CN100554234C - 用于制备高厚度涂层的透明的光可聚合体系 - Google Patents

用于制备高厚度涂层的透明的光可聚合体系 Download PDF

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Publication number
CN100554234C
CN100554234C CNB2004800224878A CN200480022487A CN100554234C CN 100554234 C CN100554234 C CN 100554234C CN B2004800224878 A CNB2004800224878 A CN B2004800224878A CN 200480022487 A CN200480022487 A CN 200480022487A CN 100554234 C CN100554234 C CN 100554234C
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CN
China
Prior art keywords
methyl
phenyl
hydroxy
formula
propan
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Expired - Fee Related
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CNB2004800224878A
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English (en)
Chinese (zh)
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CN1832912A (zh
Inventor
G·诺西尼
S·罗马纳诺
M·维斯孔蒂
G·利巴希
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Lamberti SpA
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Lamberti SpA
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/10—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms
    • C07D295/104—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms with the ring nitrogen atoms and the doubly bound oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
    • C07D295/108—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms with the ring nitrogen atoms and the doubly bound oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C225/00—Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones
    • C07C225/02—Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones having amino groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C225/14—Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones having amino groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being unsaturated
    • C07C225/16—Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones having amino groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being unsaturated and containing six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/46—Friedel-Crafts reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/63—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/64—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of functional groups containing oxygen only in singly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/76—Ketones containing a keto group bound to a six-membered aromatic ring
    • C07C49/84—Ketones containing a keto group bound to a six-membered aromatic ring containing ether groups, groups, groups, or groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/46—Polymerisation initiated by wave energy or particle radiation
    • C08F2/48—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C08F2/50—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light with sensitising agents
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/004—Photosensitive materials
    • G03F7/027—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds
    • G03F7/028—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds with photosensitivity-increasing substances, e.g. photoinitiators
    • G03F7/031—Organic compounds not covered by group G03F7/029
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • General Physics & Mathematics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polymerisation Methods In General (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CNB2004800224878A 2003-08-07 2004-08-03 用于制备高厚度涂层的透明的光可聚合体系 Expired - Fee Related CN100554234C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ITVA2003A000028 2003-08-07
IT000028A ITVA20030028A1 (it) 2003-08-07 2003-08-07 Sistemi fotopolimerizzabili trasparenti per la preparazione di rivestimenti ad elevato spessore.

Publications (2)

Publication Number Publication Date
CN1832912A CN1832912A (zh) 2006-09-13
CN100554234C true CN100554234C (zh) 2009-10-28

Family

ID=34131257

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2004800224878A Expired - Fee Related CN100554234C (zh) 2003-08-07 2004-08-03 用于制备高厚度涂层的透明的光可聚合体系

Country Status (10)

Country Link
US (1) US7534880B2 (enExample)
EP (1) EP1670740B1 (enExample)
JP (1) JP4638869B2 (enExample)
CN (1) CN100554234C (enExample)
AT (1) ATE507200T1 (enExample)
CA (1) CA2532458C (enExample)
DE (1) DE602004032452D1 (enExample)
DK (1) DK1670740T3 (enExample)
IT (1) ITVA20030028A1 (enExample)
WO (1) WO2005014515A2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104974053A (zh) * 2015-06-24 2015-10-14 天津久日化学股份有限公司 一种新的氨基酮类光引发剂及在uv-led光固化体系的应用

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ITVA20030040A1 (it) * 2003-10-27 2005-04-28 Lamberti Spa Fotoiniziatore solido bianco in polvere e procedimento per la sua preparazione.
ITVA20050049A1 (it) * 2005-08-05 2007-02-06 Lamberti Spa Sistemi fotopolimerizzabili contenenti coiniziatori a bassa estraibilita' e volatilita'
CN103601629B (zh) 2010-11-12 2015-08-26 深圳市有为化学技术有限公司 对位或间位官能团化芳香酮类化合物、其制备方法及其光聚合引发剂
CN102504054B (zh) * 2011-11-01 2014-07-02 长沙新宇高分子科技有限公司 降低直至消除voc排放的多官能团羟基酮光引发剂
BE1022066B1 (nl) * 2013-06-28 2016-02-15 Chemstream Bvba Oppervlakteactief middel en bereiding daarvan
DK3392232T3 (da) 2015-12-15 2021-04-12 Changzhou Tronly Advanced Electronic Mat Co Ltd Multifunktionel fluorenfotoinitiator og fremstilling og anvendelse deraf, og fotosensitiv resinsammensætning indeholdende fluorenfotoinitiator og anvendelse deraf
JP6833171B2 (ja) 2016-09-13 2021-02-24 常州強力先端電子材料有限公司Ｃｈａｎｇｚｈｏｕ Ｔｒｏｎｌｙ Ａｄｖａｎｃｅｄ Ｅｌｅｃｔｒｏｎｉｃ Ｍａｔｅｒｉａｌｓ Ｃｏ．，Ｌｔｄ． フルオレン類光開始剤、その製造方法、それを有する光硬化性組成物、及び光硬化分野におけるフルオレン類光開始剤の使用
US11399986B2 (en) * 2016-12-16 2022-08-02 The Procter & Gamble Company Article comprising energy curable ink
EP3584242A4 (en) 2017-02-17 2020-12-23 Changzhou Tronly Advanced Electronic Materials Co., Ltd. FLUORENYLAMINOCETONE PHOTOINITIATOR, ITS PREPARATION PROCESS AND UV PHOTOSETTING COMPOSITION CONTAINING IT
KR102764847B1 (ko) * 2018-06-29 2025-02-06 가부시키가이샤 아데카 옥심에스테르 화합물 및 이것을 함유하는 광중합개시제
CN109678735B (zh) * 2018-12-28 2022-02-22 山东久日化学科技有限公司 一种烷基胺原位回收利用技术制备

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0003002A2 (de) * 1977-12-22 1979-07-11 Ciba-Geigy Ag Verwendung von aromatisch-aliphatischen Ketonen als Photoinitiatoren, photopolymerisierbare Systeme enthaltend solche Ketone und neue aromatisch-aliphatische Ketone
US6492514B1 (en) * 1998-11-19 2002-12-10 Lamberti S.P.A. Bifunctional photoinitiators suitable for photopolymerization and photopolymerizable systems containing the same

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3715293A (en) 1971-12-17 1973-02-06 Union Carbide Corp Acetophenone-type photosensitizers for radiation curable coatings
DE2722264C2 (de) * 1977-05-17 1984-06-28 Merck Patent Gmbh, 6100 Darmstadt Verwendung von substituierten Oxyalkylphenonen als Photosensibilisatoren
EP0088050B1 (de) * 1982-02-26 1986-09-03 Ciba-Geigy Ag Photohärtbare gefärbte Massen
IT1176018B (it) * 1984-04-12 1987-08-12 Lamberti Flli Spa Chetoni aromatico alifatici polimerici o polimerizzabili adatti all'impiego come fotoiniziatori di polimerizzazione
IT1208494B (it) 1985-01-28 1989-07-10 Lamberti Flli Spa Polimerizzazione. derivati solforati di chetoni aromatico-alifatici e alifatici come fotoiniziatori di
DE3880868D1 (en) * 1987-03-26 1993-06-17 Ciba Geigy Ag Neue alpha-aminoacetophenone als photoinitiatoren.
AU3606195A (en) 1995-09-11 1997-04-01 Lamberti S.P.A. Betaketosulfonic derivatives suitable to the use as polymerization photoinitiators and photopolymerizable systems containing the same
ES2207485T3 (es) * 1999-01-12 2004-06-01 Clariant Finance (Bvi) Limited Benzofenonas y su uso como fotoiniciadores.

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0003002A2 (de) * 1977-12-22 1979-07-11 Ciba-Geigy Ag Verwendung von aromatisch-aliphatischen Ketonen als Photoinitiatoren, photopolymerisierbare Systeme enthaltend solche Ketone und neue aromatisch-aliphatische Ketone
US6492514B1 (en) * 1998-11-19 2002-12-10 Lamberti S.P.A. Bifunctional photoinitiators suitable for photopolymerization and photopolymerizable systems containing the same

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104974053A (zh) * 2015-06-24 2015-10-14 天津久日化学股份有限公司 一种新的氨基酮类光引发剂及在uv-led光固化体系的应用

Also Published As

Publication number Publication date
CA2532458C (en) 2012-01-03
WO2005014515A2 (en) 2005-02-17
WO2005014515A3 (en) 2005-04-28
EP1670740B1 (en) 2011-04-27
US7534880B2 (en) 2009-05-19
CN1832912A (zh) 2006-09-13
EP1670740A2 (en) 2006-06-21
ATE507200T1 (de) 2011-05-15
DE602004032452D1 (de) 2011-06-09
US20060246228A1 (en) 2006-11-02
JP4638869B2 (ja) 2011-02-23
DK1670740T3 (da) 2011-08-15
CA2532458A1 (en) 2005-02-17
ITVA20030028A1 (it) 2005-02-08
JP2007501776A (ja) 2007-02-01

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Granted publication date: 20091028

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