CN101163804A - 用于从化合物或金属中除去氧的电化学方法和装置 - Google Patents
用于从化合物或金属中除去氧的电化学方法和装置 Download PDFInfo
- Publication number
- CN101163804A CN101163804A CNA2006800137065A CN200680013706A CN101163804A CN 101163804 A CN101163804 A CN 101163804A CN A2006800137065 A CNA2006800137065 A CN A2006800137065A CN 200680013706 A CN200680013706 A CN 200680013706A CN 101163804 A CN101163804 A CN 101163804A
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- CN
- China
- Prior art keywords
- metal
- melt
- compound
- anode
- aforementioned
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 53
- 239000002184 metal Substances 0.000 title claims abstract description 53
- 150000001875 compounds Chemical class 0.000 title claims abstract description 49
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 239000001301 oxygen Substances 0.000 title claims abstract description 29
- 229910052760 oxygen Inorganic materials 0.000 title claims abstract description 29
- 238000002848 electrochemical method Methods 0.000 title description 2
- 239000000155 melt Substances 0.000 claims abstract description 28
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 11
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 4
- 150000001340 alkali metals Chemical class 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 56
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 42
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 29
- 229910045601 alloy Inorganic materials 0.000 claims description 21
- 239000000956 alloy Substances 0.000 claims description 21
- 239000007787 solid Substances 0.000 claims description 21
- 230000005611 electricity Effects 0.000 claims description 20
- 239000000463 material Substances 0.000 claims description 18
- 238000000354 decomposition reaction Methods 0.000 claims description 17
- 229910052728 basic metal Inorganic materials 0.000 claims description 12
- 150000003818 basic metals Chemical class 0.000 claims description 12
- 239000011734 sodium Substances 0.000 claims description 10
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 9
- 229910000765 intermetallic Inorganic materials 0.000 claims description 8
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 8
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 8
- 229910052742 iron Inorganic materials 0.000 claims description 7
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 6
- 229910000272 alkali metal oxide Inorganic materials 0.000 claims description 6
- 239000001257 hydrogen Substances 0.000 claims description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- 229910000480 nickel oxide Inorganic materials 0.000 claims description 5
- 239000002243 precursor Substances 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 229910000990 Ni alloy Inorganic materials 0.000 claims description 4
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims description 4
- 238000004062 sedimentation Methods 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 3
- 239000010941 cobalt Substances 0.000 claims description 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- 239000011701 zinc Substances 0.000 claims description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 claims description 2
- 229910001950 potassium oxide Inorganic materials 0.000 claims description 2
- 229910017052 cobalt Inorganic materials 0.000 claims 2
- 229910052802 copper Inorganic materials 0.000 claims 2
- 239000011133 lead Substances 0.000 claims 2
- 229910052725 zinc Inorganic materials 0.000 claims 2
- 150000002816 nickel compounds Chemical class 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 15
- 229910052799 carbon Inorganic materials 0.000 description 7
- 150000003839 salts Chemical class 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 238000009792 diffusion process Methods 0.000 description 4
- 230000002349 favourable effect Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000001110 calcium chloride Substances 0.000 description 3
- 229910001628 calcium chloride Inorganic materials 0.000 description 3
- 150000002736 metal compounds Chemical class 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- FVAUCKIRQBBSSJ-UHFFFAOYSA-M sodium iodide Chemical compound [Na+].[I-] FVAUCKIRQBBSSJ-UHFFFAOYSA-M 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 229910001413 alkali metal ion Inorganic materials 0.000 description 2
- 239000010405 anode material Substances 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000007769 metal material Substances 0.000 description 2
- JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 229910021607 Silver chloride Inorganic materials 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(II) oxide Inorganic materials [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 description 1
- 229910000431 copper oxide Inorganic materials 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000002484 cyclic voltammetry Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 229910001026 inconel Inorganic materials 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N lead(II) oxide Inorganic materials [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- -1 plumbous oxide compound Chemical class 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000007569 slipcasting Methods 0.000 description 1
- 235000009518 sodium iodide Nutrition 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- XLOMVQKBTHCTTD-UHFFFAOYSA-N zinc oxide Inorganic materials [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/129—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B15/00—Other processes for the manufacture of iron from iron compounds
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B5/00—General methods of reducing to metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/10—Reduction of greenhouse gas [GHG] emissions
- Y02P10/134—Reduction of greenhouse gas [GHG] emissions by avoiding CO2, e.g. using hydrogen
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Electrolytic Production Of Metals (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Electrodes For Compound Or Non-Metal Manufacture (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB0504444.1A GB0504444D0 (en) | 2005-03-03 | 2005-03-03 | Method and apparatus for removing oxygen from a solid compound or metal |
GB0504444.1 | 2005-03-03 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN101163804A true CN101163804A (zh) | 2008-04-16 |
Family
ID=34430598
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNA2006800137065A Pending CN101163804A (zh) | 2005-03-03 | 2006-03-03 | 用于从化合物或金属中除去氧的电化学方法和装置 |
Country Status (9)
Country | Link |
---|---|
US (1) | US20080302655A1 (fr) |
EP (1) | EP1866448A1 (fr) |
JP (1) | JP2008531854A (fr) |
CN (1) | CN101163804A (fr) |
AU (1) | AU2006219725A1 (fr) |
EA (1) | EA200701896A1 (fr) |
GB (2) | GB0504444D0 (fr) |
WO (1) | WO2006092615A1 (fr) |
ZA (1) | ZA200707266B (fr) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112941567A (zh) * | 2018-07-10 | 2021-06-11 | 东北大学 | 潮湿气氛的高温熔盐电解的电化学方法和装置 |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NO20060806L (no) * | 2006-02-17 | 2007-08-20 | Norsk Titanium Metals As | Fremgangsmate og anordning for metallproduksjon |
US20120041083A1 (en) * | 2008-12-18 | 2012-02-16 | Silicon Fire Ag | Silicon or elementary metals as energy carriers |
EP2647596A3 (fr) | 2008-12-18 | 2014-08-27 | Silicon Fire AG | Procédé et appareil pour fournir une source d'énergie en utilisant du dioxyde de carbone comme source de carbone et de l'énergie électrique |
SA110310372B1 (ar) * | 2009-05-12 | 2014-08-11 | Metalysis Ltd | جهاز وطريقة اختزال مخزون التغذية الصلب |
EP2461922A4 (fr) * | 2009-08-09 | 2014-04-16 | Rolls Royce Corp | Résistance à la corrosion pour un procédé de lixivation |
US8764962B2 (en) * | 2010-08-23 | 2014-07-01 | Massachusetts Institute Of Technology | Extraction of liquid elements by electrolysis of oxides |
BR112013011941A2 (pt) * | 2010-11-18 | 2016-11-01 | Metalysis Ltd | método e sistema para reduzir eletroliticamente uma matéria - prima sólida |
MY180279A (en) | 2010-11-18 | 2020-11-26 | Metalysis Ltd | Electrolysis apparatus |
US8900439B2 (en) | 2010-12-23 | 2014-12-02 | Ge-Hitachi Nuclear Energy Americas Llc | Modular cathode assemblies and methods of using the same for electrochemical reduction |
GB201223375D0 (en) * | 2012-12-24 | 2013-02-06 | Metalysis Ltd | Method and apparatus for producing metal by electrolytic reduction |
NL2015759B1 (en) | 2015-11-10 | 2017-05-26 | Stichting Energieonderzoek Centrum Nederland | Additive manufacturing of metal objects. |
NL2018890B1 (en) | 2017-05-10 | 2018-11-15 | Admatec Europe B V | Additive manufacturing of metal objects |
NL2021611B1 (en) | 2018-09-12 | 2020-05-06 | Admatec Europe B V | Three-dimensional object and manufacturing method thereof |
CN113802149B (zh) * | 2021-08-11 | 2023-06-27 | 华北理工大学 | 一种从锌窑渣中提取金属铁的方法 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL282584A (fr) * | 1961-08-30 | |||
SU651602A1 (ru) * | 1977-09-26 | 1980-01-05 | Институт общей и неорганической химии АН Украинской ССР | Способ получени порошка висмута электролизом |
DE2914094C2 (de) * | 1979-04-07 | 1983-02-10 | Kernforschungsanlage Jülich GmbH, 5170 Jülich | Poröse Nickelelektrode für alkalische Elektrolysen, Verfahren zur Herstellung derselben und deren Verwendung |
US4454015A (en) * | 1982-09-27 | 1984-06-12 | Aluminum Company Of America | Composition suitable for use as inert electrode having good electrical conductivity and mechanical properties |
JPS59177865A (ja) * | 1983-03-29 | 1984-10-08 | Japan Storage Battery Co Ltd | ガス拡散電極 |
GB9812169D0 (en) * | 1998-06-05 | 1998-08-05 | Univ Cambridge Tech | Purification method |
US6372099B1 (en) * | 1998-07-30 | 2002-04-16 | Moltech Invent S.A. | Cells for the electrowinning of aluminium having dimensionally stable metal-based anodes |
US6540902B1 (en) * | 2001-09-05 | 2003-04-01 | The United States Of America As Represented By The United States Department Of Energy | Direct electrochemical reduction of metal-oxides |
US6911134B2 (en) * | 2002-09-06 | 2005-06-28 | The University Of Chicago | Three-electrode metal oxide reduction cell |
-
2005
- 2005-03-03 GB GBGB0504444.1A patent/GB0504444D0/en not_active Ceased
-
2006
- 2006-03-03 US US11/817,458 patent/US20080302655A1/en not_active Abandoned
- 2006-03-03 EA EA200701896A patent/EA200701896A1/ru unknown
- 2006-03-03 JP JP2007557592A patent/JP2008531854A/ja active Pending
- 2006-03-03 CN CNA2006800137065A patent/CN101163804A/zh active Pending
- 2006-03-03 GB GBGB0604348.3A patent/GB0604348D0/en not_active Ceased
- 2006-03-03 WO PCT/GB2006/000765 patent/WO2006092615A1/fr active Application Filing
- 2006-03-03 EP EP06709988A patent/EP1866448A1/fr not_active Withdrawn
- 2006-03-03 AU AU2006219725A patent/AU2006219725A1/en not_active Abandoned
-
2007
- 2007-08-28 ZA ZA200707266A patent/ZA200707266B/xx unknown
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112941567A (zh) * | 2018-07-10 | 2021-06-11 | 东北大学 | 潮湿气氛的高温熔盐电解的电化学方法和装置 |
CN112941567B (zh) * | 2018-07-10 | 2024-02-23 | 东北大学 | 潮湿气氛的高温熔盐电解的电化学方法和装置 |
Also Published As
Publication number | Publication date |
---|---|
EA200701896A1 (ru) | 2008-02-28 |
AU2006219725A1 (en) | 2006-09-08 |
US20080302655A1 (en) | 2008-12-11 |
EP1866448A1 (fr) | 2007-12-19 |
GB0604348D0 (en) | 2006-04-12 |
JP2008531854A (ja) | 2008-08-14 |
WO2006092615A1 (fr) | 2006-09-08 |
GB0504444D0 (en) | 2005-04-06 |
ZA200707266B (en) | 2008-09-25 |
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