CN100559962C - A kind of preparation method of dry water plant powder - Google Patents
A kind of preparation method of dry water plant powder Download PDFInfo
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- CN100559962C CN100559962C CNB2007100707934A CN200710070793A CN100559962C CN 100559962 C CN100559962 C CN 100559962C CN B2007100707934 A CNB2007100707934 A CN B2007100707934A CN 200710070793 A CN200710070793 A CN 200710070793A CN 100559962 C CN100559962 C CN 100559962C
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- water plant
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- plant powder
- water
- dry
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 65
- 239000000843 powder Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 241000196324 Embryophyta Species 0.000 claims abstract description 51
- 206010033546 Pallor Diseases 0.000 claims abstract description 16
- 239000013505 freshwater Substances 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 239000003963 antioxidant agent Substances 0.000 claims description 20
- 230000003078 antioxidant effect Effects 0.000 claims description 20
- 235000006708 antioxidants Nutrition 0.000 claims description 20
- 244000207867 Pistia stratiotes Species 0.000 claims description 18
- 235000006440 Pistia stratiotes Nutrition 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 18
- 244000207740 Lemna minor Species 0.000 claims description 17
- 235000006439 Lemna minor Nutrition 0.000 claims description 17
- 235000001855 Portulaca oleracea Nutrition 0.000 claims description 17
- 239000007864 aqueous solution Substances 0.000 claims description 14
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical compound CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 12
- 239000012065 filter cake Substances 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 11
- 238000005119 centrifugation Methods 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 8
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 8
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 7
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 claims description 6
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid group Chemical group C(C1=CC=CC=C1)(=O)O WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 6
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 6
- VZCYOOQTPOCHFL-OWOJBTEDSA-N fumaric acid group Chemical group C(\C=C\C(=O)O)(=O)O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims description 6
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 6
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 claims description 6
- 239000004250 tert-Butylhydroquinone Substances 0.000 claims description 6
- 235000019281 tert-butylhydroquinone Nutrition 0.000 claims description 6
- 235000017879 Nasturtium officinale Nutrition 0.000 claims description 5
- 240000005407 Nasturtium officinale Species 0.000 claims description 5
- 239000000839 emulsion Substances 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- KNENSDLFTGIERH-UHFFFAOYSA-N 2,2,4,4-tetramethyl-3-phenylpentan-3-ol Chemical compound CC(C)(C)C(O)(C(C)(C)C)C1=CC=CC=C1 KNENSDLFTGIERH-UHFFFAOYSA-N 0.000 claims description 4
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 4
- 239000004258 Ethoxyquin Substances 0.000 claims description 4
- 240000001085 Trapa natans Species 0.000 claims description 4
- 229930003268 Vitamin C Natural products 0.000 claims description 4
- 159000000007 calcium salts Chemical class 0.000 claims description 4
- 235000019285 ethoxyquin Nutrition 0.000 claims description 4
- DECIPOUIJURFOJ-UHFFFAOYSA-N ethoxyquin Chemical group N1C(C)(C)C=C(C)C2=CC(OCC)=CC=C21 DECIPOUIJURFOJ-UHFFFAOYSA-N 0.000 claims description 4
- 229940093500 ethoxyquin Drugs 0.000 claims description 4
- 159000000003 magnesium salts Chemical class 0.000 claims description 4
- 230000003204 osmotic effect Effects 0.000 claims description 4
- 235000010388 propyl gallate Nutrition 0.000 claims description 4
- 235000009165 saligot Nutrition 0.000 claims description 4
- 239000002002 slurry Substances 0.000 claims description 4
- 229940079827 sodium hydrogen sulfite Drugs 0.000 claims description 4
- 235000010265 sodium sulphite Nutrition 0.000 claims description 4
- 235000019154 vitamin C Nutrition 0.000 claims description 4
- 239000011718 vitamin C Substances 0.000 claims description 4
- 150000003751 zinc Chemical class 0.000 claims description 4
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 3
- 239000005711 Benzoic acid Substances 0.000 claims description 3
- 235000011054 acetic acid Nutrition 0.000 claims description 3
- 235000010233 benzoic acid Nutrition 0.000 claims description 3
- LDCRTTXIJACKKU-ONEGZZNKSA-N dimethyl fumarate Chemical compound COC(=O)\C=C\C(=O)OC LDCRTTXIJACKKU-ONEGZZNKSA-N 0.000 claims description 3
- 229960004419 dimethyl fumarate Drugs 0.000 claims description 3
- OPGYRRGJRBEUFK-UHFFFAOYSA-L disodium;diacetate Chemical compound [Na+].[Na+].CC([O-])=O.CC([O-])=O OPGYRRGJRBEUFK-UHFFFAOYSA-L 0.000 claims description 3
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims description 3
- 235000019253 formic acid Nutrition 0.000 claims description 3
- 239000001530 fumaric acid Substances 0.000 claims description 3
- 235000019260 propionic acid Nutrition 0.000 claims description 3
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical group O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 3
- 239000001632 sodium acetate Substances 0.000 claims description 3
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 3
- 239000004299 sodium benzoate Substances 0.000 claims description 3
- 235000010234 sodium benzoate Nutrition 0.000 claims description 3
- 235000017454 sodium diacetate Nutrition 0.000 claims description 3
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 claims description 3
- 235000010262 sodium metabisulphite Nutrition 0.000 claims description 3
- 235000010199 sorbic acid Nutrition 0.000 claims description 3
- 239000004334 sorbic acid Substances 0.000 claims description 3
- 229940075582 sorbic acid Drugs 0.000 claims description 3
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 235000015165 citric acid Nutrition 0.000 claims description 2
- 150000001879 copper Chemical class 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 159000000000 sodium salts Chemical class 0.000 claims description 2
- 240000003826 Eichhornia crassipes Species 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 7
- 230000008901 benefit Effects 0.000 abstract description 5
- 238000005265 energy consumption Methods 0.000 abstract description 4
- 235000016709 nutrition Nutrition 0.000 abstract description 4
- 240000008042 Zea mays Species 0.000 abstract description 2
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 abstract description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 abstract description 2
- 235000005822 corn Nutrition 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 239000002932 luster Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 235000012054 meals Nutrition 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 108010082495 Dietary Plant Proteins Proteins 0.000 abstract 1
- 240000004658 Medicago sativa Species 0.000 abstract 1
- 235000017587 Medicago sativa ssp. sativa Nutrition 0.000 abstract 1
- 244000046052 Phaseolus vulgaris Species 0.000 abstract 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 abstract 1
- 244000144972 livestock Species 0.000 abstract 1
- 238000012856 packing Methods 0.000 abstract 1
- 244000144977 poultry Species 0.000 abstract 1
- 241000169203 Eichhornia Species 0.000 description 21
- 241001465754 Metazoa Species 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 3
- 241000195493 Cryptophyta Species 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 210000000170 cell membrane Anatomy 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 230000037213 diet Effects 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 230000002147 killing effect Effects 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 239000004289 sodium hydrogen sulphite Substances 0.000 description 2
- 239000003643 water by type Substances 0.000 description 2
- 208000019901 Anxiety disease Diseases 0.000 description 1
- 239000002028 Biomass Substances 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 101710138460 Leaf protein Proteins 0.000 description 1
- 102000004316 Oxidoreductases Human genes 0.000 description 1
- 108090000854 Oxidoreductases Proteins 0.000 description 1
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 229930003451 Vitamin B1 Natural products 0.000 description 1
- 229930003779 Vitamin B12 Natural products 0.000 description 1
- 229930003471 Vitamin B2 Natural products 0.000 description 1
- LXNHXLLTXMVWPM-UHFFFAOYSA-N Vitamin B6 Natural products CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 230000036506 anxiety Effects 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 description 1
- 239000001639 calcium acetate Substances 0.000 description 1
- 235000011092 calcium acetate Nutrition 0.000 description 1
- 229960005147 calcium acetate Drugs 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- AGVAZMGAQJOSFJ-WZHZPDAFSA-M cobalt(2+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+2].N#[C-].[N-]([C@@H]1[C@H](CC(N)=O)[C@@]2(C)CCC(=O)NC[C@@H](C)OP(O)(=O)O[C@H]3[C@H]([C@H](O[C@@H]3CO)N3C4=CC(C)=C(C)C=C4N=C3)O)\C2=C(C)/C([C@H](C\2(C)C)CCC(N)=O)=N/C/2=C\C([C@H]([C@@]/2(CC(N)=O)C)CCC(N)=O)=N\C\2=C(C)/C2=N[C@]1(C)[C@@](C)(CC(N)=O)[C@@H]2CCC(N)=O AGVAZMGAQJOSFJ-WZHZPDAFSA-M 0.000 description 1
- 229910000365 copper sulfate Inorganic materials 0.000 description 1
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
- 235000020247 cow milk Nutrition 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- WBZKQQHYRPRKNJ-UHFFFAOYSA-N disulfurous acid Chemical compound OS(=O)S(O)(=O)=O WBZKQQHYRPRKNJ-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- 210000000416 exudates and transudate Anatomy 0.000 description 1
- 235000011087 fumaric acid Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000000819 hypertonic solution Substances 0.000 description 1
- 229940021223 hypertonic solution Drugs 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- WALYXZANOBBHCI-UHFFFAOYSA-K magnesium sodium trichloride hydrate Chemical compound O.[Cl-].[Na+].[Mg+2].[Cl-].[Cl-] WALYXZANOBBHCI-UHFFFAOYSA-K 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- RADKZDMFGJYCBB-UHFFFAOYSA-N pyridoxal hydrochloride Natural products CC1=NC=C(CO)C(C=O)=C1O RADKZDMFGJYCBB-UHFFFAOYSA-N 0.000 description 1
- ZUFQODAHGAHPFQ-UHFFFAOYSA-N pyridoxine hydrochloride Chemical compound Cl.CC1=NC=C(CO)C(CO)=C1O ZUFQODAHGAHPFQ-UHFFFAOYSA-N 0.000 description 1
- 229960002477 riboflavin Drugs 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 235000015424 sodium Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229910000679 solder Inorganic materials 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229960003495 thiamine Drugs 0.000 description 1
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 230000007723 transport mechanism Effects 0.000 description 1
- AVBGNFCMKJOFIN-UHFFFAOYSA-N triethylammonium acetate Chemical compound CC(O)=O.CCN(CC)CC AVBGNFCMKJOFIN-UHFFFAOYSA-N 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000010374 vitamin B1 Nutrition 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
- 235000019163 vitamin B12 Nutrition 0.000 description 1
- 239000011715 vitamin B12 Substances 0.000 description 1
- 235000019164 vitamin B2 Nutrition 0.000 description 1
- 239000011716 vitamin B2 Substances 0.000 description 1
- 235000019158 vitamin B6 Nutrition 0.000 description 1
- 239000011726 vitamin B6 Substances 0.000 description 1
- 229940011671 vitamin b6 Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000004246 zinc acetate Substances 0.000 description 1
Landscapes
- Cultivation Of Plants (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a kind of preparation method of dry water plant powder, it be the fresh water plant that will gather through chopping, blanching complete, permeating and dewatering, slurrying, filtration, oven dry, metering, packing make dry water plant powder; Preparation method's operating condition gentleness of the present invention, energy consumption are little, are easy to realize extensive chemical industry production; Compare with existing dry water plant powder preparation method, the constant product quality that the inventive method makes, and the original local flavor of water plant, color and luster and nutritional quality have been kept, can all or part of alternative corn, vegetable protein such as dregs of beans, alfalfa meal is used for livestock and poultry, aquatic feeds, for feed resource exploitation, solution water pollute practical measures is provided, has good economic and social benefit.
Description
Technical field
The present invention relates to water plant recycling field, relate in particular to a kind of preparation method of dry water plant powder.
Background technology
Utilize that high water plant such as water hyacinth, water lettuce and duckweed etc. are harnessed a river, the eutrophication of lake, pond and reservoir is a kind of very fruitful method: the nutriment that high water plants such as (1) water hyacinth, water lettuce and duckweed can absorb in the water body fast in a large number is required for self growth, their root exudates has inhibition or killing action to algae, germ, can effectively suppress growing of harmful algae, germ, improve water quality rapidly; (2) water plant such as some height itself is the plants waterborne with ornamental value, for rivers and lakes increase beautiful sceneries, beautifies the waters view.Comparing with traditional sewage water treatment method, have small investment, advantage of low energy consumption, is a kind of very potential " green " treatment technology.
Yet,, fast growth strong just because of water plant adaptability such as water hyacinth, water lettuce and duckweeds, make biomass form huge accumulation, occupy reservoir, lake, stop up river course, feed ditch, cause The loss of biodiversity, the ecosystem is done great damage, harm agricultural production, water transportation and human health.Particularly water hyacinth overflows in China south, has caused serious economy loss and social danger to some areas.In recent years, the threat that waters such as China Dian Chi, Taihu Lake continue to be subjected to water hyacinth causes significant impact to social economy, people's lives, and it is extremely urgent to administer water hyacinth.
How to give full play to the pollution treatment ability of high water plants such as water hyacinth, water lettuce and duckweed, stop its drawback, key is that it is carried out effective recycling treatment utilization.Method commonly used at present is to salvage the back as garbage loading embeading, but there is very big hidden danger in this processing scheme, because high water plants such as water hyacinth, water lettuce and duckweed contain a large amount of moisture and organic matter, not only can ferment behind the landfill produces great number of flammable gas, but also produces a large amount of percolates and become secondary pollution.
On the other hand, fast development along with China population growth and animal husbandry, the contradiction that people and animals strive grain becomes increasingly conspicuous, current and even long term from now on, China's Developing of Animal Industry will be subjected to the restriction of diet wretched insufficiency, active development utilizes the grain-saving feed resource, is to solve current diet anxiety, quickens the important directions of animal husbandry development.
High water plant nutritional labelings such as water hyacinth, water lettuce and duckweed are abundant, are vegetalitas high-protein feed resources.Reach 19.6%, 26.3%, 17.0% and 19.1% respectively as the contained protein of root, stem, leaf and the petiole of water hyacinth (dry weight), water hyacinth protein contained TEAA surpass paddy, oat, wheat, jowar and cotton seed meal, can match in excellence or beauty with soybean and corn, near the level of cow's milk and concentrated leaf protein; Fat content can reach 0.8%, 1.9%, 3.5% and 2.6% respectively; Contain vitamin B1, B2, B6 and B12 in per kilogram (dry weight) water hyacinth and reach 5.91mg, 30.7mg, 15.2mg and 0.012mg respectively.Therefore, development of resources has very high value to high water plants such as water hyacinth, water lettuce and duckweed as animal feed, not only can alleviate the present feed shortage of resources, also is pollution control of water, and changing harmful to treasure provides practical measures.
Technological difficulties such as there is the accumulating difficulty in the utilization of high water plants such as fresh water cucurbit, water lettuce and duckweed, be easy to rot, existing dry powder of water hyacinth technology of preparing exists to some extent also that the utilization of resources is insufficient, technology is loaded down with trivial details, disposal ability is low, economic benefit is not obvious, is difficult to realize problems such as heavy industrialization processing.Therefore, provide a kind of suitable heavy industrialization to handle the high-efficiency dehydration drying means of water plant resource, when reducing production costs, guarantee the nutritive value that the water plant resource is higher, become main purpose of the present invention.
Summary of the invention
The preparation method who the purpose of this invention is to provide a kind of dry water plant powder.
The preparation method of dry water plant powder comprises the steps:
1) the fresh water plant chopping that will gather is 0.001~5% at the antioxidant mass percent concentration, and temperature is that blanching completed 0.1~10 minute in 45~100 ℃ the aqueous solution;
2) mass percent concentration be add in 0.1~20% the inorganic or organic salt mass percent concentration that antioxidant and anticorrisive agent be configured to antioxidant be 0.001~5% and the mass percent concentration of anticorrisive agent be 0.001~3% high osmotic pressure solution, above-mentioned water plant after the scalding completes is put in the high osmotic pressure solution, cooling, permeating and dewatering 0.1~10 hour are made slurry with high pressure homogenizer or high-shear emulsion machine again;
3) with step 2) gained slurries filtration or centrifugation, filter cake drying, metering, pack dry water plant powder, filtrate is returned step 2) recycle.
Described water plant is water hyacinth, water lettuce, duckweed, green water cress or water caltrop.Inorganic salts are inorganic sodium, inorganic magnesium salt, inorganic calcium salt, inorganic mantoquita or do not have zinc salt.Organic salt is organic sodium salt, organic magnesium salts, organic calcium salt, organic copper salt or organic zinc salt.Antioxidant is ethoxyquin, di-tert-butyl hydroxy toluene, n-propyl gallate, TBHQ, vitamin C, sodium sulfite, sodium hydrogensulfite or sodium pyrosulfite.Anticorrisive agent is propionic acid, sorbic acid, sodium Diacetate, acetic acid, formic acid or citric acid, benzoic acid or Sodium Benzoate, fumaric acid or dimethyl fumarate.
Advantage of the present invention is that operating condition gentleness, energy consumption are little, compares with existing dry water plant powder technology of preparing, and the constant product quality that makes is easy to realize large-scale industrial production, has good economic and social benefit.
The specific embodiment
The drying of water plant is the combined process of thermal phenomenon, biological and chemical phenomenon, for guaranteeing the quality of product, must consider moisture state, hydro-thermal transport mechanism and influence factor of water plant and the problems such as quality variation in the water plant dry run.
The browning phenomenon of flavescence, browning or blackening can take place at dry run or product duration of storage in water plant, can be divided into two kinds of situations of enzymatic browning and non-enzymatic browning.The preparation method of dry water plant powder of the present invention, it is characterized in that under the protection of antioxidant, complete by blanching and to change the character of water plant cell membrane wall, shorten the time of oven dry, and destroy its oxidase active, reduce the particularly loss of vitamin of nutritional labeling, keep the original local flavor of water plant, color and luster, nutritional quality; Blanching also has the effect of cleaning and killing microorganisms and parasitic ovum concurrently.The preparation method of a kind of dry water plant powder of the present invention; it is characterized in that under the protection of antioxidant; the blanching living plant of treated water that completes is immersed the solution of hyperosmosis; utilize the semipermeability of cell membrane to make intracellular water transport in solution; help subsequent handling and shorten drying time, reduce baking temperature.The preparation method of a kind of dry water plant powder of the present invention, it is characterized in that the living plant of hypertonic solution treated water is pulverized slurrying with high pressure homogenizer or high-shear emulsion machine, increase its surface area on the one hand, can improve the oven dry speed of continuous operation, avoid the high energy consumption of dry material dry pulverization process on the other hand.Filter and the method for oven dry is well-known, filtration can be adopted common filter press, centrifuge or horizontal screw centrifuge, and oven dry can be with artificial drying or air dry.
The present invention is further described in conjunction with following example, but content of the present invention is not limited only to content related among the embodiment.
Embodiment 1:
1) with the fresh water cucurbit chopping of gathering, be 0.001% at the ethoxyquin mass percent concentration, temperature is that blanching completed 0.1 minute in 100 ℃ the aqueous solution;
2) in mass percent concentration is 0.1% sodium chloride solution, add ethoxyquin and propionic acid, the mass percent concentration that makes antioxidant is 0.001% and the mass percent concentration 3% of anticorrisive agent, water hyacinth input that will be after the scalding completes wherein, cooling, permeating and dewatering 10 hours; Use the slurrying in 10 minutes of high pressure homogenizer homogeneous again;
3) with step 2) the gained filter press filters, filter cake with band drier dry to water content less than 15%, through metering, pack dry water plant powder, filtrate is returned step 2) recycle.
Embodiment 2:
1) the fresh water caltrop chopping that will gather is 5% at the di-tert-butyl hydroxy toluene mass percent concentration, and temperature is that blanching completed 10 minutes in 45 ℃ the aqueous solution;
2) in mass percent concentration concentration is 20% SAS, add di-tert-butyl hydroxy toluene and sorbic acid, make the antioxidant mass percent concentration be 5% and the anticorrisive agent mass percent concentration be 0.001%, water hyacinth input that will be after the scalding completes wherein, cooling, permeating and dewatering 10 hours; Use the slurrying in 2 minutes of high-shear emulsion machine homogeneous again;
3) with step 2) the gained filter press filters, filter cake with canal drier dry to water content less than 10%, through metering, pack water caltrop dry powder, filtrate is returned step 2) recycle.
Embodiment 3:
1) with the water lettuce chopping of gathering, be 0.05% in n-propyl gallate concentration, temperature is that blanching completed 2 minutes in 60 ℃ the aqueous solution;
2) in mass percent concentration concentration is 5% calcium chloride water, add n-propyl gallate and benzoic acid, make the antioxidant mass percent concentration be 1% and the anticorrisive agent mass percent concentration be 2%, water lettuce after the scalding completes is dropped into wherein cooling, permeating and dewatering 3 hours; Use the slurrying in 2 minutes of high-shear emulsion machine homogeneous again;
3) with step 2) gained filters or centrifugation, filter cake drying, metering, pack water lettuce dry powder, filtrate is returned step 2) recycle.
Embodiment 4:
1) the fresh duckweed chopping that will gather is 0.5% in TBHQ concentration, and temperature is that blanching completed 8 minutes in 95 ℃ the aqueous solution;
2) in mass percent concentration concentration is 15% the calcium acetate aqueous solution, add TBHQ and Sodium Benzoate, make the antioxidant mass percent concentration be 0.5% and the anticorrisive agent mass percent concentration be 2.5%, duckweed after the scalding completes is dropped into wherein cooling, permeating and dewatering 5 hours; Use the slurrying in 1 minute of high pressure homogenizer homogeneous again;
3) with step 2) gained filters or centrifugation, filter cake is dried to water content less than 10% with roller drier, measure, pack duckweed dry powder, filtrate is returned step 2) recycle.
Embodiment 5:
1) the fresh green water cress chopping that will gather is 4% in vitamin C concentration, and temperature is that blanching completed 0.5 minute in 55 ℃ the aqueous solution;
2) in mass percent concentration concentration is 10% magnesium chloride brine, add vitamin C and fumaric acid, make the antioxidant mass percent concentration be 0.5% and the anticorrisive agent mass percent concentration be 1.5%, green water cress input that will be after the scalding completes wherein, cooling, permeating and dewatering 1 hour; Use the slurrying in 0.5 minute of high pressure homogenizer homogeneous again;
3) with step 2) gained filters or centrifugation, filter cake is dried to water content less than 10% with roller drier, measure, pack green water cress dry powder, filtrate is returned step 2) recycle.
Embodiment 6:
1) with the fresh water cucurbit chopping of gathering, be 3.5% at concentration of sodium sulfite, temperature is that blanching completed 0.8 minute in 75 ℃ the aqueous solution;
2) in mass percent concentration concentration is 10% magnesium sulfate solution, add sodium sulfite and dimethyl fumarate, make the antioxidant mass percent concentration be 0.5% and the anticorrisive agent mass percent concentration be 2.5%, water hyacinth input that will be after the scalding completes wherein, cooling, permeating and dewatering 5 hours; Use the slurrying in 1 minute of high pressure homogenizer homogeneous again;
3) with step 2) gained filters or centrifugation, filter cake is dried to water content less than 13% with pneumatic drier, measure, pack dry powder of water hyacinth, filtrate is returned step 2) recycle.
Embodiment 7:
1) the fresh duckweed chopping that will gather is 2% at concentration of sodium bisulphite, and temperature is that blanching completed 9 minutes in 55 ℃ the aqueous solution;
2) in mass percent concentration concentration is 10% copper chloride solution, add sodium hydrogensulfite and sodium Diacetate, make the antioxidant mass percent concentration be 0.4% and the anticorrisive agent mass percent concentration be 1.5%, water lettuce after the scalding completes is dropped into wherein cooling, permeating and dewatering 5 hours; Use the slurrying in 1 minute of high pressure homogenizer homogeneous again;
3) with step 2) gained filters or centrifugation, filter cake is dried to water content less than 10% with roller drier, measure, pack duckweed dry powder, filtrate is returned step 2) recycle.
Embodiment 8:
1) the fresh duckweed chopping that will gather is 0.009% at the pyrosulfurous acid na concn, and temperature is that blanching completed 0.4 minute in 90 ℃ the aqueous solution;
2) in mass percent concentration concentration is 10% copper sulfate solution, add sodium pyrosulfite and acetic acid, make the antioxidant mass percent concentration be 4.5% and the anticorrisive agent mass percent concentration be 1.5%, water lettuce after the scalding completes is dropped into wherein cooling, permeating and dewatering 6 hours; Use the slurrying in 1 minute of high pressure homogenizer homogeneous again;
3) with step 2) gained filters or centrifugation, filter cake is dried to water content less than 10% with roller drier, measure, pack duckweed dry powder, filtrate is returned step 2) recycle.
Embodiment 9:
1) the fresh water lettuce chopping that will gather is 0.01% at concentration of sodium bisulphite, and temperature is that blanching completed 3 minutes in 80 ℃ the aqueous solution;
2) in mass percent concentration concentration is 10% solder(ing)acid, add sodium hydrogensulfite and formic acid, make the antioxidant mass percent concentration be 0.05% and the anticorrisive agent mass percent concentration be 0.5%, water lettuce after the scalding completes is dropped into wherein cooling, permeating and dewatering 8 hours; Use the slurrying in 0.5 minute of high pressure homogenizer homogeneous again;
3) with step 2) gained filters or centrifugation, filter cake is dried to water content less than 10% with roller drier, measure, pack water lettuce dry powder, filtrate is returned step 2) recycle.
Embodiment 10:
1) with the fresh water cucurbit chopping of gathering, be 0.004% in TBHQ concentration, temperature is that blanching completed 6 minutes in 60 ℃ the aqueous solution;
2) in mass percent concentration concentration is 10% zinc acetate aqueous solution, add TBHQ and citric acid, make the antioxidant mass percent concentration be 0.05% and the anticorrisive agent mass percent concentration be 2%, water hyacinth input that will be after the scalding completes wherein, cooling, permeating and dewatering 2 hours; Use the slurrying in 2 minutes of high pressure homogenizer homogeneous again;
3) with step 2) gained filters or centrifugation, the filter cake air dry to water content less than 15%, measure, pack dry powder of water hyacinth, filtrate is returned step 2) recycle.
Claims (8)
1. the preparation method of a dry water plant powder is characterized in that comprising the steps:
1) the fresh water plant chopping that will gather is 0.001~5% at the antioxidant mass percent concentration, and temperature is that blanching completed 0.1~10 minute in 45~100 ℃ the aqueous solution;
2) in mass percent concentration is 0.1~20% inorganic or organic slat solution, add antioxidant and anticorrisive agent, the mass percent concentration that is configured to antioxidant be 0.001~5% and the mass percent concentration of anticorrisive agent be 0.001~3% high osmotic pressure solution, above-mentioned water plant after the scalding completes is put in the high osmotic pressure solution, cooling, permeating and dewatering 0.1~10 hour are made slurry with high pressure homogenizer or high-shear emulsion machine again;
3) with step 2) gained slurries filtration or centrifugation, filter cake drying, metering, pack dry water plant powder, filtrate is returned step 2) recycle.
2. the preparation method of a kind of dry water plant powder according to claim 1 is characterized in that described water plant is water hyacinth, water lettuce, duckweed, green water cress or water caltrop.
3. the preparation method of a kind of dry water plant powder according to claim 1 is characterized in that described inorganic salts are inorganic sodium, inorganic magnesium salt, inorganic calcium salt, inorganic mantoquita or do not have zinc salt.
4. the preparation method of a kind of dry water plant powder according to claim 1 is characterized in that described organic salt is organic sodium salt, organic magnesium salts, organic calcium salt, organic copper salt or organic zinc salt.
5. the preparation method of a kind of dry water plant powder according to claim 1 is characterized in that described antioxidant is ethoxyquin, di-tert-butyl hydroxy toluene, n-propyl gallate, TBHQ, vitamin C, sodium sulfite, sodium hydrogensulfite or sodium pyrosulfite.
6. the preparation method of a kind of dry water plant powder according to claim 1 is characterized in that described anticorrisive agent is propionic acid, sorbic acid, sodium Diacetate, acetic acid, formic acid or citric acid.
7. the preparation method of a kind of dry water plant powder according to claim 1 is characterized in that described anticorrisive agent is benzoic acid or Sodium Benzoate.
8. the preparation method of a kind of dry water plant powder according to claim 1 is characterized in that described anticorrisive agent is fumaric acid or dimethyl fumarate.
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US10405506B2 (en) | 2009-04-20 | 2019-09-10 | Parabel Ltd. | Apparatus for fluid conveyance in a continuous loop |
CN103416691A (en) * | 2013-07-24 | 2013-12-04 | 浙江大学 | Preparing method for preparing mulberry leaf dry powder |
CN103539479B (en) * | 2013-09-30 | 2014-12-03 | 梁洪奎 | Preparation method of pre-swelling plant particle pore-forming agent |
CN103815123A (en) * | 2013-11-26 | 2014-05-28 | 费洪标 | Water hyacinth feed for animals |
CN105211618A (en) * | 2014-05-28 | 2016-01-06 | 吴光平 | A kind of preparation method of dry water plant powder |
WO2016201381A1 (en) | 2015-06-10 | 2016-12-15 | Parabel Ltd. | Methods and systems for forming moisture absorbing products from a microcrop |
AU2016275066B2 (en) | 2015-06-10 | 2020-09-10 | Parabel Nutrition, Inc. | Apparatuses, methods, and systems for cultivating a microcrop involving a floating coupling device |
AU2016276972B8 (en) | 2015-06-10 | 2022-09-22 | Lemnature Aquafarms Corporation | Methods and systems for extracting protein and carbohydrate rich products from a microcrop and compositions thereof |
WO2017007830A1 (en) | 2015-07-06 | 2017-01-12 | Parabel Ltd. | Methods and systems for extracting a polysaccharide product from a microcrop and compositions thereof |
WO2017027634A1 (en) | 2015-08-10 | 2017-02-16 | Parabel Ltd. | Methods and systems for extracting reduced oxalic acid protein from aquatic species and compositions thereof |
CN108347991B (en) * | 2015-09-10 | 2022-01-25 | 帕拉贝尔营养股份有限公司 | Apparatus and method for producing high concentration protein product from blanched biomass |
CN105124312A (en) * | 2015-09-27 | 2015-12-09 | 常州市奥普泰科光电有限公司 | Preparation method of weaned suckling pig feed |
CN105360696A (en) * | 2015-12-15 | 2016-03-02 | 苏州市阳澄农业科技有限公司 | Poultry feed using aquatic plants as raw materials and preparation method |
CN108522785A (en) * | 2017-12-08 | 2018-09-14 | 重庆昇顺科技有限公司 | A kind of fowl water plant fermentation protein feedstuff |
CN110813238A (en) * | 2019-12-02 | 2020-02-21 | 深圳市碧园环保技术有限公司 | Wetland plant resource utilization method |
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