CN101177468B - Water-soluble crylic acid resin and preparation method thereof - Google Patents
Water-soluble crylic acid resin and preparation method thereof Download PDFInfo
- Publication number
- CN101177468B CN101177468B CN2007100321248A CN200710032124A CN101177468B CN 101177468 B CN101177468 B CN 101177468B CN 2007100321248 A CN2007100321248 A CN 2007100321248A CN 200710032124 A CN200710032124 A CN 200710032124A CN 101177468 B CN101177468 B CN 101177468B
- Authority
- CN
- China
- Prior art keywords
- water
- acrylic resin
- mercaptoethanol
- water soluble
- soluble acrylic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000002360 preparation method Methods 0.000 title abstract description 10
- 239000011347 resin Substances 0.000 title description 8
- 229920005989 resin Polymers 0.000 title description 8
- 239000002253 acid Substances 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 23
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 12
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 12
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 12
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims abstract description 11
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims abstract description 11
- DNJIEGIFACGWOD-UHFFFAOYSA-N ethyl mercaptane Natural products CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 claims abstract description 11
- DGVVWUTYPXICAM-UHFFFAOYSA-N β‐Mercaptoethanol Chemical compound OCCS DGVVWUTYPXICAM-UHFFFAOYSA-N 0.000 claims abstract description 11
- VVWRJUBEIPHGQF-UHFFFAOYSA-N propan-2-yl n-propan-2-yloxycarbonyliminocarbamate Chemical compound CC(C)OC(=O)N=NC(=O)OC(C)C VVWRJUBEIPHGQF-UHFFFAOYSA-N 0.000 claims description 10
- -1 Bing Xisuandingzhi Chemical compound 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 4
- 239000000178 monomer Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims 1
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 239000003960 organic solvent Substances 0.000 abstract description 4
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 abstract 2
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 abstract 1
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 abstract 1
- 239000002904 solvent Substances 0.000 description 7
- 239000011248 coating agent Substances 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 208000027418 Wounds and injury Diseases 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 208000014674 injury Diseases 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- 229920002554 vinyl polymer Polymers 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010528 free radical solution polymerization reaction Methods 0.000 description 1
- 239000003999 initiator Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007100321248A CN101177468B (en) | 2007-12-05 | 2007-12-05 | Water-soluble crylic acid resin and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007100321248A CN101177468B (en) | 2007-12-05 | 2007-12-05 | Water-soluble crylic acid resin and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101177468A CN101177468A (en) | 2008-05-14 |
CN101177468B true CN101177468B (en) | 2012-07-04 |
Family
ID=39403906
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2007100321248A Expired - Fee Related CN101177468B (en) | 2007-12-05 | 2007-12-05 | Water-soluble crylic acid resin and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN101177468B (en) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103387637B (en) * | 2013-08-06 | 2016-02-10 | 江苏泰格油墨有限公司 | A kind of water-soluble self-crosslinking acrylic resin composition and method of making the same |
CN103666166A (en) * | 2013-11-27 | 2014-03-26 | 湖州立方农艺科技发展有限公司 | Environment-friendly painting coating |
CN104073117A (en) * | 2014-06-23 | 2014-10-01 | 无锡市崇安区科技创业服务中心 | Water-soluble acrylic resin coating and preparation method thereof |
CN104403044B (en) * | 2014-11-12 | 2016-09-28 | 安徽优科新材料科技有限公司 | A kind of Lacquer finish type water soluble acrylic resin and preparation method thereof |
CN104497207B (en) * | 2014-12-31 | 2017-12-05 | 广东佳景科技股份有限公司 | A kind of air knife spraying binder and preparation method thereof |
CN106349422A (en) * | 2016-08-31 | 2017-01-25 | 江苏李文甲化工有限公司 | Water-soluble acrylate resin and synthesis method thereof |
CN107674144B (en) * | 2017-05-05 | 2019-10-01 | 南昌大学 | A kind of exterior coating preparation method of water soluble acrylic resin |
CN107936715A (en) * | 2017-12-22 | 2018-04-20 | 威海新元化工有限公司 | A kind of water-based fishing rod solid color enamel resin and preparation method thereof |
CN109021183A (en) * | 2018-06-22 | 2018-12-18 | 安徽菱湖漆股份有限公司 | A kind of water soluble polymer condensation copolymerization resin, process for preparing resins and its application |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1908023A (en) * | 2006-08-16 | 2007-02-07 | 海洋化工研究院 | Acrylic acid bulk hybridization emulsion composition |
CN1978472A (en) * | 2005-12-06 | 2007-06-13 | 江苏三木集团有限公司 | Water-soluble acrylic resin and its preparing method |
CN101067011A (en) * | 2007-04-30 | 2007-11-07 | 江苏三木集团有限公司 | Water soluble acrylic resin and its prepn |
-
2007
- 2007-12-05 CN CN2007100321248A patent/CN101177468B/en not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1978472A (en) * | 2005-12-06 | 2007-06-13 | 江苏三木集团有限公司 | Water-soluble acrylic resin and its preparing method |
CN1908023A (en) * | 2006-08-16 | 2007-02-07 | 海洋化工研究院 | Acrylic acid bulk hybridization emulsion composition |
CN101067011A (en) * | 2007-04-30 | 2007-11-07 | 江苏三木集团有限公司 | Water soluble acrylic resin and its prepn |
Non-Patent Citations (3)
Title |
---|
唐林生等.涂料用水溶性丙烯酸树脂的合成.《青岛化工学院学报》.2002,第23卷(第3期),20-21. * |
费华等.丙烯酸类树脂为基料的水性油墨的研究.《华中师范大学学报(自然科学版)》.2001,第35卷(第3期),319-320. * |
赵晶丽等.羟基丙烯酸树脂制备及其应用.《山西化工》.2002,第22卷(第3期),21-22. * |
Also Published As
Publication number | Publication date |
---|---|
CN101177468A (en) | 2008-05-14 |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C56 | Change in the name or address of the patentee | ||
CP03 | Change of name, title or address |
Address after: Chashan town Tong Kok village 523393 Guangdong city of Dongguan Province on Tong industrial area Patentee after: GUANGDONG YINGKE GROUP Co.,Ltd. Address before: Chashan town Tong Kok village 523050 Guangdong city of Dongguan Province on Tong industrial area Patentee before: Yingke (Dongguan) Printing Ink Mfg., Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20211201 Address after: 314300 Shu Pu Zhen Chang Qing Lu, Haiyan County, Jiaxing City, Zhejiang Province Patentee after: Zhejiang Yingke ink material Co.,Ltd. Address before: Chashan town Tong Kok village 523393 Guangdong city of Dongguan Province on Tong industrial area Patentee before: GUANGDONG YINGKE GROUP Co.,Ltd. |
|
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120704 |