CN101012131A - Method of manufacturing ice-crystal glaze - Google Patents

Method of manufacturing ice-crystal glaze Download PDF

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Publication number
CN101012131A
CN101012131A CN 200710034392 CN200710034392A CN101012131A CN 101012131 A CN101012131 A CN 101012131A CN 200710034392 CN200710034392 CN 200710034392 CN 200710034392 A CN200710034392 A CN 200710034392A CN 101012131 A CN101012131 A CN 101012131A
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CN
China
Prior art keywords
glaze
oxide
ball
calcite
crystal
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Granted
Application number
CN 200710034392
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Chinese (zh)
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CN100432028C (en
Inventor
潘俊明
张袆一
曾日伦
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HUNAN TAIXIN CERAMICS CO Ltd
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HUNAN TAIXIN CERAMICS CO Ltd
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Application filed by HUNAN TAIXIN CERAMICS CO Ltd filed Critical HUNAN TAIXIN CERAMICS CO Ltd
Priority to CNB2007100343923A priority Critical patent/CN100432028C/en
Publication of CN101012131A publication Critical patent/CN101012131A/en
Application granted granted Critical
Publication of CN100432028C publication Critical patent/CN100432028C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The invention discloses a making method of ice-crystal glaze, which comprises the following steps: adopting zinc oxide, lithium carbonate, titanium oxide, calcite, transparent fused block, kaolin, quartz flour and copper oxide as raw material with copper oxide as coloring oxide; balling through wet method; sieving; allocating slurry with density at 45-65 Baume's degree; fetching smooth ceramic blank to immerse glaze in the kiln; sintering in the oxidizing atmosphere under 1160-1200 deg.c rapidly; obtaining the product with glitter surface.

Description

A kind of method of manufacturing ice-crystal glaze
Technical field
The present invention relates to a kind of preparation method of ice crystal glaze.
Background technology
In the porcelain industry, it is very important that base substrate is made moulding, the allotment of glaze more can demonstrate the attractive in appearance of product, the base substrate of same moulding, often produce Different Effects because of the different visions of overglaze to the human consumer, the sort of sparkling and crystal-clear moist and strange and new visual effect, exquisite perfection of more apparent product and fashion.
Summary of the invention
The objective of the invention is to prepare and a kind ofly can in 1180-1200 ℃ oxidizing atmosphere, burn till ice crystal overglaze glaze fast, described ice crystal glaze is to gain the name to form a kind of similar frost flower shape crystallization material in the glaze, ice crystal glaze crystallization is greatly brilliant and spread all over whole glaze and unusual, and its crystalline substance spends big diameter can reach 10mm.Just as pure white crystalline frost flower, frost flower flicker has sparkling and crystal-clear glossyly so-called ice crystal glaze, gives the people a kind of pure and noble, the sense of pretty ease elegance under irradiate light.
A kind of method of manufacturing ice-crystal glaze is characterized in that: get the raw materials ready by following prescription (1): zinc oxide 15~20%, Quilonum Retard 8~15%, titanium oxide 8~13%, calcite 15~20%, clear frit 5~8%, kaolin 13~20%, silica powder 20~35%, cupric oxide 0.1~1.5%; Each component percentage composition sum is 100%; Clear frit in getting the raw materials ready is commercially available dedicated transparent frit, adopts cupric oxide as coloring oxide.
(2) wet ball grinding 12-14 hour, selected material: ball: water=1: 1.5: 0.6;
(3) glaze behind the ball milling is crossed 200 mesh sieves, again the slurry of furnishing concentration 45~65 degree Beaume;
(4) get the bright and clean porcelain base substrate of appearance and soak glaze and go into to burn till fast roller kiln, under 1180~1200 ℃ oxidizing atmosphere, fire.
That is to say that the ice crystal glaze is immersed in the present invention on bright and clean porcelain base substrate goods top layer, glaze layer thickness 0.2-0.4mm burns till by burning till roller kiln fast; Gained finished product porcelain surface glaze layer has frost flower shape decorative effect.
Embodiment
By following formulated ice crystal glaze (described raw material all is a technical grade): zinc oxide 17%, Quilonum Retard 10%, titanium oxide 9%, calcite 16%, clear frit 6%, kaolin 16%, silica powder 25%, cupric oxide 1%; Carried out selected material: ball: water=1: 1.5: 0.6 wet ball grinding 12-14 hour; Glaze behind the ball milling is crossed 200 mesh sieves, again the slurry of furnishing concentration 45~65 degree Beaume; Get the bright and clean porcelain base substrate of appearance and soak glaze and go into to burn till fast roller kiln, under the oxidizing atmospheres of 1180~1200 degree, fire and form.The flicker of gained glaze frost flower, sparkling and crystal-clear glossy, give a kind of pure and noble sense of people.

Claims (1)

1, the making method of ice crystal glaze is characterized in that:
(1) get the raw materials ready by following prescription:
Zinc oxide 15~20% Quilonum Retards 8~15% titanium oxide 8~13%
Calcite 15~20% clear frits 5~8% kaolin 13~20%
Silica powder 20~35% cupric oxide 0.1~1.5%;
Each component percentage composition sum is 100%;
(2) wet ball grinding 12-14 hour, selected material: ball: water=1: 1.5: 0.6;
(3) glaze behind the ball milling is crossed 200 mesh sieves, again the slurry of furnishing concentration 45~65 degree Beaume;
(4) get the bright and clean porcelain base substrate of appearance and soak glaze and go into to burn till fast roller kiln, under 1180~1200 ℃ oxidizing atmosphere, fire.
CNB2007100343923A 2007-02-07 2007-02-07 Method of manufacturing ice-crystal glaze Expired - Fee Related CN100432028C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2007100343923A CN100432028C (en) 2007-02-07 2007-02-07 Method of manufacturing ice-crystal glaze

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2007100343923A CN100432028C (en) 2007-02-07 2007-02-07 Method of manufacturing ice-crystal glaze

Publications (2)

Publication Number Publication Date
CN101012131A true CN101012131A (en) 2007-08-08
CN100432028C CN100432028C (en) 2008-11-12

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Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2007100343923A Expired - Fee Related CN100432028C (en) 2007-02-07 2007-02-07 Method of manufacturing ice-crystal glaze

Country Status (1)

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CN (1) CN100432028C (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102515857A (en) * 2011-12-14 2012-06-27 广东松发陶瓷股份有限公司 Leadless ceramic glaze and its preparation method
CN110316968A (en) * 2019-08-13 2019-10-11 江西陶瓷工艺美术职业技术学院 It is a kind of to burn polymorphic multicolour crystalline glaze and its preparation method and application fastly
CN110407217A (en) * 2019-08-29 2019-11-05 淄博三锐陶瓷科技有限公司 The method of the waste lithium cell positive electrode preparation high light inorganic material of nanometer
CN111003942A (en) * 2020-01-08 2020-04-14 湖南泰鑫瓷业有限公司 Frost crystal glaze and preparation method thereof
CN112225453A (en) * 2020-09-10 2021-01-15 醴陵陶润实业发展有限公司 Crystalline glaze and preparation method thereof
CN114426397A (en) * 2022-01-10 2022-05-03 蒙娜丽莎集团股份有限公司 Preparation method of snow-powder fritted glaze and ceramic tile with snow-powder effect

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1096499A (en) * 1993-06-14 1994-12-21 杨智敏 Colour glazed sand for building
CN1440944A (en) * 2003-04-04 2003-09-10 张连峰 Prepn of bake-free glaze

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102515857A (en) * 2011-12-14 2012-06-27 广东松发陶瓷股份有限公司 Leadless ceramic glaze and its preparation method
CN110316968A (en) * 2019-08-13 2019-10-11 江西陶瓷工艺美术职业技术学院 It is a kind of to burn polymorphic multicolour crystalline glaze and its preparation method and application fastly
CN110407217A (en) * 2019-08-29 2019-11-05 淄博三锐陶瓷科技有限公司 The method of the waste lithium cell positive electrode preparation high light inorganic material of nanometer
CN111003942A (en) * 2020-01-08 2020-04-14 湖南泰鑫瓷业有限公司 Frost crystal glaze and preparation method thereof
CN112225453A (en) * 2020-09-10 2021-01-15 醴陵陶润实业发展有限公司 Crystalline glaze and preparation method thereof
CN114426397A (en) * 2022-01-10 2022-05-03 蒙娜丽莎集团股份有限公司 Preparation method of snow-powder fritted glaze and ceramic tile with snow-powder effect
CN114426397B (en) * 2022-01-10 2023-01-24 蒙娜丽莎集团股份有限公司 Preparation method of snow-powder fritted glaze and ceramic tile with snow-powder effect

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Publication number Publication date
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Granted publication date: 20081112