CN101161085A - Cold squeeze preparing technique of persic oil - Google Patents
Cold squeeze preparing technique of persic oil Download PDFInfo
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- CN101161085A CN101161085A CNA2006100480184A CN200610048018A CN101161085A CN 101161085 A CN101161085 A CN 101161085A CN A2006100480184 A CNA2006100480184 A CN A2006100480184A CN 200610048018 A CN200610048018 A CN 200610048018A CN 101161085 A CN101161085 A CN 101161085A
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- Prior art keywords
- oil
- water
- aquation
- almond
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 title claims description 12
- 239000003921 oil Substances 0.000 claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- 235000011437 Amygdalus communis Nutrition 0.000 claims abstract description 16
- 241000220304 Prunus dulcis Species 0.000 claims abstract description 16
- 235000020224 almond Nutrition 0.000 claims abstract description 16
- 230000036571 hydration Effects 0.000 claims abstract description 15
- 238000006703 hydration reaction Methods 0.000 claims abstract description 15
- 239000012535 impurity Substances 0.000 claims abstract description 12
- 229940037003 alum Drugs 0.000 claims abstract description 7
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000084 colloidal system Substances 0.000 claims abstract description 5
- 239000001944 prunus armeniaca kernel oil Substances 0.000 claims description 20
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 18
- 239000010779 crude oil Substances 0.000 claims description 18
- 239000007864 aqueous solution Substances 0.000 claims description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 14
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 14
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 238000009413 insulation Methods 0.000 claims description 8
- 238000007670 refining Methods 0.000 claims description 8
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- 229930182558 Sterol Natural products 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 150000003432 sterols Chemical class 0.000 claims description 4
- 235000003702 sterols Nutrition 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 3
- 239000011260 aqueous acid Substances 0.000 claims description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
- 239000000243 solution Substances 0.000 claims description 3
- 239000003643 water by type Substances 0.000 claims description 3
- 235000019198 oils Nutrition 0.000 abstract description 20
- 235000019489 Almond oil Nutrition 0.000 abstract description 5
- 239000008168 almond oil Substances 0.000 abstract description 5
- 238000003825 pressing Methods 0.000 abstract description 5
- -1 phosphor ester Chemical class 0.000 abstract description 2
- 239000002253 acid Substances 0.000 abstract 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 1
- 238000005202 decontamination Methods 0.000 abstract 1
- 230000003588 decontaminative effect Effects 0.000 abstract 1
- 230000007935 neutral effect Effects 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 abstract 1
- 230000035764 nutrition Effects 0.000 abstract 1
- 230000020477 pH reduction Effects 0.000 abstract 1
- 238000010422 painting Methods 0.000 abstract 1
- 235000002639 sodium chloride Nutrition 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 3
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 2
- 229930003427 Vitamin E Natural products 0.000 description 2
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- LOAUVZALPPNFOQ-UHFFFAOYSA-N quinaldic acid Chemical compound C1=CC=CC2=NC(C(=O)O)=CC=C21 LOAUVZALPPNFOQ-UHFFFAOYSA-N 0.000 description 2
- 229910052711 selenium Inorganic materials 0.000 description 2
- 239000011669 selenium Substances 0.000 description 2
- 235000011649 selenium Nutrition 0.000 description 2
- 229940046009 vitamin E Drugs 0.000 description 2
- 235000019165 vitamin E Nutrition 0.000 description 2
- 239000011709 vitamin E Substances 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- 229930195730 Aflatoxin Natural products 0.000 description 1
- XWIYFDMXXLINPU-UHFFFAOYSA-N Aflatoxin G Chemical compound O=C1OCCC2=C1C(=O)OC1=C2C(OC)=CC2=C1C1C=COC1O2 XWIYFDMXXLINPU-UHFFFAOYSA-N 0.000 description 1
- 235000002413 Prunus ansu Nutrition 0.000 description 1
- 239000005409 aflatoxin Substances 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000010729 system oil Substances 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
Almond oil cold pressing preparing technics, which is made by breaking the shell of the almond to fetch benvolence, cold pressing filter with temperature of 20 to 50 DEG C, the through three hydration of the produced semifinished oil: firstly, to implement hydration by water solution containing acid so as to remove cyanide, phosphor ester, colloid etc.; secondly, to implement hydration by alkaline water solution to remove impurity such as hard oiliness, neutral acid etc.; at last, to implement refine processing by intenerating water containing common salt and alum, the hydration temperature controls between 60 to 120 DEG C, after acidification, basification as well as water decontamination to produce almond oil. By means of the present invention, it is not only to save various nutrition components in the almond oil, but remove various harmful impurity availably, prelong storing period; apart from eat, the almond oil can be used for various business such as medical health care as well as hairdressing face-painting.
Description
Technical field
The squeezing manufacturing process, particularly cold press that the present invention relates to apricot kernel oil prepare the method for apricot kernel oil.
Background technology
Disclosed at present apricot kernel oil pressing method has the frying squeezing, the patent No.: 200410096101.x, be with almond 50～500 ℃ of temperature range fryings and push fuel-displacedly, under this high temperature, effective ingredients such as the selenium in the almond, vitamin E, Ge Su are all destroyed to be fallen; Common filtration method can not be removed water-soluble in the crude oil, oil-soluble impurities, and apricot kernel oil is become sour, and the holding time of guaranteeing the quality is shorter.
Summary of the invention
The objective of the invention is to overcome the defective that exists in the above-mentioned squeezing process, a kind of cold press preparation technology of apricot kernel oil is provided, adopt this method can keep not only that effective ingredient is not destroyed in the almond, can also remove the various impurity that influence the apricot kernel oil quality, obtain refining apricot kernel oil.
The present invention adopts low-temperature cold pressing and aquation purification techniques to produce apricot kernel oil, be that the broken shell of almond is got benevolence, squeezing, filtration, the crude oil of making is made with extra care through aquation and is removed water-soluble and oil soluble impurities such as cyanide, phosphoric acid, colloid, sterol, it is characterized in that adopting comprising that following method is prepared into refining apricot kernel oil;
A) almond is pressed in 20～50 ℃ of temperatures, filter and make the almond crude oil;
B) hydrochloric acid or phosphoric acid, sulfuric acid are added hydrochloric acid or phosphoric acid 6～12g according to per hundred kilograms of crude oils, sulfuric acid 5～10g, be added in 25～50 ℃ of hot water and make aqueous acid, again the aqueous solution is joined and carry out aquation in the crude oil, the aqueous solution: the weight ratio of crude oil is 1: 2～3.5, stir insulation 30～40 minutes under 60～80 ℃, water layer obtained aquation oil one time bottom calmness was removed;
C) with the weight of sodium carbonate according to per hundred kg of water carburetion adding, 5～15g, join the aqueous solution of making alkali in 25～50 ℃ of hot water, again the aqueous solution is added to and carries out secondary hydration in the aquation oil, aquation oil: the weight ratio of the aqueous solution is 1: 0.5～1.0, stir insulation 30～40 minutes under 60～90 ℃, water layer got secondary hydration oil bottom calmness was removed;
D) 100～120 ℃ of demineralized waters are added in the secondary hydration oil, aquation oil: the weight ratio of demineralized water is 1: 0.5～1, again salt and alum are joined in the oil solution by per hundred kg of water carburetion 100～300g salt and 6～15g alum, stir insulation 30～40 minutes under 80～100 ℃, the impurity water layer obtained refining apricot kernel oil bottom calmness was removed.
Make cyanide in the semen armeniacae amarae, aflatoxin, phosphatide, colloid, cured matter, protein, quinaldine acid, sterol etc. water-soluble and oil-soluble impurities is separated removes by aquation.
In order to regulate the taste of apricot kernel oil, optional adding citric acid in first time hydration process, it is 6～8g that per hundred kilograms of crude oils add weight.In order to improve the almond oil yield, add 2～5% water in the almond before squeezing, under 70～80 ℃, soften and handled 5～10 minutes.
Technology of the present invention compared with prior art has following advantage:
1, adopts low-temperature cold pressing technology, make refining apricot kernel oil quality-improving, preserved multiple nutrients composition in the apricot kernel oil to fancy grade;
2, adopt repeatedly aquation to make with extra care apricot kernel oil, can remove contained various objectionable impurities such as water-soluble and fat-soluble in the crude oil effectively, the storage period of having improved apricot kernel oil;
3, be rich in multiple components such as nonmetalloid selenium, linoleic acid, vitamin E, amino acid in the apricot kernel oil of the present invention's preparation, show according to product quality inspection superintendent office testing result: product of the present invention all reaches or is better than every technical indicator of edible oil, edible safety, this product is not only edible, also is widely used in every profession and trades such as medicine, health products, beauty and make-up.
Below in conjunction with the specific embodiment invention is described in detail.
Step of preparation process of the present invention is as follows:
One, raw material is selected to handle:
1, select ansu apricot nuclear, broken shell is got benevolence;
2, the softening processing: in almond, spray water, make that water content is controlled at about 2～3% in the almond, the softening processing 5～10 minutes under 70～80 ℃ of temperature.
Two, squeezing system oil
1, adopt 90 type oil presses, in 20～50 ℃, preferably 25～30 ℃ of temperatures press oil with almond;
2, adopt precipitation apparatus and plate thick stick formula squeezer to carry out the sedimentation filtration and make the almond crude oil.
Three, the apricot kernel oil aquation is refining
Select the hydrochloric acid or 90% phosphoric acid of content 32% for use, 95% sulfuric acid.
1, earlier hydrochloric acid or phosphoric acid, sulfuric acid are added hydrochloric acid or phosphoric acid 6～12g according to per hundred kilograms of crude oils, sulfuric acid 5～10g, add citric acid 6～8g, be added in 25～50 ℃ of hot water and make aqueous acid, again the aqueous solution is joined and carry out aquation in the crude oil, the aqueous solution: the weight ratio of crude oil is 1: 2～3.5, stirs down in 60～80 ℃ and is incubated 30～40 minutes, and the peaceful bottom water layer of removing obtains aquation oil one time; One time aquation can be sloughed cyanide, phosphatide, colloid and cured matter;
2, the weight that again sodium carbonate is added 5～15g according to per hundred kg of water carburetion, join the aqueous solution of making alkali in 25～50 ℃ of hot water, again the aqueous solution is added to and carries out secondary hydration in the aquation oil, aquation oil: the weight ratio of the aqueous solution is 1: 0.5～1.0, stir insulation 30～40 minutes under 60～90 ℃, water layer got secondary hydration oil bottom calmness was removed; Secondary hydration can remove impurity such as hard oil matter, quinaldine acid, sterol;
3, at last 100～120 ℃ of demineralized waters are added in the secondary hydration oil, aquation oil: the weight ratio of demineralized water is 1: 0.5～1, again salt and alum are joined in the oil solution by per hundred kg of water carburetion 100～300g salt and 6～15g alum, stir insulation 30～40 minutes under 80～100 ℃, the impurity water layer obtained refining apricot kernel oil bottom calmness was removed.
Claims (4)
1. cold squeeze preparing technique of persic oil, be that the broken shell of almond is got benevolence, squeezing, filtration, the crude oil of making is made with extra care through aquation and is removed water-soluble and oil soluble impurities such as cyanide, phosphoric acid, colloid, sterol, it is characterized in that adopting comprising that following method is prepared into refining apricot kernel oil;
A) almond is pressed in 20～50 ℃ of temperatures, filter and make the almond crude oil;
B) hydrochloric acid or phosphoric acid, sulfuric acid are added hydrochloric acid or phosphoric acid 6～12g according to per hundred kilograms of crude oils, sulfuric acid 5～10g, be added in 25～50 ℃ of hot water and make aqueous acid, again the aqueous solution is joined and carry out aquation in the crude oil, the aqueous solution: the weight ratio of crude oil is 1: 2～3.5, stir insulation 30～40 minutes under 60～80 ℃, water layer obtained aquation oil one time bottom calmness was removed;
C) with the weight of sodium carbonate according to per hundred kg of water carburetion adding, 5～15g, join the aqueous solution of making alkali in 25～50 ℃ of hot water, again the aqueous solution is added to and carries out secondary hydration in the aquation oil, aquation oil: the weight ratio of the aqueous solution is 1: 0.5～1.0, stir insulation 30～40 minutes under 60～90 ℃, water layer got secondary hydration oil bottom calmness was removed;
D) 100～120 ℃ of demineralized waters are added in the secondary hydration oil, aquation oil: the weight ratio of demineralized water is 1: 0.5～1, again salt and alum are joined in the oil solution by per hundred kg of water carburetion 100～300g salt and 6～15g alum, stir insulation 30～40 minutes under 80～100 ℃, the impurity water layer obtained refining apricot kernel oil bottom calmness was removed.
2. according to the described cold squeeze preparing technique of persic oil of claim 1, it is characterized in that selecting adding citric acid in an aquation, it is 6～8g that per hundred kilograms of crude oils add weight.
3. according to claim 1 or 2 described cold squeeze preparing technique of persic oil, add 2～5% water in the almond before it is characterized in that squeezing, under 70～80 ℃, soften and handled 5～10 minutes.
4. according to the described cold squeeze preparing technique of persic oil of claim 1, it is characterized in that described cold press temperature elects 25～30 ℃ as.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100480184A CN100554390C (en) | 2006-10-11 | 2006-10-11 | Cold squeeze preparing technique of persic oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100480184A CN100554390C (en) | 2006-10-11 | 2006-10-11 | Cold squeeze preparing technique of persic oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101161085A true CN101161085A (en) | 2008-04-16 |
| CN100554390C CN100554390C (en) | 2009-10-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100480184A Expired - Fee Related CN100554390C (en) | 2006-10-11 | 2006-10-11 | Cold squeeze preparing technique of persic oil |
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| Country | Link |
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| CN (1) | CN100554390C (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101822293A (en) * | 2010-03-30 | 2010-09-08 | 湖北襄樊九康粮油有限责任公司 | Processing method of coldly-squeezed sesame oil |
| CN101589745B (en) * | 2009-05-22 | 2013-06-05 | 西北农林科技大学 | Method for producing detoxified almond oil |
| CN104130854A (en) * | 2014-07-14 | 2014-11-05 | 新疆天鹰生物科技有限公司 | Cold oil pressing method |
| CN104673482A (en) * | 2013-12-03 | 2015-06-03 | 天津市中敖饲料有限公司 | Extraction method of pseudo-ginseng oil |
| CN106281656A (en) * | 2016-08-24 | 2017-01-04 | 张立军 | A kind of processing technique of almond oil |
-
2006
- 2006-10-11 CN CNB2006100480184A patent/CN100554390C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101589745B (en) * | 2009-05-22 | 2013-06-05 | 西北农林科技大学 | Method for producing detoxified almond oil |
| CN101822293A (en) * | 2010-03-30 | 2010-09-08 | 湖北襄樊九康粮油有限责任公司 | Processing method of coldly-squeezed sesame oil |
| CN101822293B (en) * | 2010-03-30 | 2012-09-19 | 湖北襄樊九康粮油有限责任公司 | Processing method of coldly-squeezed sesame oil |
| CN104673482A (en) * | 2013-12-03 | 2015-06-03 | 天津市中敖饲料有限公司 | Extraction method of pseudo-ginseng oil |
| CN104130854A (en) * | 2014-07-14 | 2014-11-05 | 新疆天鹰生物科技有限公司 | Cold oil pressing method |
| CN106281656A (en) * | 2016-08-24 | 2017-01-04 | 张立军 | A kind of processing technique of almond oil |
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| Publication number | Publication date |
|---|---|
| CN100554390C (en) | 2009-10-28 |
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Effective date of registration: 20190203 Address after: 122000 Twelve Tai Villages, Liucheng Street, Chaoyang County, Liaoning Province Patentee after: Chaoyang Shengkangjia Wild Apricot Development Co., Ltd. Address before: No. 185, No. 4, Zhulin Road, Chaoyang City, Liaoning Province, 122000 Patentee before: Ma Yulin |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20091028 Termination date: 20201011 |