CN100551289C - Method for manufacturing flame-retardant nylon fastening tape - Google Patents
Method for manufacturing flame-retardant nylon fastening tape Download PDFInfo
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- CN100551289C CN100551289C CNB2007101538539A CN200710153853A CN100551289C CN 100551289 C CN100551289 C CN 100551289C CN B2007101538539 A CNB2007101538539 A CN B2007101538539A CN 200710153853 A CN200710153853 A CN 200710153853A CN 100551289 C CN100551289 C CN 100551289C
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- chinlon gluing
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Abstract
The invention relates to a method for manufacturing a flame-retardant nylon fastening tape, which comprises the steps of putting the nylon fastening tape into a dip dyeing machine for cleaning, and then carrying out whitening finishing; dehydrating the whitened nylon fastening tape, and raising with a raising machine; drying the treated nylon fastening tape, putting the dried nylon fastening tape into a dip dyeing machine, soaking the nylon fastening tape with a fire retardant, and dehydrating after soaking; then, the dehydrated nylon fastening tape is subjected to fire retardant finishing and gluing on a gluing machine, and finally, drying is carried out. The nylon fastening tape manufactured by the method of the invention is not easy to burn and has good flame retardant property. When the safety protection device is used for vehicles such as airplanes and automobiles, the safety of the vehicles in use can be improved.
Description
One, technical field:
The present invention relates to a kind of processing and treating method of cingulum, particularly a kind of manufacture method of flame-proof chinlon gluing buckle.
Two, background technology:
Existing common chinlon gluing buckle, when being used for the magic tape of the vehicles such as aircraft, automobile, burning easily brings potential safety hazard for the person and the vehicles.
Three, summary of the invention:
For overcoming above defective, the invention provides a kind of manufacture method of flame-proof chinlon gluing buckle, chinlon gluing buckle is carried out fire-retardant special arrangement, with the prepared flame-proof chinlon gluing buckle of this manufacture method, have anti-flaming function, can improve the safety in utilization of the vehicles.
The manufacture method of flame-proof chinlon gluing buckle of the present invention is earlier chinlon gluing buckle to be put into impregnating mangle with web-like to clean, with the finish and the spot of removing fiber surface; Chinlon gluing buckle after will cleaning is again put into band shape and is padded continuous dyeing machine and carry out whitening finishing, becomes web-like after going out machine; Chinlon gluing buckle behind whitening finishing volume is untied, dewatered with the machine of ungirding; The chinlon gluing buckle of dehydration back band hair side is fluffed with raising machine, to form fine and closely woven uniform fine hair; Then chinlon gluing buckle is dried; In impregnating mangle, at normal temperatures the chinlon gluing buckle of oven dry is soaked with fireproof agent, make fireproof agent be penetrated into chinlon gluing buckle inside, then carry out processed; On the gluing machine chinlon gluing buckle after the dehydration is being carried out flame-proof treatment and gluing with fire retardant, glue and auxiliary agent subsequently, to improve adsorbance and the fastness of fire retardant on the chinlon gluing buckle surface; At last will be in dryer through the chinlon gluing buckle oven dry of arrangement.
According to the manufacture method of flame-proof chinlon gluing buckle of the present invention, when chinlon gluing buckle was cleaned, the prescription of cleaning agent was:
Chinlon gluing buckle 180-200kg
Emulsifying agent LF100 900-1000g
Sheet alkali PJ 300-400g
Water 3800-4300kg
According to the manufacture method of flame-proof chinlon gluing buckle of the present invention, chinlon gluing buckle is carried out the process conditions of whitening finishing, be when the finishing agent temperature is 40-100 ℃, chinlon gluing buckle was handled 5-7 minute; Be preferably in the time of 60-95 ℃ and handled 5-7 minute.
In whitening finishing technology of the present invention, the prescription of finishing agent is:
Chinlon gluing buckle 180-200kg
Emulsifying agent LF-100 600-1000g
Sheet alkali PJ 50-100g
The smart SP 6000-7200cc of fluorescence
Acid gorgeous blue A2R 1100-2600cc
Glacial acetic acid HAC 300-600cc
Water softener EP-60 400-600cc
Water 3800-4300kg
In whitening finishing technology of the present invention, the finishing agent prescription is preferably:
Chinlon gluing buckle 180-200kg
Emulsifying agent LF-100 700-900g
Sheet alkali PJ 70-90g
The smart SP 6500-7000cc of fluorescence
Acid gorgeous blue A2R 1500-2400cc
Glacial acetic acid HAC 400-500cc
Water softener EP-60 400-600cc
Water 4000-4200kg
Among the present invention chinlon gluing buckle being carried out the process conditions that fireproof agent soaks is: at normal temperatures, with fireproof agent chinlon gluing buckle is carried out 3-6 hour immersion, be preferably at normal temperatures, chinlon gluing buckle is carried out 5-6 hour immersion with fireproof agent.
In fireproof agent soaking technology of the present invention, the prescription of fireproof agent is:
Fireproof agent 3500 1-3%
Water 90-110%
Fireproof agent 3500 of the present invention can be buied from clear rainbow Industry Co.,Ltd
In fireproof agent soaking technology of the present invention, the fireproof agent prescription is preferably:
Fireproof agent 3500 2-3%
Water 100-110%
The process conditions of among the present invention chinlon gluing buckle being carried out fire retardant arrangement and gluing are: with fire retardant, glue and auxiliary agent chinlon gluing buckle is carried out flame-proof treatment and the gluing of 5-10min in the time of 90-110 ℃, be preferably flame-proof treatment and the gluing of with fire retardant, glue and auxiliary agent chinlon gluing buckle being carried out 8-10min in the time of 100-110 ℃.
In flame-proof treatment of the present invention and photoresist coating process, the prescription of fire retardant, glue and auxiliary agent is:
PU oily gum 90-110%
N.N-dimethyl formamide DMF 10-20%
Fire prevention powder 608F 8-12%
PU oily gum of the present invention can be from high ancient cooking vessel fine chemistry industry (Kunshan) Co., Ltd) buy, N.N-dimethyl formamide DMF can buy from clear rainbow Industry Co.,Ltd from the powder 608F that buys, prevents fires of Wuxi Wu Yue chemical industry Co., Ltd.
In flame-proof treatment of the present invention and photoresist coating process, fire retardant, glue and auxiliary formula are preferably:
PU oily gum 100-110%
N.N-dimethyl formamide DMF 10-20%
Fire prevention powder 608F 10-12%
Chinlon gluing buckle with the inventive method manufacturing has good flame retardancy.When being used for the vehicles such as aircraft, automobile, can improve the security of the vehicles in using.
In the present invention, if not refer in particular to, all percentages are benchmark with the magic tape gross weight all, and all raw materials and equipment all can be buied from market, the conventional method in field under the compound method of each finishing agent all adopts.
Four, the specific embodiment:
Specific embodiment given below can further specify the present invention.But they are not limitation of the invention.
Embodiment 1: carry out as follows:
1, chinlon gluing buckle is put in four jiaos of cylinder impregnating mangles with web-like, carried out 30 minutes cleaning with 80 ℃ cleaning agents.
The prescription of cleaning agent is:
Chinlon gluing buckle 200kg
Emulsifying agent LF100 1000g
Sheet alkali PJ 400g
Water 3800kg
2, the chinlon gluing buckle after will cleaning is put into band shape and is padded in the continuous dyeing machine, with 60 ℃ whitening finishing agent chinlon gluing buckle is carried out 7 minutes whitening finishing, go out machine after magic tape be web-like.
In the whitening finishing technology, the prescription of whitening finishing agent is:
Chinlon gluing buckle 200kg
Emulsifying agent LF-100 800g
Sheet alkali PJ 100g
The smart SP 7200cc of fluorescence
Acid gorgeous blue A2R 2500cc
Glacial acetic acid HAC 600cc
Water softener EP-60 600cc
Water 3800kg
3, the volume of the chinlon gluing buckle behind the whitening finishing is untied with the machine of ungirding, and the chinlon gluing buckle of band hair side is carried out 3 minutes processed with dewaterer.
4, will dewatering afterwards, the chinlon gluing buckle of band hair side fluffs with raising machine.
5, the band hair side chinlon gluing buckle after the buckle face chinlon gluing buckle untied and dehydration, the fluffing is put into drying baker, in the time of 50 ℃, carry out 5 minutes prebake, and then handle 120 ℃ of oven dry of carrying out 3 minutes.
6, the chinlon gluing buckle after will drying is put in the impregnating mangle, carries out 4 hours immersion at normal temperatures with fireproof agent.
In the fire prevention soaking technology, the prescription of fireproof agent is:
Fireproof agent 3,500 3%
Water 110%
7, the chinlon gluing buckle after the fireproof agent immersion is carried out 3 minutes processed with dewaterer.
8, with JC-CT125-1 gluing machine (can become mechanical Co., Ltd to buy) from the village, Xiamen to 110 ℃ antiflaming finishing agent, carry out 10 minutes flame-proof treatment and gluing through the chinlon gluing buckle after the above-mentioned arrangement.
In flame-proof treatment and the photoresist coating process, the prescription of fire retardant, glue and auxiliary agent is:
PU oily gum 90%
N.N-dimethyl formamide DMF 20%
Fire prevention powder 608F 8%
9, will put into the drying baker at gluing machine rear portion through the chinlon gluing buckle after flame-proof treatment and the gluing, in the time of 50 ℃, carry out 5 minutes prebake, and then handle 120 ℃ of oven dry of carrying out 3 minutes.
Embodiment 2: carry out as follows:
1, chinlon gluing buckle is put in the common impregnating mangle with web-like, carried out 20 minutes cleaning with 90 ℃ cleaning agents.
The prescription of cleaning agent is:
Chinlon gluing buckle 200kg
Emulsifying agent LF100 900g
Sheet alkali PJ 300g
Water 4000kg
2, the chinlon gluing buckle after will cleaning is put into band shape and is padded in the continuous dyeing machine, with 80 ℃ whitening finishing agent chinlon gluing buckle is carried out 6 minutes whitening finishing, go out machine after magic tape be web-like.
In the whitening finishing technology, the prescription of whitening finishing agent is:
Chinlon gluing buckle 200kg
Emulsifying agent LF-100 900g
Sheet alkali PJ 85g
The smart SP 7000cc of fluorescence
Acid gorgeous blue A2R 2200cc
Glacial acetic acid HAC 500cc
Water softener EP-60 500cc
Water 4000kg
3, the volume of the chinlon gluing buckle behind the whitening finishing is untied with the machine of ungirding, and the chinlon gluing buckle of band hair side is carried out 3 minutes processed with dewaterer.
4, will dewatering afterwards, the chinlon gluing buckle of band hair side fluffs with raising machine.
5, the rear portion drying baker that the chinlon gluing buckle and the band hair side chinlon gluing buckle after the dehydration of the buckle face untied are put into gluing machine again carries out 3 minutes prebake, and then handles 110 ℃ of oven dry of carrying out 4 minutes in the time of 55 ℃.
6, the chinlon gluing buckle after will drying is put in the impregnating mangle, carries out 5 hours immersion at normal temperatures with fireproof agent.
In the fire prevention soaking technology, the prescription of fireproof agent is:
Fireproof agent 3,500 2%
Water 100%
7, the chinlon gluing buckle after the fireproof agent immersion is carried out 3 minutes processed with dewaterer.
8, with the JC-CT125-1 gluing machine in 100 ℃ antiflaming finishing agent, carry out 8 minutes flame-proof treatment and gluing through the chinlon gluing buckle after the above-mentioned processing.
In flame-proof treatment and the photoresist coating process, the prescription of fire retardant, glue and auxiliary agent is:
PU oily gum 100%
N.N-dimethyl formamide DMF 15%
Fire prevention powder 608F 10%
9, will put into the rear portion drying baker of gluing machine through the chinlon gluing buckle of flame-proof treatment and gluing again, and in the time of 55 ℃, carry out 3 minutes prebake, and then the oven dry of carrying out in the time of 110 ℃ 4 minutes is handled.
Embodiment 3: carry out as follows:
1, chinlon gluing buckle is put in the common impregnating mangle with web-like, carried out 30 minutes cleaning with 80 ℃ cleaning agents.
The prescription of cleaning agent is:
Chinlon gluing buckle 200kg
Emulsifying agent LF100 1000g
Sheet alkali PJ 400g
Water 4300kg
2, the chinlon gluing buckle after will cleaning is put into band shape and is padded in the continuous dyeing machine, with 100 ℃ whitening finishing agent chinlon gluing buckle is carried out 5 minutes whitening finishing, go out machine after magic tape be web-like.
In the whitening finishing technology, the prescription of whitening finishing agent is:
Chinlon gluing buckle 200kg
Emulsifying agent LF-100 1000g
Sheet alkali PJ 65g
The smart SP 6500cc of fluorescence
Acid gorgeous blue A2R 1200cc
Glacial acetic acid HAC 400cc
Water softener EP-60 400cc
Water 4300kg
3, the volume of the chinlon gluing buckle behind the whitening finishing is untied with the machine of ungirding, and the chinlon gluing buckle of band hair side is carried out 3 minutes processed with dewaterer.
4, will dewatering afterwards, the chinlon gluing buckle of band hair side fluffs with raising machine.
5, the rear portion drying baker that the chinlon gluing buckle and the band hair side chinlon gluing buckle after the dehydration of the buckle face untied are put into gluing machine is again handled 100 ℃ of oven dry of carrying out 5 minutes.
6, the chinlon gluing buckle after will drying is put in the impregnating mangle, carries out 6 hours immersion at normal temperatures with fireproof agent.
In the fire prevention soaking technology, the prescription of fireproof agent is:
Fireproof agent 3,500 1%
Water 90%
7, the chinlon gluing buckle after the fireproof agent immersion is carried out 3 minutes processed with dewaterer.
8, with the JC-CT125-1 gluing machine in 90 ℃ antiflaming finishing agent, carry out 6 minutes flame-proof treatment and gluing through the chinlon gluing buckle after the above-mentioned processing.
In flame-proof treatment and the photoresist coating process, the prescription of fire retardant, glue and auxiliary agent is:
PU oily gum 110%
N.N-dimethyl formamide DMF 10%
Fire prevention powder 608F 12%
9, will put into the drying baker at gluing machine rear portion through the chinlon gluing buckle of flame-proof treatment and gluing again, the oven dry of carrying out in the time of 100 ℃ 5 minutes is handled.
The experimental result of flame-proof chinlon gluing buckle of the present invention and existing common chinlon gluing buckle contrast (according to test of US Airways fire-protection standard and comparison) as shown in table 1:
Table 1
| Code name | Sample | The average residual flame time (Sec) | The mean droplet flame time (Sec) | Average burning length (cm) |
| 1 | Existing common chinlon gluing buckle | ＞15 do not meet standard | ＞5 do not meet standard | ＞20.3 do not meet standard |
| 2 | The flame-proof chinlon gluing buckle of the embodiment of the invention 1 | ＜15 meet standard | ＜5 meet standard | ＜20.3 meet standard |
| 3 | The flame-proof chinlon gluing buckle of the embodiment of the invention 2 | ＜15 meet standard | ＜5 meet standard | ＜20.3 meet standard |
| 4 | The flame-proof chinlon gluing buckle of the embodiment of the invention 3 | ＜15 meet standard | ＜5 meet standard | ＜20.3 meet standard |
As seen from Table 1, sample of the present invention is stronger than common chinlon gluing buckle fire retardancy, can be used for the vehicles such as aircraft, automobile.
Claims (4)
1, a kind of manufacture method of flame-proof chinlon gluing buckle, it is characterized in that earlier in impregnating mangle chinlon gluing buckle being carried out 20-30 minute cleaning with 80-90 ℃ cleaning agent, then chinlon gluing buckle is carried out 5-7 minute whitening finishing with 40-100 ℃ whitening finishing agent, then dewater, oven dry, at normal temperatures, the chinlon gluing buckle of oven dry is put into impregnating mangle to be soaked 3-6 hour with fireproof agent, dehydration then, in gluing machine, in the time of 90-110 ℃, use fire retardant then, glue and auxiliary agent carry out 5-10 minute flame-proof treatment and gluing to the chinlon gluing buckle after dewatering, and dry 3-5 minute in the time of 100-120 ℃ in drying baker at last;
Wherein: the prescription of described cleaning agent is:
Chinlon gluing buckle 180-200kg emulsifying agent LF100 900-1000g
Sheet alkali PJ 300-400g water 3800-4300kg;
The prescription of described whitening finishing agent is:
Chinlon gluing buckle 180-200kg emulsifying agent LF-100 600-1000g
The smart SP 6000-7200cc of sheet alkali PJ 50-100g fluorescence
Acid gorgeous blue A2R 1100-2600cc glacial acetic acid HAC 300-600cc
Water softener EP-60 400-600cc water 3800-4300kg;
The prescription of described fireproof agent is that percentage is benchmark with the magic tape gross weight:
Fireproof agent 3500 1-3% water 90-110%;
Described fire retardant, glue and auxiliary formula are that percentage is benchmark with the magic tape gross weight:
PU oily gum 90-110% N.N-dimethyl formamide DMF 10-20%
Fire prevention powder 608F 8-12%.
2, a kind of manufacture method of flame-proof chinlon gluing buckle, it is characterized in that earlier in impregnating mangle chinlon gluing buckle being carried out 20-30 minute cleaning with 80-90 ℃ cleaning agent, then chinlon gluing buckle is carried out 5-7 minute whitening finishing with 60-95 ℃ whitening finishing agent, then dewater, oven dry, at normal temperatures, the chinlon gluing buckle of oven dry is put into impregnating mangle to be soaked 5-6 hour with fireproof agent, dehydration then, in gluing machine, in the time of 100-110 ℃, use fire retardant then, glue and auxiliary agent carry out 8-10 minute flame-proof treatment and gluing to the chinlon gluing buckle after dewatering, and dry 3-5 minute in the time of 100-120 ℃ in drying baker at last;
Wherein: the prescription of described cleaning agent is:
Chinlon gluing buckle 180-200kg emulsifying agent LF100 900-1000g
Sheet alkali PJ 300-400g water 3800-4300kg;
The prescription of described whitening finishing agent is:
Chinlon gluing buckle 180-200kg emulsifying agent LF-100 600-1000g
The smart SP 6000-7200cc of sheet alkali PJ 50-100g fluorescence
Acid gorgeous blue A2R 1100-2600cc glacial acetic acid HAC 300-600cc
Water softener EP-60 400-600cc water 3800-4300kg;
The prescription of described fireproof agent is that percentage is benchmark with the magic tape gross weight:
Fireproof agent 3500 1-3% water 90-110%;
Described fire retardant, glue and auxiliary formula are that percentage is benchmark with the magic tape gross weight:
PU oily gum 90-110% N.N-dimethyl formamide DMF 10-20%
Fire prevention powder 608F 8-12%.
3, the manufacture method of flame-proof chinlon gluing buckle according to claim 1 and 2 is characterized in that the prescription of described whitening finishing agent is:
Chinlon gluing buckle 180-200kg emulsifying agent LF-100 700-900g
The smart SP 6500-7000cc of sheet alkali PJ 70-90g fluorescence
Acid gorgeous blue A2R 1500-2400cc glacial acetic acid HAC 400-500cc
Water softener EP-60 400-600cc water 4000-4200kg.
4, the manufacture method of flame-proof chinlon gluing buckle according to claim 1 and 2 is characterized in that the prescription of described fire retardant, glue and auxiliary agent is, percentage is benchmark with the magic tape gross weight:
PU oily gum 100-110% fire prevention powder 608F 10-12%
N.N-dimethyl formamide DMF 10-20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007101538539A CN100551289C (en) | 2007-09-14 | 2007-09-14 | Method for manufacturing flame-retardant nylon fastening tape |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007101538539A CN100551289C (en) | 2007-09-14 | 2007-09-14 | Method for manufacturing flame-retardant nylon fastening tape |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101116566A CN101116566A (en) | 2008-02-06 |
| CN100551289C true CN100551289C (en) | 2009-10-21 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2007101538539A Active CN100551289C (en) | 2007-09-14 | 2007-09-14 | Method for manufacturing flame-retardant nylon fastening tape |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101942763B (en) * | 2010-05-28 | 2012-06-27 | 无锡百和织造股份有限公司 | Method for manufacturing halogen-free flame retardant nylon sticky buckle strap |
| CN102182058B (en) * | 2011-03-17 | 2012-09-12 | 无锡百和织造股份有限公司 | Method for manufacturing halogen-free, washing-resistant and flame retardant polyamide hook and loop fastener |
| CN103572611B (en) * | 2013-11-20 | 2015-08-26 | 无锡百和织造股份有限公司 | Heat-resistant flame-retardant polyester and nylon interwoven magic tape and manufacturing method thereof |
| CN105297457A (en) * | 2015-10-29 | 2016-02-03 | 六安市海洋羽毛有限公司 | Flame retardant treatment technology for down feather |
| CN111227448A (en) * | 2020-03-16 | 2020-06-05 | 无锡百和织造股份有限公司 | Manufacturing method of low-smoke low-toxicity flame-retardant nylon fastening tape |
| CN111764152A (en) * | 2020-07-08 | 2020-10-13 | 无锡百和织造股份有限公司 | Manufacturing method of low-cost, low-smoke, low-toxicity and flame-retardant nylon fastening tape |
| CN111920146A (en) * | 2020-08-04 | 2020-11-13 | 天津兴华织造有限公司 | Manufacturing method of low-smoke low-toxicity antistatic fastening tape |
| CN113892732A (en) * | 2021-09-24 | 2022-01-07 | 瑞安市华升塑料织带有限公司 | Method for manufacturing fireproof fastening tape |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020160143A1 (en) * | 1997-09-03 | 2002-10-31 | Shepard William H. | Fastener loop material, its manufacture, and products incorporating the material |
| CN1393189A (en) * | 2001-07-03 | 2003-01-29 | 台湾百和工业股份有限公司 | Adhesive fastening belt and its making method |
-
2007
- 2007-09-14 CN CNB2007101538539A patent/CN100551289C/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020160143A1 (en) * | 1997-09-03 | 2002-10-31 | Shepard William H. | Fastener loop material, its manufacture, and products incorporating the material |
| CN1393189A (en) * | 2001-07-03 | 2003-01-29 | 台湾百和工业股份有限公司 | Adhesive fastening belt and its making method |
| WO2003089705A2 (en) * | 2002-04-18 | 2003-10-30 | Velcro Industries B.V. | Fastener loop material, its manufacture, and products incorporating the material |
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| CN101116566A (en) | 2008-02-06 |
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Application publication date: 20080206 Assignee: Dongguan Bai Hong Industrial Co., Ltd. Assignor: Wuxi Baihe Weaving Co., Ltd. Contract record no.: 2010320000054 Denomination of invention: Method for preparation of flame-proof chinlon gluing buckle Granted publication date: 20091021 License type: Common License Record date: 20100220 |
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Address after: No.18 Hexin Road, Xishan Economic Development Zone, Wuxi City, Jiangsu Province Patentee after: Jiangsu Baihong composite material technology Co.,Ltd. Address before: 214101 Jiangsu city of Wuxi province Xishan Economic Development Zone Foreign Industrial Park Hexin Road No. 18 Patentee before: WUXI PAIHO TEXTILES Co.,Ltd. |
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