CN100557048C - Continuous magnesium smelting device of a kind of induction heating and continuous process for smelting magnesium thereof - Google Patents
Continuous magnesium smelting device of a kind of induction heating and continuous process for smelting magnesium thereof Download PDFInfo
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- CN100557048C CN100557048C CNB2007100359298A CN200710035929A CN100557048C CN 100557048 C CN100557048 C CN 100557048C CN B2007100359298 A CNB2007100359298 A CN B2007100359298A CN 200710035929 A CN200710035929 A CN 200710035929A CN 100557048 C CN100557048 C CN 100557048C
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Abstract
The invention discloses a cover continuous magnesium smelting device of induction heating and a continuous process for smelting magnesium.Described device comprises continuous-feeding device, induction heating reaction chamber, magnesium vapour condensation device and continuous discharging slag device; Wherein, feeding device is made up of feed bin and screw feeder mechanism, reaction chamber is made up of load coil, heat generating member, dividing plate and slag refrigerating unit with holes, condensing works is made up of the baffle plate with eyed structure, dust setting chamber, magnesium vapor condensation chamber, and the continuous discharging slag device comprises spiral clinker pusher structure and slag storehouse.Continuously process for smelting magnesium comprises the reaction furnace charge to operations such as coming out of the stove of the continuous condensation of the pushing continuously of reaction chamber, magnesium steam and liquid magnesium, comprises that simultaneously the reaction slag enters the slag storehouse continuously and step such as slag tap.Heat energy utilization rate height of the present invention, and can the low-cost continuous production of realizing MAGNESIUM METAL.
Description
Technical field
The present invention relates to a kind of induction heating and reduce refining magnesium system continuously, the invention still further relates to and use this induction heating and reduce the technology that refining magnesium system refines magnesium continuously continuously.
Background technology
The production method of magnesium mainly contains hot reducing method and electrolytic process two classes, and at present, 70% of world's magnesium output is produced by " Pidgeon process " in the hot reducing method.Yet, there are many defectives in existing " Pidgeon process " process for smelting magnesium, be mainly reflected in: 1. adopt the fossil energy of non-renewable coal or coal gas class, the reduction jar of filling pelletizing is directly carried out in air outside the heating type of heating, not only make the effective rate of utilization of heat energy low, reduction jar life-span is short, and heat is difficult to pass to fast a reduction jar center and makes the recovery time long, in addition, the employing of fossil energy causes reduction process to produce a large amount of flue gases inevitably; 2. the accumbency arrangement mode and the gap mode of production of reduction jar make that not only labor strength is excessive, production efficiency is low, and the production capacity of single devices are little.
The defective that existing in order to overcome " Pidgeon process " process for smelting magnesium exists, patent such as " Inner Heating Magnesium Refining Production Technology And Apparatus (CN1163622C) " and " pipe type thermal method magnesium-smelting production technology and equipment thereof (CN1042841C) " has proposed the equipment or the technology of continuous refining magnesium, but the direct energy source that they all adopt is coal or coal gas, and this can make inevitably and produce a large amount of flue gases in the magnesium reduction process.Patent " induction heating reduction magnesium smelting device (CN2265379) " has proposed a kind of with the induction heating magnesium smelting reducing device of electricity as direct energy source, but this patent difficulty avoids the defective of external heating mode (short as the reduction jar life-span, recovery time is long etc.), and can not implement the serialization operation.Patent " multiple heat resources-electric warming magnesium smelting apparatus and technology (CN1928134A) " also proposed with exchange or direct current as the energy, refine the technology and the equipment of magnesium continuously as the radiant heat of electrode generation with Si/C, C or metallic substance, but there are some defectives equally in this patent, mainly show: the heating element that 1. is arranged in the stove is easy to make furnace charge " bridge formation " phenomenon to occur, and " bridge formation " phenomenon also might appear in the slag in warm sludge storehouse; When 2. adopting powder, unavoidably have a large amount of dust in the crystallization magnesium, the burden that this not only strengthens the magnesium refining procedure causes the quadratic loss of magnesium to strengthen, but also the possibility contaminated vacuum system; 3. resulting crystallization magnesium also needs to carry out refining, and this not only causes the quadratic loss of magnesium, and, also with consumes energy.
Summary of the invention
Technical problem to be solved by this invention provides a kind of low cost, high heat energy utilization rate, is convenient to the device and the technology of the continuous reduction refining magnesium of automated operation.
In order to solve the problems of the technologies described above, induction heating provided by the invention refines the magnesium system continuously, an induction heating reaction chamber is connected with the continuous feeding device of at least one cover, is connected with at least two cover magnesium vapor condensations and becomes the condensing works of liquid magnesium and the continuous discharging slag device of at least one cover.
Stove outer covering is welded by steel plate, and the material of steel plate is A3 steel or No. 45 steel, and the thickness of outer steel shell is 10～30mm; Be lined with the thermal insulation fire-resistant layer in the described stove outer covering; Body of heater is provided with first vision slit more than two.
Described continuous-feeding device comprises feed bin and screw feeder mechanism, and feed bin is a up-down structure, is made of feeding warehouse and storage bin, and described feeding warehouse and described storage bin are equipped with first slide valve between constituting; Be connected with first vacuum valve that externally vacuumizes, the charging opening of band gasket on the described feeding warehouse; Be connected with second vacuum valve that externally vacuumizes and second slide valve that is connected with screw feeder mechanism on the described storage bin, heating wire also is housed on the shell of described storage bin; The tubular shaft that described screw feeder mechanism includes steel casing and is welded with the feed flight; Described steel casing and described stove outer covering is seamless welds together, a cover plate that seals is arranged at the top of described tubular shaft, the bearing shell that described tubular shaft is assemblied in the band watercooling jacket with in, at least four holes are arranged in its intermediate bushing, pass through for furnace charge; The top of described tubular shaft is equipped with a gear that can link to each other with driving motor.
Described induction heating chamber comprises ruhmkorff coil, induction heating spare, dividing plate with holes, and at least one blind roaster slag cooler; Wherein said ruhmkorff coil is copper pipe or stainless steel tube, logical water coolant in copper pipe or the stainless steel tube; When described slag refrigerating unit more than when cover, all slag refrigerating units are installed on the horizontal plane, and cover with overlap between be separated by at least that to be at least furnace charge maximum sized more than 5 times for spacing; The transverse section of described induction heating spare is square or circular, material be graphite, C/Si or can anti-metal more than 1500 ℃ in one or more; Described dividing plate is formed by the high-temperature refractory ramming, and is supported on the steel plate by the refractory materials pillar stiffener; Hole is all arranged on described dividing plate and the steel plate, and the size of described hole is more than 5 times of maximum particle size in the furnace charge; Described induction heating spare vertical setting of types is indoor at described induction heating, and the interval between the adjacent heating member is greater than 10 times of maximum particle size in the furnace charge; Design has water-cooled tube in the described slag refrigerating unit; Also design in the described slag refrigerating unit ventpipe is arranged.
Described magnesium vapor condensation becomes the condensing works of liquid magnesium to comprise perforated baffle, dust setting chamber, the 3rd vacuum valve, condensing chamber, potassium sodium dust trapping chamber, and the 4th vacuum valve; Described perforated baffle be have the cancellated porous ceramics of three-dimensional through hole or can anti-porous metal more than 1350 ℃ in a kind of; One discharge gate is arranged at the bottom of described dust setting chamber, and this discharge gate bottom is equipped with first seal base of band water coolant, and dust is regularly discharged from discharge gate; Described magnesium condensing chamber includes water-cooled condenser, thermopair, and the resistance heating wire, the liquid magnesium thrust-augmenting nozzle, liquid magnesium accumulator, and second seal base of band water coolant, but the lifting device of an oscilaltion is housed under described second seal base; On liquid magnesium accumulator top second porthole is housed; Described potassium sodium dust trapping chamber bottom is equipped with band refrigerative the 3rd seal base.
Described continuous discharging slag device includes and can make continuous propulsive spiral pusher mechanism of slag and slag charge storehouse, be equipped with the 3rd slide valve between described spiral pusher mechanism and the described slag charge storehouse, one slag notch is arranged at bottom, described slag charge storehouse, and the 4th slide valve is housed on the described slag notch; The 5th vacuum valve is equipped with on top, described slag charge storehouse; One the 3rd vision slit also is equipped with on top, described slag charge storehouse.
Use induction heating and refine the technology that the magnesium system refines magnesium continuously continuously, the operation that this technology comprises has continuous-feeding, successive reaction, continuous discharging slag, and gaseous magnesium is condensed into liquid magnesium continuously, may further comprise the steps: the first step---close second slide valve, the 3rd slide valve and the 4th slide valve, open the 3rd vacuum valve, and vacuumize since the 4th vacuum valve and the 5th vacuum valve place, open all water coolants simultaneously; After vacuum tightness reaches 1～10Pa in the stove, begin first resistance heating wire to storage bin, second resistance heating wire of magnesium condensing chamber and the ruhmkorff coil of induction heating chamber and send electricity, make the storage bin temperature reach 300～500 ℃, the homo(io)thermism of magnesium condensing chamber in the homo(io)thermism of 660～700 ℃ and induction heating chamber at 1150～1300 ℃; Second step, open the charging opening and first slide valve on the feeding warehouse, being that the pelletizing made of raw material or the powder that mixes add from charging opening by calcined dolomite, ferrosilicon and fluorite, after furnace charge is filled in feeding warehouse and the storage bin, shut first slide valve and charging opening, vacuumize since first vacuum valve and the second vacuum valve place; After vacuum tightness reaches 1～10Pa in the storage bin, and after charge-temperature reaches 300～500 ℃ in the storage bin, open second slide valve, and open screw feeder mechanism simultaneously and make furnace charge enter heating chamber continuously; The 3rd step, when furnace charge behind the indoor stop 1.5～5h of induction heating, open the 3rd slide valve, and open the continuous discharging slag device, make slag slowly enter the slag charge storehouse; Magnesium steam is condensed into the liquid magnesium operation continuously and may further comprise the steps: the first step---when the liquid level of liquid magnesium in the magnesium accumulator reaches 2/3～4/5 left and right sides of accumulator height, close the 3rd vacuum valve and the 4th vacuum valve, and from the 4th vacuum valve feeding argon gas, after gaseous tension reaches 0.01～0.1Mpa in the magnesium condensing chamber, open second seal base, open lifting device and make liquid magnesium shift out the magnesium condensing chamber, carry out follow-up casting or preparation alloy; Second step---the new magnesium accumulator of in the magnesium condensing chamber, packing into, and install second seal base, vacuumize since the 4th vacuum valve place, after vacuum tightness reaches 1～10Pa in the magnesium condensing chamber, open the 3rd vacuum valve.
The continuous-feeding operation may further comprise the steps: after furnace charge in the storage bin all changes induction heating chamber over to, close second slide valve earlier, open first slide valve, make in the feeding warehouse furnace charge enter storage bin and carry out preheating; Then, close first slide valve, open the opening for feed of feeding warehouse, furnace charge is added in the feeding warehouse, behind the sealing opening for feed, open first vacuum valve and make feeding warehouse vacuum tightness reach 1～10Pa; Thereby realized the without interruption of furnace charge in the induction heating chamber.
The continuous discharging slag operation may further comprise the steps: the first step---and when the quantity of slag in the slag charge storehouse reaches 4/5 left and right sides of slag charge storehouse height, stop spiral pusher mechanism), close the 3rd slide valve, open the 4th slide valve and begin deslagging; After slag has been arranged, close the 3rd slide valve and the 4th slide valve, open the 5th vacuum valve and begin to vacuumize; After slag charge storehouse vacuum tightness reaches 1～10Pa, open the 3rd slide valve, close the 5th vacuum valve, and open spiral pusher mechanism.
Compare with known method for smelting magnesium by hot equipment and method for smelting magnesium by hot technology, the present invention has following advantage:
(1) clear energy sources---electric energy is the process for smelting magnesium heat supply in employing, produces the defective of volume of smoke and waste gas when having overcome use fossil energy (coal, coal gas and Sweet natural gas etc.) heating;
(2) adopt induction heating, utilization efficiency of heat energy is improved greatly;
(3) adopt continuous feeding and continuous discharging slag device, greatly reduce labor strength, improved labour productivity;
(4) do not need to have saved production cost greatly with the reduction jar that costs an arm and a leg, contains elements such as Ni and Cr;
(4) can improve the temperature of reaction of reaction mass by increasing coil turn and heat generating member quantity, thereby can shorten the reduction reaction time effectively, improve the output of FU time;
(5) can become liquid condensing works tricks to reach the continuous refining magnesium purpose of extensiveization by capacity, the increase magnesium vapor condensation that enlarges reaction chamber;
(6) product that obtains of the present invention is a liquid magnesium; In addition, because the magnesium steam that reaction chamber produced has passed through the filtration of porous material, and has passed through settling pocket, thereby can guarantee that the foreign matter content in the liquid magnesium is lower;
(7) the designed slag refrigerating unit in reaction chamber bottom of the present invention can make slag from α type 2CaOSiO
2Be transformed into β type 2CaOSiO
2Thereby, can guarantee the efflorescence of slag, guarantee the normal operation of continuous discharging slag device;
(8) the present invention has designed the treatment measures of furnace charge or slag appearance " bridge formation " phenomenon, promptly dispels so-called " bridge " toward interior argon gas or the hydrogen that feeds the band certain pressure of stove, thereby the production process continuation is carried out smoothly.
Description of drawings
Accompanying drawing is that induction heating refines magnesium system architecture synoptic diagram continuously.
Embodiment
Below in conjunction with the drawings and specific embodiments the present invention is elaborated, but be used for anything but limiting the scope of the invention.
A. the designed induction heating of this patent refines the magnesium system as shown in drawings continuously, comprises that the continuous feeding device of a cover, induction heating reaction chamber, two cover magnesium vapor condensations become the condensing works and the continuous slag discharging device of a cover of liquid magnesium.
B. the stove outer covering 100 that described induction heating refines the magnesium system continuously is welded by steel plate, and the material of steel plate is A3 steel or No. 45 steel, and the thickness of outer steel shell is 10～30mm; Be lined with thermal insulation fire-resistant layer 200 in the stove outer covering; Body of heater is provided with first vision slit 201 more than two, so that observe the interior charge level situation of stove and observe temperature in the stove with infrared thermometer.
C. the continuous-feeding device that described induction heating refines in the magnesium system continuously comprises feed bin and screw feeder mechanism 400, and feed bin is up-down structure, is made of feeding warehouse 300 and storage bin 310, is equipped with first slide valve 320 between feeding warehouse 300 and the storage bin 310.Be connected with first vacuum valve 301 that externally vacuumizes, the charging opening 302 of band gasket on the feeding warehouse 300; Be connected with second vacuum valve 311 that externally vacuumizes and second slide valve 313 that is connected with screw feeder mechanism 400 on the storage bin 310, in addition, first resistive heater 312 be housed also on the shell of storage bin 310.The tubular shaft 402 that screw feeder mechanism 400 includes steel casing 401 and is welded with the feed flight; Steel casing 401 and stove outer covering 100 are seamless to weld together, a cover plate that seals 405 is arranged at the top of tubular shaft 402, tubular shaft 402 is assemblied in the bearing shell 403 and bearing shell 406 of band watercooling jacket, in its intermediate bushing 406 at least four holes is arranged, and passes through for furnace charge; The top of tubular shaft 402 is equipped with a gear 404 that can link to each other with driving motor; Why tubular shaft 402 is hollow pipe, be for gas can be fed in the stove easily, particularly when reaction in furnace furnace charge or slag appearance " bridge formation " phenomenon, can in stove, feed " bridge " that the gas of being with certain pressure is broken up institute's frame by this tubular shaft, make production process can continue to carry out smoothly, also can feed gas to cleaning in the stove by this hollow pipe.402 li bodies of ventilating of tubular shaft are a kind of in argon gas or the hydrogen.
D. the induction heating chamber 500 that described induction heating refines in the magnesium system continuously comprises ruhmkorff coil 501, induction heating spare 502, dividing plate 503 with holes, and at least one blind roaster slag cooler 504.Wherein ruhmkorff coil 501 is copper pipe or stainless steel tube, logical water coolant in copper pipe or the stainless steel tube; When the slag refrigerating unit more than when cover, all slag refrigerating units are installed on the horizontal plane, and cover with overlap between be separated by at least that to be at least furnace charge maximum sized more than 5 times for spacing.The transverse section of induction heating spare 502 is square or circular, material be graphite, C/Si or can anti-metal more than 1500 ℃ in one or more; Dividing plate 503 is formed by the high-temperature refractory ramming, and is supported on the steel plate 508 by refractory materials pillar stiffener 507; On dividing plate 503 and the steel plate 508 hole is arranged all, so that the whereabouts of reaction slag, the size of described hole is more than 5 times of maximum particle size in the furnace charge; Induction heating spare 502 vertical setting of types are in induction heating chamber 500, and the interval between the adjacent heating member is greater than 10 times of maximum particle size in the furnace charge; The number of turn of ruhmkorff coil be arranged in heating member quantity in the stove by the bulk decision of induction heating chamber, to consider also simultaneously to make that furnace charges are heated to more than 1350 ℃ in the induction heating chamber 500; 504 li designs of slag refrigerating unit have water-cooled tube 505, so that logical water coolant comes cooled slag, make slag from α type 2CaOSiO
2Be transformed into β type 2CaOSiO
2, reach slag expansion, atomizing purpose, thereby make the powdery slag can enter the continuous discharging slag device smoothly; The slag refrigerating unit also designs for 504 li ventpipe 506, when " bridge formation " phenomenon appears in slag, can ventilate in stove by ventpipe, blow and step on slag institute frame " bridge ", and make slag enter slag discharging device smoothly; Ventpipe 506 body of ventilating is a kind of in argon gas or the hydrogen.
E. described induction heating refine continuously magnesium vapor condensation in the magnesium system become liquid magnesium condensing works comprise perforated baffle 601, dust setting chamber's 602, the three vacuum valves 603, condensing chamber 607, potassium sodium dust trapping chamber 611, and the 4th vacuum valve 610.Perforated baffle 601 for have the cancellated porous ceramics of three-dimensional through hole or can anti-porous metal more than 1350 ℃ in a kind of, its effect is to stop that the radiant heat of reaction chamber 500 and filtering reaction generate the dust in the magnesium steam; The effect of dust setting chamber 602 is that the dust settling that is not blocked by perforated baffle 601 is got off, and a discharge 615 is arranged at the bottom of dust setting chamber 602, and this discharge gate bottom is equipped with first seal base 616 of band water coolant, and dust is regularly discharged from discharge 615; Magnesium condensing chamber 607 includes water-cooled condenser 604, thermopair 605, the second resistance heating wires 606, liquid magnesium thrust-augmenting nozzle 608, liquid magnesium accumulator 609, and second seal base 614 of band water coolant, but second seal base is equipped with the lifting device 617 of an oscilaltion for 614 times; On liquid magnesium accumulator 609 tops second porthole 613 is housed, is used for observing the liquid level of liquid magnesium in the accumulator 609; Potassium sodium dust trapping chamber 611 bottoms are equipped with band refrigerative the 3rd seal base 612, so that regularly the potassium sodium that is captured is taken out from dust trapping chamber 611.
F. described induction heating refines continuous discharging slag device in the magnesium system continuously and includes and can make the continuous propulsive spiral pusher of slag mechanism 701 and slag charge storehouse 705, be equipped with the 3rd slide valve 702 between spiral pusher mechanism 701 and the slag charge storehouse 705,705 bottoms, slag charge storehouse have slags tap 706, slags tap the 4th slide valve 707 to be housed on 706; The 5th vacuum valve 703 is equipped with on 705 tops, slag charge storehouse; The 3rd vision slit 704 also is equipped with on 705 tops, slag charge storehouse, and slag in the slag charge storehouse 705 what are convenient to observe.
The continuous process for smelting magnesium of pelletizing furnace charge
The furnace charge that present embodiment is used is a walnut shape pelletizing, and the pelletizing apparent size is the about 26mm of major axis, the about 20mm of minor axis, the about 20mm of thickness, and the continuous process for smelting magnesium of induction heating comprises the preparation of raw material pelletizing, continuous-feeding, successive reaction, continuous discharging slag, and gaseous magnesium is condensed into steps such as liquid state continuously.Step by step present embodiment is described below:
The first step: with calcined dolomite (15～35mm), the ferrosilicon of silicon content 75% (weight) (3～5mm) and fluorite powder (200 order) prepared burden by weight 80: 17: 3, the material for preparing is added to ball mill carries out mixer mill, the granularity of powder answers 100% less than 100 orders behind the mixer mill; Then, will grind good powder pressure ball with LYQ high pressure roller ball press, the balling-up pressure-controlling is at 60～120kg/cm
2The ball that the presses exsiccant pellet feed storehouse of packing into.
Second step---close second slide valve 313, the 3rd slide valve 702 and the 4th slide valve 707, open the 3rd vacuum valve 603, and vacuumize, open all water coolants simultaneously since the 4th vacuum valve 610 and the 5th vacuum valve 703 places; After vacuum tightness reaches 1～10Pa in the stove, begin first resistance heating wire 312 to storage bin 310, second resistance heating wire 606 of magnesium condensing chamber 607 and the ruhmkorff coil 501 of induction heating chamber 500 and send electricity, make storage bin 310 temperature reach 300～500 ℃, the homo(io)thermism of magnesium condensing chamber 607 in the homo(io)thermism of 660～700 ℃ and induction heating chamber 500 at 1150～1300 ℃.
The 3rd step, open the charging opening 302 and first slide valve 320 on the feeding warehouse 300, the pelletizing furnace charge is added from charging opening 302, after furnace charge is filled in feeding warehouse 300 and the storage bin 310, shut first slide valve 320 and charging opening 302, vacuumize since first vacuum valve 301 and second vacuum valve, 311 places; After vacuum tightness reaches 1～10Pa in the storage bin 310, and after charge-temperatures reach 300～500 ℃ in the storage bin 310, open second slide valve 313, and open screw feeder mechanism 400 simultaneously and make furnace charge enter heating chamber 500 continuously;
The 4th step, when furnace charge stops 5h in induction heating chamber 500 after, open the 3rd slide valve 702, and open continuous discharging slag device 701, make slag slowly enter slag charge storehouse 705.
Continuous-feeding operation in the present embodiment may further comprise the steps: after furnace charge all changes induction heating chamber 500 in the storage bin 310, close second slide valve 313 earlier, open first slide valve 320, make in the feeding warehouse 300 furnace charge enter storage bin 310 and carry out preheating; Then, close first slide valve 320, open the opening for feed 302 of feeding warehouse 300, furnace charge is added in the feeding warehouse 300, behind sealing opening for feed 302, open first vacuum valve 301 and make feeding warehouse 300 vacuum tightnesss reach 1～10Pa; Thereby realized the without interruption of furnace charge in the induction heating chamber 500.
The operation that magnesium steam in the present embodiment is condensed into liquid magnesium continuously may further comprise the steps: the first step---when the liquid level of liquid magnesium in the magnesium accumulator 609 reaches 2/3～4/5 left and right sides of accumulator height, close the 3rd vacuum valve 603 and the 4th vacuum valve 610, and from the 4th vacuum valve 610 feeding argon gas, after gaseous tension reaches 0.01～0.1Mpa in magnesium condensing chamber 607, open second seal base 614, open lifting device 617 and make liquid magnesium shift out magnesium condensing chamber 607, carry out follow-up casting or preparation alloy; Second step---the new magnesium accumulator of in magnesium condensing chamber 607, packing into, and install second seal base 614,610 places vacuumize since the 4th vacuum valve, after vacuum tightness reaches 1～10Pa in the magnesium condensing chamber, open the 3rd vacuum valve 603.
Continuous discharging slag operation in the present embodiment may further comprise the steps: the first step---and when the quantity of slag in the slag charge storehouse 705 reaches 4/5 left and right sides of slag charge storehouse height, stop spiral pusher mechanism 701, close the 3rd slide valve 702, open the 4th slide valve 707 beginning deslagginves; After slag has been arranged, close the 3rd slide valve 702 and the 4th slide valve 707, open the 5th vacuum valve 703 and begin to vacuumize; After slag charge storehouse 705 vacuum tightnesss reach 1～10Pa, open the 3rd slide valve 702, close the 5th vacuum valve 703, and open spiral pusher mechanism 701.
In the present embodiment implementation process, if " bridge formation " phenomenon appears in furnace charge or slag, can dispel so-called " bridge " toward the argon gas or the hydrogen of feeding band certain pressure in the stove, make production process can continue to carry out smoothly.The concrete operations step is: close the 3rd vacuum valve 603 earlier, then toward 506 li argon gas or hydrogen that feed the band certain pressure of tubular shaft 402 and ventpipe, and open the 3rd slide valve 702 and the 4th slide valve 707 simultaneously.
Claims (7)
1, the continuous magnesium smelting device of a kind of induction heating, it is characterized in that: an induction heating reaction chamber is connected with the continuous feeding device of at least one cover, be connected with at least two cover magnesium vapor condensations and become the condensing works of liquid magnesium and the continuous discharging slag device of at least one cover, stove outer covering (100) is welded by steel plate, the material of steel plate is A3 steel or No. 45 steel, and the thickness of outer steel shell is 10～30mm; Be lined with thermal insulation fire-resistant layer (200) in the described stove outer covering (100); Body of heater is provided with first vision slit (201) more than two, described continuous-feeding device comprises feed bin and screw feeder mechanism (400), feed bin is a up-down structure, be made of feeding warehouse (300) and storage bin (310), described feeding warehouse (300) and described storage bin (310) are equipped with first slide valve (320) between constituting; Be connected with first vacuum valve (301) that externally vacuumizes, the charging opening (302) of band gasket on the described feeding warehouse (300); Be connected with second vacuum valve (311) that externally vacuumizes and second slide valve (313) that is connected with screw feeder mechanism (400) on the described storage bin (310), first resistive heater (312) also is housed on the shell of described storage bin (310); The tubular shaft (402) that described screw feeder mechanism (400) includes steel casing (401) and is welded with the feed flight; Described steel casing (401) welds together with stove outer covering (100) is seamless, a cover plate that seals (405) is arranged at the top of described tubular shaft (402), described tubular shaft (402) is assemblied in the bearing shell (403,406) of band watercooling jacket, its intermediate bushing has at least four holes in (406), passes through for furnace charge; The top of described tubular shaft (402) is equipped with a gear that links to each other with driving motor (404).
2, the continuous magnesium smelting device of induction heating according to claim 1, it is characterized in that: induction heating reaction chamber (500) comprises ruhmkorff coil (501), induction heating spare (502), dividing plate with holes (503), and at least one blind roaster slag cooler (504); Wherein said ruhmkorff coil (501) is copper pipe or stainless steel tube, logical water coolant in copper pipe or the stainless steel tube; When described slag refrigerating unit (504) more than when cover, all slag refrigerating units (504) are installed on the horizontal plane, and cover with overlap between be separated by that to be at least furnace charge maximum sized more than 5 times for spacing; The transverse section of described induction heating spare (502) is square or circular, material be graphite, C/Si or can anti-metal more than 1500 ℃ in one or more; Described dividing plate (503) is formed by the high-temperature refractory ramming, and is supported on the steel plate (508) by refractory materials pillar stiffener (507); On described dividing plate (503) and the steel plate (508) hole is arranged all, the size of described hole is more than 5 times of maximum particle size in the furnace charge; Described induction heating spare (502) vertical setting of types is in described induction heating reaction chamber (500), and the interval between the adjacent heating member is greater than 10 times of maximum particle size in the furnace charge; The design of described slag refrigerating unit (504) lining has water-cooled tube (505); Ventpipe (506) is also designed in described slag refrigerating unit (504) lining.
3, the continuous magnesium smelting device of induction heating according to claim 1, it is characterized in that: described magnesium vapor condensation becomes the condensing works of liquid magnesium to comprise perforated baffle (601), dust setting chamber (602), the 3rd vacuum valve (603), condensing chamber (607), potassium sodium dust trapping chamber (611), and the 4th vacuum valve (610); Described perforated baffle (601) for have the cancellated porous ceramics of three-dimensional through hole or can anti-porous metal more than 1350 ℃ in a kind of; One discharge gate (615) is arranged at the bottom of described dust setting chamber (602), and this discharge gate bottom is equipped with first seal base (616) of band water coolant, and dust is regularly discharged from discharge gate (615); Magnesium condensing chamber (607) includes water-cooled condenser (604), thermopair (605), second resistance heating wire (606), liquid magnesium thrust-augmenting nozzle (608), liquid magnesium accumulator (609), and second seal base (614) of band water coolant, described second seal base (614) but under the lifting device (617) of an oscilaltion is housed; On liquid magnesium accumulator (609) top second porthole (613) is housed; Described potassium sodium dust trapping chamber (611) bottom is equipped with band refrigerative the 3rd seal base (612).
4, the continuous magnesium smelting device of induction heating according to claim 1, it is characterized in that: described continuous discharging slag device includes and can make continuous propulsive spiral pusher mechanism of slag (701) and slag charge storehouse (705), be equipped with the 3rd slide valve (702) between described spiral pusher mechanism (701) and the described slag charge storehouse (705), one slag notch (706) is arranged at bottom, described slag charge storehouse (705), and the 4th slide valve (707) is housed on the described slag notch (706); The 5th vacuum valve (703) is equipped with on top, described slag charge storehouse (705); The 3rd vision slit (704) also is equipped with on top, described slag charge storehouse (705).
5, application rights requires the technology that the continuous magnesium smelting device of 1 described induction heating refines magnesium continuously, the operation that this technology comprises has continuous-feeding, successive reaction, continuous discharging slag, and gaseous magnesium is condensed into liquid magnesium continuously, it is characterized in that: may further comprise the steps: the first step---close second slide valve (313), the 3rd slide valve (702) and the 4th slide valve (707), open the 3rd vacuum valve (603), and locate to vacuumize since the 4th vacuum valve (610) and the 5th vacuum valve (703), open all water coolants simultaneously; After vacuum tightness reaches 1～10Pa in the stove, begin first resistance heating wire (312) to storage bin (310), second resistance heating wire (606) of magnesium condensing chamber (607) and the ruhmkorff coil (501) of induction heating reaction chamber (500) and send electricity, make storage bin (310) temperature reach 300～500 ℃, the homo(io)thermism of magnesium condensing chamber (607) in the homo(io)thermism of 660～700 ℃ and induction heating reaction chamber (500) at 1150～1300 ℃; Second step, open charging opening (302) and first slide valve (320) on the feeding warehouse (300), being that the pelletizing made of raw material or the powder that mixes add from charging opening (302) by calcined dolomite, ferrosilicon and fluorite, after furnace charge is filled in feeding warehouse (300) and the storage bin (310), shut first slide valve (320) and charging opening (302), locate to vacuumize since first vacuum valve (301) and second vacuum valve (311); After vacuum tightness reaches 1～10Pa in the storage bin (310), and after the interior charge-temperature of storage bin (310) reaches 300～500 ℃, open second slide valve (313), and open screw feeder mechanism (400) simultaneously and make furnace charge enter induction heating reaction chamber (500) continuously; The 3rd step, when furnace charge stops 1.5～5h in induction heating reaction chamber (500) after, open the 3rd slide valve (702), and open continuous discharging slag device (701), make slag slowly enter slag charge storehouse (705); Magnesium steam is condensed into the liquid magnesium operation continuously and may further comprise the steps: the first step---in the magnesium accumulator (609) liquid level of liquid magnesium reach the accumulator height 2/3～4/5 the time, close the 3rd vacuum valve (603) and the 4th vacuum valve (610), and feed argon gas from the 4th vacuum valve (610), after gaseous tension reaches 0.01～0.1Mpa in magnesium condensing chamber (607), open second seal base (614), open lifting device (617) and make liquid magnesium shift out magnesium condensing chamber (607), carry out follow-up casting or preparation alloy; Second step---the new magnesium accumulator of in magnesium condensing chamber (607), packing into, and install second seal base (614), locate to vacuumize since the 4th vacuum valve (610), after vacuum tightness reaches 1～10Pa in the magnesium condensing chamber, open the 3rd vacuum valve (603).
6, the continuous magnesium smelting device of the induction heating according to claim 5 technology of refining magnesium continuously, it is characterized in that the continuous-feeding operation may further comprise the steps: after furnace charge all changes induction heating reaction chamber (500) in the storage bin (310), close second slide valve (313) earlier, open first slide valve (320), make the middle furnace charge of feeding warehouse (300) enter storage bin (310) and carry out preheating; Then, close first slide valve (320), open the opening for feed (302) of feeding warehouse (300), furnace charge is added in the feeding warehouse (300), behind sealing opening for feed (302), open first vacuum valve (301) and make feeding warehouse (300) vacuum tightness reach 1～10Pa; Thereby realized the without interruption of the middle furnace charge of induction heating reaction chamber (500).
7, the continuous magnesium smelting device of the induction heating according to claim 5 technology of refining magnesium continuously, it is characterized in that the continuous discharging slag operation may further comprise the steps: the first step---in slag charge storehouse (705) quantity of slag reach slag charge storehouse height 4/5 the time, stop spiral pusher mechanism (701), close the 3rd slide valve (702), open the 4th slide valve (707) beginning deslagging; After slag has been arranged, close the 3rd slide valve (702) and the 4th slide valve (707), open the 5th vacuum valve (703) and begin to vacuumize; After slag charge storehouse (705) vacuum tightness reaches 1～10Pa, open the 3rd slide valve (702), close the 5th vacuum valve (703), and open spiral pusher mechanism (701).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100359298A CN100557048C (en) | 2007-10-18 | 2007-10-18 | Continuous magnesium smelting device of a kind of induction heating and continuous process for smelting magnesium thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100359298A CN100557048C (en) | 2007-10-18 | 2007-10-18 | Continuous magnesium smelting device of a kind of induction heating and continuous process for smelting magnesium thereof |
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| Publication Number | Publication Date |
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| CN101157989A CN101157989A (en) | 2008-04-09 |
| CN100557048C true CN100557048C (en) | 2009-11-04 |
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| CNB2007100359298A Expired - Fee Related CN100557048C (en) | 2007-10-18 | 2007-10-18 | Continuous magnesium smelting device of a kind of induction heating and continuous process for smelting magnesium thereof |
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| KR101242701B1 (en) * | 2010-12-28 | 2013-03-18 | 재단법인 포항산업과학연구원 | Vertical type thermal reduction apparatus for magnesium production |
| CN102409185A (en) * | 2011-11-14 | 2012-04-11 | 宁夏华亿镁业股份有限公司 | Novel reduction method in pidgeon magnesium refining process |
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2007
- 2007-10-18 CN CNB2007100359298A patent/CN100557048C/en not_active Expired - Fee Related
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| CN101157989A (en) | 2008-04-09 |
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