the top layer of domestic ceramics device have the magnetosphere body;
B: when titanium rod produced bias current, hot donut when making the temperature of vacuum chamber reach 200 ℃, was extracted the vacuum indoor gas out, makes that the vacuum tightness in the vacuum chamber reaches 5 * 10
-3Pa puts into the nitrogen gas 450ml～980ml of air pressure at 1Mpa～1.2MPa constantly;
C: open multi sphere titanium target, galvanic current in the multi sphere titanium target be 70 peaces doubly, volts DS is 450 volt-ampere hours, produce the ion electrode electric current, this ion electrode electric current and titanium target pulse mutually impinge upon the nitrogen gas in the vacuum chamber and produce imitative gold color deposited particles and produce rete in ceramic surface, decontrol gas and can take out product.
Embodiment 3
In the present embodiment, process gold-plated domestic ceramics device, the present invention includes following processing step:
A: at first the domestic ceramics device is put into the vacuum chamber suspension member of the vacuum arc deposition film machine with magnetic control function, described vacuum arc deposition film machine with magnetic control function is a prior art.Make the carrying magnetic titanium rod in the vacuum arc deposition film machine produce bias current by magnetic control means earlier, in electric current 48 peaces doubly, voltage 490 volt-ampere hours produce positive ion magnetic substance deposited particles makes the top layer of domestic ceramics device have the magnetosphere body;
B: when titanium rod produced bias current, hot donut when making the temperature of vacuum chamber reach 350 ℃, was extracted the vacuum indoor gas out, makes that the vacuum tightness in the vacuum chamber reaches 3 * 10
-2During Pa, put into the nitrogen gas 450ml～980ml of air pressure at 1Mpa～1.2MPa;
C: open multi sphere titanium target, galvanic current in the multi sphere titanium target be 95 peaces doubly, volts DS is 490 volt-ampere hours, produce the ion electrode electric current, this ion electrode electric current and titanium target pulse mutually impinge upon the nitrogen gas in the vacuum chamber and produce imitative gold color deposited particles and produce rete in ceramic surface, decontrol gas and can take out product.
Claims (2)
1. ceramic vacuum coating technique is characterized in that it comprises following processing step:
A: the vacuum chamber suspension member of at first the domestic ceramics device being put into vacuum arc deposition film machine with magnetic control function, make magnetic titanium rod produce bias current by magnetic control means earlier, in electric current 40～48 peaces doubly, voltage 450～490 volt-ampere hours generation positive ion magnetic substance deposited particles makes domestic ceramics device top layer have the magnetosphere body;
B: when the titanium rod produced bias current, hot donut made the temperature of vacuum chamber reach between 200～350 ℃, extracted the vacuum indoor gas out and reached vacuum tightness 3 * 10
-2Pa～5 * 10
-3During Pa, put into argon gas or the nitrogen gas 450ml～980ml of air pressure at 1Mpa～1.2MPa;
C: open multi sphere titanium target doubly in galvanic current 70～95 peaces, volts DS 450～490 volt-ampere hours produce ion electrode electric current and titanium target mutually pulse impinge upon in the vacuum chamber to produce and imitate the gold color with the nitrogen gas phase reaction, produce silver color deposited particles with the argon gas phase reaction and produce rete, decontrol gas and can take out product in ceramic surface.
2. the ceramic vacuum coating technique described in claim 1 is characterized in that described selection process step is:
A: the vacuum chamber suspension member of at first the domestic ceramics device being put into vacuum arc deposition film machine with magnetic control function, make magnetic titanium rod produce bias current by magnetic control means earlier, in electric current 45 peaces doubly, voltage 480 volt-ampere hours produce positive ion magnetic substance deposited particles makes domestic ceramics device top layer have the magnetosphere body
B: when the titanium rod produced bias current, hot donut made the temperature of vacuum chamber reach between room temperature 280 degree, extracts the vacuum indoor gas out and reaches vacuum tightness 4 * 10
-2During Pa, put into argon gas or the nitrogen gas 450ml～980ml of air pressure at 1Mpa～1.2MPa;
C: open multi sphere titanium target doubly in galvanic current 80 peaces, volts DS 470 volt-ampere hours produce ion electrode electric current and titanium target mutually pulse impinge upon in the vacuum chamber to produce and imitate the gold color with the nitrogen gas phase reaction, produce silver color deposited particles with the argon gas phase reaction and produce rete, decontrol gas and can take out product in ceramic surface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006101579623A CN100554502C (en) | 2006-12-22 | 2006-12-22 | Ceramic vacuum coating technique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006101579623A CN100554502C (en) | 2006-12-22 | 2006-12-22 | Ceramic vacuum coating technique |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101205603A true CN101205603A (en) | 2008-06-25 |
| CN100554502C CN100554502C (en) | 2009-10-28 |
Family
ID=39566085
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006101579623A Expired - Fee Related CN100554502C (en) | 2006-12-22 | 2006-12-22 | Ceramic vacuum coating technique |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100554502C (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101962271A (en) * | 2010-06-17 | 2011-02-02 | 张元胜 | Golden coated glass and preparation process thereof |
| CN101974731A (en) * | 2010-11-30 | 2011-02-16 | 东莞星晖真空镀膜塑胶制品有限公司 | Vacuum magnetic control coating process |
| CN116103612A (en) * | 2023-03-02 | 2023-05-12 | 江苏富乐华功率半导体研究院有限公司 | Method for manufacturing titanium nitride film |
-
2006
- 2006-12-22 CN CNB2006101579623A patent/CN100554502C/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101962271A (en) * | 2010-06-17 | 2011-02-02 | 张元胜 | Golden coated glass and preparation process thereof |
| CN101974731A (en) * | 2010-11-30 | 2011-02-16 | 东莞星晖真空镀膜塑胶制品有限公司 | Vacuum magnetic control coating process |
| CN101974731B (en) * | 2010-11-30 | 2013-02-13 | 东莞星晖真空镀膜塑胶制品有限公司 | Vacuum magnetic control coating process |
| CN116103612A (en) * | 2023-03-02 | 2023-05-12 | 江苏富乐华功率半导体研究院有限公司 | Method for manufacturing titanium nitride film |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100554502C (en) | 2009-10-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104211444A (en) | Preparation method of furnace transmutation sorghum red-flower glaze | |
| CN100554502C (en) | Ceramic vacuum coating technique | |
| CN106435489B (en) | A kind of preparation method of the anti-oxidant self-healing Cr/NiCr coating of niobium primary surface | |
| CN106191564A (en) | House ornamentation dark DE Specular Lighting pool aluminium alloy and preparation technology thereof | |
| CN105671513A (en) | Novel vacuum color coating process | |
| CN102173761A (en) | Ceramic clay used for powder paint decoration and production method of powder paint decorative ceramic prepared from same | |
| WO2014109425A1 (en) | Method for producing thin film on nanocrystalline max | |
| CN107695358B (en) | A kind of preparation method of welding electrode | |
| CN107740030B (en) | Strontium-doped titanium oxide coating composition, coating and preparation method thereof | |
| CN103088285A (en) | Preparation method of nickel-copper alloy depositing layer | |
| JP2854104B2 (en) | Manufacturing method of ceramic coating material | |
| CN102896826B (en) | Film-coated part | |
| Borisov et al. | Microplasma spraying of bioceramic coatings | |
| ES2185454A1 (en) | Method for obtaining transparent, electrically conducting oxides by means of sputtering | |
| CN109055891A (en) | A kind of preparation method of power battery ceramic connector metalization layer | |
| CN108878091A (en) | A kind of preparation method of the Mn-Bi permanent magnet with ceramic protection layer | |
| CN1438356A (en) | Multihead ion film-plating method for ceramic product | |
| CN102051569B (en) | Method for preparing titanium/hydroxyapatite composite coating | |
| KR102075938B1 (en) | Plating method of dental prosthesis | |
| CN102373412A (en) | Vacuum-plated part and its manufacturing method | |
| CN102477530A (en) | Shell and manufacture method thereof | |
| Novinski et al. | Advanced Copper--Nickel Indium Coatings by HVOF Deposition | |
| CN117488245A (en) | Antibacterial ceramic tile based on magnetron sputtering technology and preparation method thereof | |
| KR101589631B1 (en) | Gold plating method of metal or metal alloy containing no nickel | |
| CN112323016A (en) | Ceramic metal sputtering film forming process |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Raoping County Xiangyuan Industry Co., Ltd. Assignor: Shenzhen Xiangyuan Industry & Trade Co., Ltd. Contract record no.: 2010440000466 Denomination of invention: Ceramic vacuum coating technique Granted publication date: 20091028 License type: Exclusive License Open date: 20080625 Record date: 20100505 |
|
| ASS | Succession or assignment of patent right |
Owner name: RAOPING XIANGYUAN INDUSTRIAL + TRADING CO., LTD. Free format text: FORMER OWNER: SHENZHEN XIANGYUAN INDUSTRY + TRADE CO., LTD. Effective date: 20111209 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 518002 SHENZHEN, GUANGDONG PROVINCE TO: 515734 CHAOZHOU, GUANGDONG PROVINCE |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20111209 Address after: 515734, Guangdong, Raoping Province three Rao Town, three Rao neighborhood committee, Chengdong Road, No. 16 Patentee after: Raoping County Xiangyuan Industry Co., Ltd. Address before: 518002 Guangdong Province, Shenzhen City People's road Jianingna Plaza B block, room 1806 Patentee before: Shenzhen Xiangyuan Industry & Trade Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20091028 Termination date: 20151222 |
|
| EXPY | Termination of patent right or utility model |