CN101019603B - Process of producing active protein and oil with maggot and earth worm - Google Patents
Process of producing active protein and oil with maggot and earth worm Download PDFInfo
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Abstract
The process of producing active protein and oil with maggot and earthworm as material belongs to the field of feed producing technology. The automatic production process can produce full protein powder, granular full protein product, defatted protein powder, defatted granular protein product and separated maggot or earthworm oil. The production process can maintain the activity of the protein, amino acids and other active matter unchanged, raise the biological potency and digesting and absorbing rate of the products. The present invention also provides relevant large scale production process.
Description
Technical field:
The invention belongs to aquaculture production of fodder manufacturing technology field.
Background technology:
Bulk raw materials such as the required corn of production of fodder, dregs of beans, fish meal, grease account for 80% of total production cost---and 85%.These cost of material soar day by day, have increased the production cost of feed industry and aquaculture greatly.The Chinese Central Television's 7 channel experience of getting rich columns were once repeatedly reported fly maggot, earthworm protein powder process technology, but just with fly maggot or earthworm through collect, clean, dry, pulverize, packing, the albumen powder that adopts such explained hereafter to come out, its nutritional labeling and active material have suffered largely to destroy, and digestive utilization ratio in animal body is lower.Granted publication number a kind of for the Chinese patent of CN1254190C discloses " utilizing earthworm to handle the technology of the high-quality forage protein of low-quality protein production " with the screening of low-quality protein raw materials such as cottonseed cake, oil meal, mix, carries out ultramicro grinding then, and fine powder is standby; With bright earthworm screening, remove impurity such as wormcast, add water then and pull an oar, the ratio of bright earthworm and water is 5～9: 1, making beating liquid filters filtrate for later use with 20 mesh sieves; With low-quality protein raw materials fine powder, earthworm filtrate and water in 1～2: 1: 1 ratio is mixed, and reacts under certain temperature and pH value condition, per hour stirs once between the stage of reaction; After reaction is finished reactant is taken out flash baking; Pulverize after the oven dry, the product after the pulverizing is a finished product.With this feed import substitution fish meal, high-quality dregs of beans etc.What this explained hereafter obtained is finished product feedstuff, is not activated protein, more can not produce defatted active albumen and grease.In addition, be not the technological process of the large-scale continuous production activated protein of raw material also now with fly maggot, earthworm.
Summary of the invention:
The purpose of this invention is to provide a kind of method of making activated protein and grease with fly maggot, earthworm, both can produce full-cream protein powder, full-cream protein particle series of products or defatted protein powder, degreasing protein particle series of products can also be isolated fly maggot or earthworm grease simultaneously.Can keep product protein, amino acid isoreactivity material that sex change does not take place in process of production, improve the rate that digests and absorbs of the biological value (the true digestible protein of animal body) of protein product.Another object of the present invention provides the technological process of the large-scale continuous production of energy.
The inventive method is according to the following steps:
1, clean after fly maggot, earthworm raw material are collected removal of impurities, be to tell mud in 10～11 solution at pH value then, and kill the parasite of fly maggot and earthworm body surface and remove residual bait in its body.
2, the fly maggot or the earthworm that will tell after mud finishes directly sent into beater, or sends into beater again after sending into boiling vessel earlier.If send into beater again after sending into boiling vessel earlier, then in boiling vessel in 80 ℃～95 ℃ boilings 8～15 minutes.
Adopt this boiling can make the insoluble protein in maggot, the earthworm raw material keep high-load, isolated grease also can reach high-load, PH is near the isoelectric point of protein in maggot, the earthworm raw material, pressed liquor output height, oil, water and solid content good separating effect, nutritional labeling such as protein and amino acid is difficult for sex change takes place, and active component (biological value) is the highest, the effect of the sterilization that reaches a high temperature again simultaneously.
3, be full-cream protein as if what produce, then then carry out according to the following steps after the step 2: it is 6.5～7 that the slurry after will pulling an oar is transferred PH matter, add or do not add additive, after modified mixing, carry out the wet method ultramicro grinding again, carry out again obtaining the full-cream protein powder after high temperature, vacuum, the high pressure moment spray-drying, or further granulation gets the full-cream protein particle.
Can add dissimilar raw material or additive according to the difference of user's request, make this technology satisfy the requirement of production seriation, multifunctional protein product, it is minimum again production cost to be dropped to, and product quality is protected.Adopt drying process with atomizing that raw material is contacted with hot-air under high temperature, vacuum environment, produce vaporific particulate in effect following moment of high pressure again, except the purpose that reaches transpiring moisture and drying, also prevent or reduced the oxidation of grease, the decomposition of protein, amino acid whose sex change, both keep high-quality nutritional labeling, played the effect of kill virus and bacterium again.
4, be defatted protein powder and oil and fat product as if what produce, then then carry out according to the following steps after the step 2: centrifugation obtains solid content, contains the liquid phase and the oil of solid content; The liquid phase that contains solid content obtains slag, You Heshui through centrifugation; Oil and water obtain paste after evaporation and concentration.Carrying out the wet method ultramicro grinding after solid content, slag, the modified mixing of paste, carry out again obtaining defatted protein powder after high temperature, vacuum, the high pressure moment spray-drying, or further granulation gets the degreasing protein particle.Oil obtains product oil after refining.
The present invention adopts wet method, the resulting active protein series product of centrifugal process automatic production process has the full-cream protein powder, the full-cream protein particle, defatted protein powder, degreasing protein particle and grease be totally five classes, the purposes of this five series products both can be used as fish meal, dregs of beans, digested tankage, blood meal, dried silkworm chrysalis meal, wheat bran, rice bran, rapeseed dregs, peanut meal, rapeseed oil, lard, the substitute of of animal or plant nature albumen such as butter or energy feed raw material, be processed into mixed feed after also can cooperating, be used for livestock and poultry with other feedstuff such as corn, the breed of aquaculture and economic animal.Wherein also contain fly maggot antibacterial protein (claiming antibacterial peptide again), unrighted acid (palmitic acid, palmitin oleic acid), linoleic acid, leukotrienes, agglutinin in the protein product, various active materials such as earthworm enzyme, terrestro-lumbrolysin, earthworm antibacterial peptide (acid four decapeptides), nucleic acid derivative.These active materials to letting animals feed all have anti-inflammation, analgesic, calm, end dysentery, relieving asthma, strengthen immunity of organism, improve effects such as efficiency of feed utilization and raising production performance; After in feed, using this product in 5%～20% ratio, to swine enzootic pneumonia, chronic respiratory disease, the intestines problem of the red dysentery characterized by white mucous stool of pigling, white diarrhea, global-worm illness and fish etc., prevention and supplemental treatment effect are preferably arranged, can reduce or without antibiotics, obvious effect be arranged improving livestock and poultry, aquatic products growth rate and improving the animal products quality.
Good effect of the present invention: both can produce full-cream protein powder, full-cream protein particle series of products or defatted protein powder, degreasing protein particle series of products can also be isolated fly maggot or earthworm grease simultaneously.Can keep product protein, amino acid isoreactivity material that sex change does not take place in process of production, improve the rate that digests and absorbs of the biological value of protein product, and the technological process of the large-scale continuous production of energy is provided.
The present invention adopts wet method, centrifugal process production technology, fly maggot, earthworm are manufactured activated protein and grease substitutes expensive fish meal and other animal protein and energy feed raw material, this product is applied in the feed formula design, compare with conventional composition of raw materials, can make the formulation cost pancake of fish meal per ton hang down 200～300 yuan; Wherein, No. 1 material of grass carp and carp (fish fry material) is 300～400 yuan/ton; No. 2 material and No. 3 material are 200～300 yuan/ton; To animal and fowl fodder, on average can reduce by 80～150 yuan/ton.In addition, the product nutrient easily satisfies the designing requirement of standard formula, applied widely, can be applied in the feed in animal-breeding fields such as livestock and poultry, aquatic products, except that can substituting animal plant feedstufves such as fish meal and portion of energy feed, can also substitute part or directly substitute antibiotics feed medicated premix, to preventing or reduce the generation of livestock and poultry, aquaculture Animal diseases, improve livestock and poultry, aquatic product quality has obvious effect, meets the world, the development trend that pollution-free food was cultured and produced in nuisanceless animal husbandry is greatly developed in domestic requirement.Can be used in idol and play in class animal and other livestock and poultry and the aquaculture, not have " rabid ox disease " factor.Low cost of manufacture, the cost of producing 1 kilogram of activated protein only is 1/4 of a fish meal price, 1/2 of digested tankage and blood meal, 3/5 of dregs of beans.
Description of drawings
Fig. 1 is the process chart of embodiment.
The specific embodiment
Embodiment: see technological process shown in Figure 1.To collect the fly maggot or the earthworm of (1) through raw material and clean removal of impurities (2), in telling mud device (3), be added with quick lime, adjust pH is 10～11, fly maggot or earthworm are sent in first storage bin (4) standby by conveying worm after containing telling of quick lime solution and stopping 10～15 minutes in the mud device.First valve (5) of first storage bin (4) discharging opening and second valve (6) are respectively applied for control beater (7) and boiling vessel (8) opening or closing when raw material is carried.Boiling vessel (8) adopts high temperature or isoelectric point cooking process, keeps 80 ℃～95 ℃ of vapor (steam) temperatures, boiling 8～15 minutes.Boiling vessel can adopt the automatic feed of stainless steel cylindrical multi-layer, discharging and temperature regulating device, also can adopt to be used to make the required multilayer boiling vessel of aquatic granulated feed in the existing feed manufacturing industry and to substitute.Place the pipe magnetic separator (9) at beater (7) discharging opening place to be used for removing the metallics that raw material is carried secretly after beater (7) making beating.First storage tank (10) is used to store slurries, is welded by stainless steel material, adds the material of adjust pH in first storage tank (10), and as sodium acid carbonate, phosphoric acid or salt acid starting material, adjust pH are 6～7.Open first control valve (11) of first storage tank (10) discharging opening slurries are sent into storage in second storage tank (12), in second storage tank, can add dissimilar additives according to the difference of user's request, make this technology satisfy the requirement of production seriation, multifunctional protein product, it is minimum again production cost to be dropped to, and product quality is protected.The additive that adds in second storage tank (12) can be for the compound additive of antioxidant or calcic, P elements etc.After adding additive, send in the modified mixer (13) by feeder, through modified mixing in 7～12 minutes, in sending into micronizer (14), adopts by conveying worm wet method low temperature ultramicro grinding technology, raw material 90% is by 60～120 mesh standard sieves, and pulverizer (14) discharging opening is provided with pipe magnetic separator (9) in order to remove the metal impurities in the material.In sending into spray dryer (15), conveying worm carries out high temperature, vacuum, high pressure moment spray-drying.Drying equipment can be selected two types of press atomization or centrifugal sprays for use.The product that obtains after spray-dried is sent in the storage bin (16) standby by elevator.Control valve (17), (29) of storage bin (16) discharging opening are respectively applied for control and make opening or closing of particulate material or powder product technology needed raw material; Open control valve (29) when producing powder, closed control valve (17), through weighing (23), packing (24), check (25), press activated protein and oil and fat product sense organ identification beacon (table 1) during check, product nutritional labeling and physical and chemical index (table 2), 17 kinds of micronutrient levels of activated protein product (table 3), fly maggot, earthworm oil fatty acid component content (table 4), activated protein product sanitary index (table 5) carries out.(28) are sold in finished product (26) warehouse-in (27) back, are the production process of full-cream protein powder.Open the control valve (17) of storage bin (16) discharging opening when producing the full-cream protein grain products and closed control valve (29), material is imported granulation in the comminutor (18) through conveyer, the material after the granulation is divided into (22) two kinds of particulate material (20) and powders through screen analysis (19); Particulate material drying machine (21) drying, drying equipment can adopt two types in hot blast or cold wind; Powder (22) is sent into through conveyer and is turned back to granulation in the comminutor (18) in the storage bin (16) again; The dry good particulate material of drying machine (21) is through weighing (23), packing 24, check (25), and checkout procedure is identical with the production albumen powder.When producing defatted protein powder and oil and fat product, open the discharging opening control valve (30) of storage tank (10), closed control valve (11) is sent into horizontal centrifuge through feeder and is carried out centrifugation (31), obtain solid content (32), contain solid content liquid phase (33) and oil (34).Liquid phase (33) obtains slag (36) and oil water mixture (37) through vertical centrifugal machine (35) separation; Oil water mixture (37) obtains paste (39) after multi-effect evaporator concentrates (38), through conveyer solid content (32), slag (36), paste (39) are sent in the storage tank (12), can be produced defatted protein powder or degreasing protein particle according to the subsequent process of full-cream protein powder or full-cream protein particle again.Oil (34) obtains product oil (41), gets finished product (26) through weighing (42), can (43), check (25) again after refining (40).Clean knot screen (2) and tell mud device (3) and all be connected with sewage disposal device (45) by blow-off line, blow-off pipe is provided with blowoff valve (44), after producing end, open blowoff valve (44) sewage discharge is handled sewage in sewage disposal device (45), sewage is capable of circulation after treatment to be used for the cleaning of fly maggot, earthworm or the irrigation of crops is used.
Activated protein target level of product quality and check thereof: see activated protein and oil and fat product sense organ identification beacon (table 1), product nutritional labeling and physical and chemical index (table 2), 17 kinds of micronutrient levels of activated protein product (table 3), fly maggot, earthworm oil fatty acid component content (table 4), activated protein product sanitary index (table 5).Use to feed manufacturers and plant through promptly can be applicable to feed preparation or direct marketing after the assay was approved.
Table 1: activated protein and oil and fat product sense organ identification beacon
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Table 2: activated protein product physical and chemical index (theoretical estimated value)
Table 3: 17 kinds of micronutrient levels of activated protein product (PPM)
Table 4: fly maggot, earthworm oil fatty acid component content
Table 5: activated protein product sanitary index
Present embodiment uses and shows; can effectively solve current feed industry, the required animal protein raw material imbalance between supply and demand in short supply of livestock breeding industry; product safety, economy, environmental protection, high-quality, nutritious, biological value is high, also can satisfy scale continuous uninterrupted modern production requirement.
Claims (3)
1. make the method for activated protein and grease with fly maggot, earthworm for one kind, it is characterized in that according to the following steps:
(1), clean removal of impurities after fly maggot, earthworm raw material collected, be to tell mud in 10～11 solution in pH value then, kill the parasite of fly maggot and earthworm body surface and remove the interior residual bait of its body;
(2), the fly maggot or the earthworm that will tell after mud finishes directly send into beater, or sends into beater again after sending into boiling vessel earlier, if send into beater again after sending into boiling vessel earlier, then in boiling vessel in 80 ℃～95 ℃ boilings 8～15 minutes;
(3), be full-cream protein as if what produce, then then carry out according to the following steps after the step 2: the slurry adjust pH after will pulling an oar is 6.5～7, add or do not add additive, after modified mixing, carry out the wet method ultramicro grinding again, carry out again obtaining the full-cream protein powder after high temperature, vacuum, the high pressure moment spray-drying, or further the granulation of full-cream protein powder is got the full-cream protein particle;
(4), if what produce is defatted protein powder and oil and fat product, then then carry out according to the following steps after the step 2: centrifugation obtains solid content, contains the liquid phase and the oil of solid content; The liquid phase that contains solid content obtains slag, You Heshui through centrifugation; Oil and water obtain paste after evaporation and concentration, carrying out the wet method ultramicro grinding after solid content, slag, the modified mixing of paste, carry out obtaining defatted protein powder after high temperature, vacuum, the high pressure moment spray-drying, or further granulation gets the degreasing protein particle again; Oil obtains product oil after refining.
2. as the said method of claim 1, it is characterized in that according to the following steps:
To collect the fly maggot or the earthworm of (1) through raw material and clean removal of impurities (2), in telling mud device (3), be added with quick lime, adjust pH is 10～11, fly maggot or earthworm are sent in first storage bin (4) standby by conveying worm after containing telling of quick lime solution and stopping 10～15 minutes in the mud device; First valve (5) of first storage bin (4) discharging opening and second valve (6) are respectively applied for control beater (7) and boiling vessel (8) opening or closing when raw material is carried; Boiling vessel (8) adopts high temperature or isoelectric point cooking process, keeps 80 ℃～95 ℃ of vapor (steam) temperatures, boiling 8～15 minutes; Place the pipe magnetic separator (9) at beater (7) discharging opening place to be used for removing the metallics that raw material is carried secretly after beater (7) making beating; First storage tank (10) is used to store slurries, is welded by stainless steel material; In first storage tank (10), add the material of transferring p H value, adjust pH is 6～7, open first storage tank (10) discharging opening first control valve (11) slurries are sent into storage in second storage tank (12), after adding additive, send in the modified mixer (13) by feeder, through modified mixing in 7～12 minutes, in sending into micronizer (14), conveying worm carries out wet method low temperature ultramicro grinding, material 90% is by 60～120 mesh standard sieves, and pulverizer (14) discharging opening is provided with pipe magnetic separator (9) in order to remove the metal impurities in the material; In sending into spray dryer (15), conveying worm carries out high temperature, vacuum, high pressure moment spray-drying; The product that obtains after spray-dried is sent in second storage bin (16) standby by elevator; The 3rd control valve (17) of second storage bin (16) discharging opening, the 4th control valve (29) are respectively applied for control and make opening or closing of particulate material or powder product technology needed raw material; Open the 4th control valve (29) when producing powder, close the 3rd control valve (17),, get the full-cream protein powder through weighing (23), packing (24), check (25); Open the 3rd control valve (17) of second storage bin (16) discharging opening when producing the full-cream protein grain products and close the 4th control valve (29), material is imported granulation in the comminutor (18) through conveyer, the material after the granulation is divided into (22) two kinds of particulate material (20) and powders through screen analysis (19); Particulate material drying machine (21) drying; Powder (22) is sent into through conveyer and is turned back to granulation in the comminutor (18) in second storage bin (16) again; The dry good particulate material of drying machine (21) is through weighing (23), packing 24, check (25); When producing defatted protein powder and oil and fat product, open discharging opening second control valve (30) of first storage tank (10), close discharging opening first control valve (11) of first storage tank (10), send into horizontal centrifuge through feeder and carry out centrifugation (31), obtain solid content (32), contain solid content liquid phase (33) and oil (34); Liquid phase (33) obtains slag (36) and oil water mixture (37) through vertical centrifugal machine (35) separation; Oil water mixture (37) obtains paste (39) after multi-effect evaporator concentrates (38), through conveyer solid content (32), slag (36), paste (39) are sent in second storage tank (12), can be produced defatted protein powder or degreasing protein particle according to the subsequent process of full-cream protein powder or full-cream protein particle again; Oil (34) obtains product oil (41), gets finished product (26) through weighing (42), can (43), check (25) again after refining (40); Clean knot screen (2) and tell mud device (3) and all be connected with sewage disposal device (45) by blow-off line, blow-off pipe is provided with blowoff valve (44), after producing end, open blowoff valve (44) sewage discharge is handled sewage in sewage disposal device (45), sewage is capable of circulation after treatment to be used for the cleaning of fly maggot, earthworm or the irrigation of crops is used.
3. as the said method of claim 2, it is characterized in that boiling vessel adopts the automatic feed of stainless steel cylindrical multi-layer, discharging and temperature regulating device, or be used to make the required multilayer boiling of aquatic granulated feed in the existing feed manufacturing industry of employing, the material that adds adjust pH in first storage tank (10) is a sodium acid carbonate, phosphoric acid or hydrochloric acid, spray dryer are press atomization or centrifugal spray.
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| CN101805672B (en) * | 2010-03-08 | 2012-01-25 | 中山大学 | Biodiesel and preparation method thereof |
| CN102796611A (en) * | 2012-07-17 | 2012-11-28 | 浙江省长三角循环经济技术研究院 | Soaking extraction process for maggot oil |
| CN102827689A (en) * | 2012-07-17 | 2012-12-19 | 浙江省长三角循环经济技术研究院 | Maggot oil preparation process |
| CN104137943A (en) * | 2013-05-07 | 2014-11-12 | 王虎生 | A continuous production method of high-activity fly maggot protein powder |
| CN106892961A (en) * | 2017-02-14 | 2017-06-27 | 广西肽王生物科技有限公司 | A kind of separating and extracting process of fly-maggot protein polypeptide and fly maggot oil |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1141130A (en) * | 1995-12-18 | 1997-01-29 | 武汉神虫珍奇养生制品有限公司 | Nutrient active matter dried powder of edible engineering maggot, method for producing same |
| CN1297691A (en) * | 1999-12-01 | 2001-06-06 | 中国科学院动物研究所 | Separation and extraction process of effective component in resource insect |
| CN1415757A (en) * | 2002-11-20 | 2003-05-07 | 江南大学 | Method for extracting protein and chitin from fly maggot by using enzyme hydrolysis as well as preparing chitosan from chitin |
| CN1657098A (en) * | 2004-02-20 | 2005-08-24 | 北京百奥药业有限责任公司 | Preparation method of earthworm kinase dry powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1141130A (en) * | 1995-12-18 | 1997-01-29 | 武汉神虫珍奇养生制品有限公司 | Nutrient active matter dried powder of edible engineering maggot, method for producing same |
| CN1297691A (en) * | 1999-12-01 | 2001-06-06 | 中国科学院动物研究所 | Separation and extraction process of effective component in resource insect |
| CN1415757A (en) * | 2002-11-20 | 2003-05-07 | 江南大学 | Method for extracting protein and chitin from fly maggot by using enzyme hydrolysis as well as preparing chitosan from chitin |
| CN1657098A (en) * | 2004-02-20 | 2005-08-24 | 北京百奥药业有限责任公司 | Preparation method of earthworm kinase dry powder |
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