CN109680483A - A kind of washable, antibacterial, the preparation process of inflaming retarding fabric - Google Patents
A kind of washable, antibacterial, the preparation process of inflaming retarding fabric Download PDFInfo
- Publication number
- CN109680483A CN109680483A CN201811600397.2A CN201811600397A CN109680483A CN 109680483 A CN109680483 A CN 109680483A CN 201811600397 A CN201811600397 A CN 201811600397A CN 109680483 A CN109680483 A CN 109680483A
- Authority
- CN
- China
- Prior art keywords
- follows
- pad
- flame
- antibiotic
- preparation process
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/12—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen combined with specific additives
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/13—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic System
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
Abstract
The invention discloses a kind of washable, antibacterials, the preparation process of inflaming retarding fabric, including sequentially follow the steps below: pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant ZR-2 400-500g/L, crosslinking agent GX-100 3-4g/L, phosphoric acid 20-23g/L, fiber protection agent DH6500 20-26g/L；During the antibiotic finish, the prescription of antibiotic finishing solution used are as follows: anti-bacteium deodorization finishing agent SCJ-2000 40-60g/L, AB resin 15-25g/L, without influencing each other between antibacterial of the present invention, flame-proof finishing process, fabric after present invention process processing, after washing 50 times, damage length≤8.0cm, antibiotic rate >=90.0%.
Description
Technical field
The present invention relates to fabric preparation fields, more particularly to a kind of washable, antibacterial, the preparation process of inflaming retarding fabric.
Background technique
C/N blended fabric has the characteristics of high-wearing feature, high-tenacity and high snugness of fit, is the required of Military Clothing
Product.However, often bringing on a disaster to us since they have inflammability.The it is proposeds such as extraordinary industrial and protective clothing, military uniform are stringent
Heat-insulating, fire-preventing requirement.From the point of view of long-range trend, fire-retardant demand is one of the primary demand in daily life.
Severe due to battlefield and field environment, for soldier in the flames of war, professional worker is inevitable in production and work
Touch various bacterium and burning, situations such as drenching with rain, in the prior art, the mutual shadow of flame-proof treatment and antibiotic finish of fabric
It rings, effect both with good the two can not be reached, and at the same time it is not washable to have fire-retardant, anti-microbial property a fabric, it can not
Meets the needs of people.
Therefore, exploitation is a suitable for C/N blended fabric, has washable, antibacterial, the preparation process of flame retarding function, urgently
It is to be solved.
Summary of the invention
It influences each other to solve the flame-proof treatment of C/N blended fabric and antibiotic finish, fabric has washable, antibacterial, resistance simultaneously
Function is fired, the present invention provides a kind of washable, antibacterial, the preparation process of inflaming retarding fabric, reaches antibacterial finishing process not and influence fire-retardant
Performance and washable, preferred due to flame-proof treatment formula of liquid, flame-proof treatment scene smell mitigates significantly, it is fire-retardant bake it is uncrosslinked
The tarring of fire retardant mitigates significantly, reduces baker cleaning time and improves production efficiency, compared with the existing technology middle CP resistance
Combustion process production efficiency improves 40%.
In order to achieve the above object, it is achieved by following technical solution:
A kind of washable, antibacterial, the preparation process of inflaming retarding fabric, including sequentially follow the steps below:
Pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant ZR-2 400-500g/
L, crosslinking agent GX-100 3-4g/L, phosphoric acid 20-23g/L, fiber protection agent DH6500 20-26g/L；
During the antibiotic finish, the prescription of antibiotic finishing solution used are as follows: anti-bacteium deodorization finishing agent SCJ-
200040-60g/L, AB resin 15-25g/L.
Preferably, the pre-treatment, process flow are as follows: cloth margin to seam → cold pad--batch → kiering bleaching → sizing is turned over, it is described cold
Roll cold rolling working solution prescription used in heap technique are as follows: caustic soda 40g/L, hydrogen peroxide 8g/L, the clot for including in cold-pad-batch process
Step is banked up, clot stacking time is 12 hours.
Preferably, working solution prescription is bleached in kiering used in the kiering bleaching process are as follows: desizing scouring agent AWR
4g/L, chelating agent 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
Preferably, the dye bottom, process flow are as follows: pad dye bottom dye liquor → preliminary drying → drying, bottom semi-finished product must be contaminated, padded
The liquid carrying rate for contaminating bottom dye liquor technique is 60%, and the temperature of the preliminary drying technique is 110 DEG C, and the temperature of stoving process is 130 DEG C.
Preferably, the stamp, process flow are as follows: dry → baking → by the semi-finished product → stamp → of dye bottom technique and steam
Change → drying obtains stamp semi-finished product.
Preferably, the CP flame-proof treatment, process flow: by stamp treated semi-finished product → pad fire retarding treating liquid
→ dry → bake → wash → soaps, and → washing → dries, it is described pad fire retarding treating liquid after, liquid carrying rate 60-70% is described
Baking temperature is 170-180 DEG C, bakes and banks up with earth time 2-3min.
Preferably, antibiotic finish, process flow: padding antibiotic finishing solution → drying, described to pad antibiotic finishing solution technique
Afterwards, liquid carrying rate 63%-67%.
Preferably, in antibacterial finishing process, the stoving process, the condition of drying is under the conditions of 130-140 DEG C of temperature
It bakes 100-180 seconds.
Preferably, the fabric is C/N blended fabric.
The utility model has the advantages that
The preparation-obtained fabric of the present invention, is provided simultaneously with washable, antibacterial, fire-retardant technical effect, while water-fastness jail
Soundness performance is very excellent, will not influence each other between antibacterial, flame-proof treatment, will not influence the color of fabric, and this hair
The bright fabric not only has antibacterial, fire-retardant function, while the fabric has good washable effect, achieves technical
It breaks through.
Without influencing each other between antibacterial of the present invention, flame-proof finishing process, after washing 50 times, damage length≤
8.0cm will not occur afterflame and to glow, and select amount of flame-retardant agent except the fire retardant of other models, the present invention, crosslinking
Agent, baking temperature cannot reach the technical effect in the present invention.
While washable flame retardant effect improves, fire-retardant treatment liquid content of formaldehyde is reduced fabric of the invention, arranges scene
Smell mitigates significantly, while the fire-retardant tarring for baking uncrosslinked fire retardant mitigates significantly, reduces baker cleaning time and mentions
High efficiency reaches 40%.
Gained antibacterial fabric of the invention is functional, after washing 50 times, still reaches >=99% level, and for using
Flame retardant property under other fire retarding treating liquids and process conditions, than the antibacterial fabric performance prepared under process conditions of the present invention
It is inferior very much.
Specific embodiment
Embodiment 1
A kind of preparation process having washable, antibacterial, flame retarding function C/N blended fabric, including sequentially follow the steps below:
Pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant ZR-2 400g/L is handed over
Join agent GX-100 3g/L, phosphoric acid 20g/L, fiber protection agent DH6500 20g/L；It is used during the antibiotic finish
The prescription of antibiotic finishing solution are as follows: anti-bacteium deodorization finishing agent SCJ-2000 40g/L, AB resin 15g/L.
The pre-treatment, process flow are as follows: turn over cloth margin to seam → cold pad--batch → kiering bleaching → sizing, the cold-pad-batch process
Used cold rolling working solution prescription are as follows: step is banked up in caustic soda 40g/L, hydrogen peroxide 8g/L, the clot for including in cold-pad-batch process,
Clot stacking time is 12 hours.
Working solution prescription is bleached in used kiering in the kiering bleaching process are as follows: desizing scouring agent AWR 4g/L, chela
Mixture 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
The dye bottom, process flow are as follows: pad dye bottom dye liquor → preliminary drying → drying, bottom semi-finished product must be contaminated, pad dye bottom dye
The liquid carrying rate of liquid technique is 60%, and the temperature of the preliminary drying technique is 110 DEG C, and the temperature of stoving process is 130 DEG C.
The stamp, process flow are as follows: dry → baking → by the semi-finished product → stamp → of dye bottom technique and evaporate → dry
It is dry, obtain stamp semi-finished product.
The CP flame-proof treatment, process flow: by stamp treated semi-finished product → pad fire retarding treating liquid → drying
→ baking → washes, and → soaping → is washed → is dried, it is described pad fire retarding treating liquid after, liquid carrying rate 60%, the baking temperature is
170 DEG C, bake and bank up with earth time 2min.
The antibiotic finish, process flow: padding antibiotic finishing solution → drying, it is described pad antibiotic finishing solution technique after,
Liquid carrying rate is 63%, and in the stoving process, the condition of drying is to bake 100 seconds under the conditions of 130 DEG C of temperature.
Fire-retardant treatment liquid content of formaldehyde of the present invention reduces, and is detected according to 100 standard of Oeko-Tex, PFOS, PFOA contain
Measure equal 0.1 μ g/m of <2, arrange live smell and mitigate significantly, the fire-retardant tarring for baking uncrosslinked fire retardant mitigates significantly, reduces
Baker cleaning time and raising production efficiency, middle CP flame retarding process production efficiency improves 30% compared with the existing technology.
Embodiment 2
A kind of washable, antibacterial, the preparation process of fire-retardant C/N blended fabric, including sequentially follow the steps below:
Pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant ZR-2 450g/L is handed over
Join agent GX-100 3.5g/L, phosphoric acid 22g/L, fiber protection agent DH6500 25g/L；It is used during the antibiotic finish
Antibiotic finishing solution prescription are as follows: SCJ-2000 50g/L, AB resin 20g/L.
The pre-treatment, process flow are as follows: turn over cloth margin to seam → cold pad--batch → kiering bleaching → sizing, the cold-pad-batch process
Used cold rolling working solution prescription are as follows: step is banked up in caustic soda 40g/L, hydrogen peroxide 8g/L, the clot for including in cold-pad-batch process,
Clot stacking time is 12 hours.
In the kiering bleaching process, working solution prescription is bleached in used kiering are as follows: desizing scouring agent AWR 4g/L, chela
Mixture 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
The dye bottom, process flow are as follows: pad dye bottom dye liquor → preliminary drying → drying, bottom semi-finished product must be contaminated, pad dye bottom dye
The liquid carrying rate of liquid technique is 60%, and the temperature of the preliminary drying technique is 110 DEG C, and the temperature of stoving process is 130 DEG C.
The stamp, process flow are as follows: dry → baking → by the semi-finished product → stamp → of dye bottom technique and evaporate → dry
It is dry, obtain stamp semi-finished product.
The CP flame-proof treatment, process flow: by stamp treated semi-finished product → pad fire retarding treating liquid → drying
→ baking → washes, and → soaping → is washed → is dried, it is described pad fire retarding treating liquid after, liquid carrying rate 65%, the baking temperature is
175 DEG C, bake and bank up with earth time 2.5min.
The antibiotic finish, process flow: padding antibiotic finishing solution → drying, it is described pad antibiotic finishing solution technique after,
Liquid carrying rate is 65%, and in the stoving process, the condition of drying is to bake 120 seconds under the conditions of 135 DEG C of temperature.
Fire-retardant treatment liquid content of formaldehyde of the present invention reduces, and is detected according to 100 standard of Oeko-Tex, PFOS, PFOA contain
Measure equal 0.1 μ g/m of <2, arrange live smell and mitigate significantly, the fire-retardant tarring for baking uncrosslinked fire retardant mitigates significantly, reduces
Baker cleaning time and raising production efficiency, middle CP flame retarding process production efficiency improves 40% compared with the existing technology.
Embodiment 3
A kind of washable, antibacterial, the preparation process of fire-retardant C/N blended fabric, including sequentially follow the steps below:
Pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant ZR-2 500g/L is handed over
Join agent GX-100 4g/L, phosphoric acid 23g/L, fiber protection agent DH6500 26g/L；It is used during the antibiotic finish
The prescription of antibiotic finishing solution are as follows: anti-bacteium deodorization finishing agent SCJ-2000 60g/L, AB resin 25g/L.
The pre-treatment, process flow are as follows: turn over cloth margin to seam → cold pad--batch → kiering bleaching → sizing, the cold-pad-batch process
Used cold rolling working solution prescription are as follows: step is banked up in caustic soda 40g/L, hydrogen peroxide 8g/L, the clot for including in cold-pad-batch process,
Clot stacking time is 12 hours.
Working solution prescription is bleached in used kiering in the kiering bleaching process are as follows: desizing scouring agent AWR 4g/L, chela
Mixture 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
The dye bottom, process flow are as follows: pad dye bottom dye liquor → preliminary drying → drying, bottom semi-finished product must be contaminated, pad dye bottom dye
The liquid carrying rate of liquid technique is 60%, and the temperature of the preliminary drying technique is 110 DEG C, and the temperature of stoving process is 130 DEG C.
The stamp, process flow are as follows: dry → baking → by the semi-finished product → stamp → of dye bottom technique and evaporate → dry
It is dry, obtain stamp semi-finished product.
The CP flame-proof treatment, process flow: by stamp treated semi-finished product → pad fire retarding treating liquid → drying
→ baking → washes, and → soaping → is washed → is dried, it is described pad fire retarding treating liquid after, liquid carrying rate 70%, the baking temperature is
180 DEG C, bake and bank up with earth time 3min.
The antibiotic finish, process flow: padding antibiotic finishing solution → drying, it is described pad antibiotic finishing solution technique after,
Liquid carrying rate is 67%, and in the stoving process, the condition of drying is to bake 180 seconds under the conditions of 140 DEG C of temperature.
Fire-retardant treatment liquid content of formaldehyde of the present invention reduces, and is detected according to 100 standard of Oeko-Tex, PFOS, PFOA contain
Measure equal 0.1 μ g/m of <2, arrange live smell and mitigate significantly, the fire-retardant tarring for baking uncrosslinked fire retardant mitigates significantly, reduces
Baker cleaning time and raising production efficiency, middle CP flame retarding process production efficiency improves 35% compared with the existing technology.
Comparative example 1
A kind of preparation process of C/N blended fabric, including sequentially follow the steps below:
Pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant ZR-2 400g/L is handed over
Join agent GX-100 2g/L, phosphoric acid 20g/L, fiber protection agent DH6500 35g/L；It is used during the antibiotic finish
The prescription of antibiotic finishing solution are as follows: anti-bacteium deodorization finishing agent SCJ-2000 20g/L, AB resin 10g/L.
The pre-treatment, process flow are as follows: turn over cloth margin to seam → cold pad--batch → kiering bleaching → sizing, the cold-pad-batch process
Used cold rolling working solution prescription are as follows: step is banked up in caustic soda 40g/L, hydrogen peroxide 8g/L, the clot for including in cold-pad-batch process,
Clot stacking time is 12 hours.
In the kiering bleaching process, working solution prescription is bleached in used kiering are as follows: desizing scouring agent AWR 4g/L, chela
Mixture 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
The dye bottom, process flow are as follows: pad dye bottom dye liquor → preliminary drying → drying, bottom semi-finished product must be contaminated, pad dye bottom dye
The liquid carrying rate of liquid technique is 60%, and the temperature of the preliminary drying technique is 110 DEG C, and the temperature of stoving process is 130 DEG C.
The stamp, process flow are as follows: dry → baking → by the semi-finished product → stamp → of dye bottom technique and evaporate → dry
It is dry, obtain stamp semi-finished product.
The CP flame-proof treatment, process flow: by stamp treated semi-finished product → pad fire retarding treating liquid → drying
→ baking → washes, and → soaping → is washed → is dried, it is described pad fire retarding treating liquid after, liquid carrying rate 65%, the baking temperature is
170 DEG C, bake and bank up with earth time 2.5min.
The antibiotic finish, process flow: padding antibiotic finishing solution → drying, it is described pad antibiotic finishing solution technique after,
Liquid carrying rate is 65%, and in the stoving process, the condition of drying is to bake 120 seconds under the conditions of 135 DEG C of temperature.
A kind of preparation process of the C/N blended fabric of comparative example 2, including sequentially follow the steps below:
Pre-treatment → dye bottom → stamp → antibiotic finish → CP flame-proof treatment → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant aflammit kwb
300g/L, crosslinking agent HX-80 1g/L, phosphoric acid 20g/L, fiber protection agent DH6500 40g/L；The process of the antibiotic finish
In, the prescription of antibiotic finishing solution used are as follows: anti-bacteium deodorization finishing agent SCJ-2000 70g/L, other commercially available crosslinked resin 10g/
L。
The pre-treatment, process flow are as follows: turn over cloth margin to seam → cold pad--batch → kiering bleaching → sizing, the cold-pad-batch process
Used cold rolling working solution prescription are as follows: step is banked up in caustic soda 40g/L, hydrogen peroxide 8g/L, the clot for including in cold-pad-batch process,
Clot stacking time is 12 hours.
In the kiering bleaching process, working solution prescription is bleached in used kiering are as follows: desizing scouring agent AWR 4g/L, chela
Mixture 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
The dye bottom, process flow are as follows: pad dye bottom dye liquor → preliminary drying → drying, bottom semi-finished product must be contaminated, pad dye bottom dye
The liquid carrying rate of liquid technique is 60%, and the temperature of the preliminary drying technique is 110 DEG C, and the temperature of stoving process is 130 DEG C.
The stamp, process flow are as follows: dry → baking → by the semi-finished product → stamp → of dye bottom technique and evaporate → dry
It is dry, obtain stamp semi-finished product.
The antibiotic finish, process flow: padding antibiotic finishing solution → drying, it is described pad antibiotic finishing solution technique after,
Liquid carrying rate is 65%, and in the stoving process, the condition of drying is to bake 120 seconds under the conditions of 135 DEG C of temperature.
The CP flame-proof treatment, process flow: semi-finished product after antibiotic finish → pad fire retarding treating liquid → drying
→ baking → washes, and → soaping → is washed → is dried, it is described pad fire retarding treating liquid after, liquid carrying rate 65%, the baking temperature is
170 DEG C, bake and bank up with earth time 2.5min.
Comparative example 3
A kind of preparation process of C/N blended fabric, including sequentially follow the steps below:
Pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant aflammit kwb
300g/L, crosslinking agent HX-80 1g/L, phosphoric acid 20g/L, fiber protection agent DH6500 40g/L；The process of the antibiotic finish
In, the prescription of antibiotic finishing solution used are as follows: anti-bacteium deodorization finishing agent SCJ-2000 70g/L.
The pre-treatment, process flow are as follows: turn over cloth margin to seam → cold pad--batch → kiering bleaching → sizing, the cold-pad-batch process
Used cold rolling working solution prescription are as follows: step is banked up in caustic soda 40g/L, hydrogen peroxide 8g/L, the clot for including in cold-pad-batch process,
Clot stacking time is 12 hours.
In the kiering bleaching process, working solution prescription is bleached in used kiering are as follows: desizing scouring agent AWR 4g/L, chela
Mixture 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
The dye bottom, process flow are as follows: pad dye bottom dye liquor → preliminary drying → drying, bottom semi-finished product must be contaminated, pad dye bottom dye
The liquid carrying rate of liquid technique is 60%, and the temperature of the preliminary drying technique is 110 DEG C, and the temperature of stoving process is 130 DEG C.
The stamp, process flow are as follows: dry → baking → by the semi-finished product → stamp → of dye bottom technique and evaporate → dry
It is dry, obtain stamp semi-finished product.
The CP flame-proof treatment, process flow: by stamp treated semi-finished product → pad fire retarding treating liquid → drying
→ baking → washes, and → soaping → is washed → is dried, it is described pad fire retarding treating liquid after, liquid carrying rate 65%, the baking temperature is
150 DEG C, bake and bank up with earth time 2.5min.
The antibiotic finish, process flow: padding antibiotic finishing solution → drying, it is described pad antibiotic finishing solution technique after,
Liquid carrying rate is 65%, and in the stoving process, the condition of drying is to bake 120 seconds under the conditions of 135 DEG C of temperature.
Reference standard:
Quality is detected according to the requirement of U.S.'s AATCC standard, the world 100 standard of Oeko-Tex,
Wherein:
Product of the present invention and comparative example are washed by GB/T17596-1998；
Product of the present invention and comparative example are by GB GB8965-98 test flame retardant property result；
Product of the present invention and comparative example are by GB/T20944.2-2007 test bacteriostasis rate result；
Product of the present invention and comparative example are by AATCC 61-2A test washing color firmness；
Product of the present invention and comparative example are by the test rub resistance grade of ISO 105；
Product of the present invention and comparative example are by the test environmental-protecting performance of Oeko-Tex 100.
Testing result such as table 1:
Table 1:
From the data in table 1, it can be seen that nothing influences each other between antibacterial of the present invention, flame-proof finishing process, after washing 50 times,
Length≤8.0cm is damaged, afterflame will not occur and is glowed, and selects the fire retardant except the fire retardant of other models, the present invention
Dosage, crosslinking agent, baking temperature cannot reach the technical effect in the present invention.
While washable flame retardant effect improves, fire-retardant treatment liquid content of formaldehyde is reduced fabric of the invention, arranges scene
Smell mitigates significantly, while the fire-retardant tarring for baking uncrosslinked fire retardant mitigates significantly, reduces baker cleaning time and mentions
High efficiency reaches 40%.
Gained antibacterial fabric of the invention is functional, after washing 50 times, still reaches >=99% level, and for using
Flame retardant property under other fire retarding treating liquids and process conditions, than the antibacterial fabric performance prepared under process conditions of the present invention
It is inferior very much.
Remarks: it is as follows that the production of substance of the present invention produces house:
The crosslinking agent GX-100, production produce family: Ke Te Chemical Co., Ltd., Shijiazhuang City federation；
The fiber protection agent DH6500, production produce family: Ke Te Chemical Co., Ltd., Shijiazhuang City federation；
The fire retardant ZR-2, Ke Te Chemical Co., Ltd., Shijiazhuang City federation；
The AB resin, production produce family: Tuo Na chemical company；
The anti-bacteium deodorization finishing agent SCJ-2000, production produce family: Beijing Jie Ershuan High Seience Technology Co., Ltd..
Obviously, various changes and modifications can be made to the invention without departing from essence of the invention by those skilled in the art
Mind and range.In this way, if these modification and variations of the invention belong to the range of the claims in the present invention and its equivalent technologies
Within, then the invention is intended to include these modification and variations.
Claims (9)
1. a kind of washable, antibacterial, the preparation process of inflaming retarding fabric, which is characterized in that including sequentially following the steps below:
Pre-treatment → dye bottom → stamp → CP flame-proof treatment → antibiotic finish → preshrunk → inspection → finished product；
Wherein, during the flame-proof treatment, fire retarding treating liquid prescription used are as follows: fire retardant ZR-2 400-500g/L is handed over
Join agent GX-100 3-4g/L, phosphoric acid 20-23g/L, fiber protection agent DH6500 20-26g/L；
During the antibiotic finish, the prescription of antibiotic finishing solution used are as follows: anti-bacteium deodorization finishing agent SCJ-200040-
60g/L, AB resin 15-25g/L.
2. preparation process according to claim 1, which is characterized in that the pre-treatment, process flow are as follows: turn over cloth margin to seam →
Cold pad--batch → kiering bleaching → sizing, cold rolling working solution prescription used in the cold-pad-batch process are as follows: caustic soda 40g/L, dioxygen
Step is banked up in water 8g/L, the clot for including in cold-pad-batch process, and clot stacking time is 12 hours.
3. preparation process according to claim 2, which is characterized in that used kiering drift in the kiering bleaching process
White working solution prescription are as follows: desizing scouring agent AWR 4g/L, chelating agent 2g/L, caustic soda 10g/L, hydrogen peroxide 5g/L, waterglass 5g/L.
4. preparation process according to claim 1, which is characterized in that the dye bottom, process flow are as follows: pad dye bottom dye liquor
→ preliminary drying → drying, must contaminate bottom semi-finished product, and the liquid carrying rate for padding dye bottom dye liquor technique is 60%, and the temperature of the preliminary drying technique is
110 DEG C, the temperature of stoving process is 130 DEG C.
5. preparation process according to claim 1, which is characterized in that the stamp, process flow are as follows: by dye bottom technique
Semi-finished product → stamp → dry → baking → and evaporate → dry, obtain stamp semi-finished product.
6. preparation process according to claim 1, which is characterized in that process flow: the CP flame-proof treatment passes through stamp
Treated, and semi-finished product → padding fire retarding treating liquid → dry → baking → washes → soaping → and wash → dry, described to pad resistance
After firing finishing fluid, liquid carrying rate 60-70%, the baking temperature is 170-180 DEG C, bakes and banks up with earth time 2-3min.
7. preparation process according to claim 1, which is characterized in that process flow: antibiotic finish pads antibiotic finishing solution
→ drying, it is described pad antibiotic finishing solution technique after, liquid carrying rate 63%-67%.
8. preparation process according to claim 7, which is characterized in that in the stoving process, the condition of drying be
It is baked 100-180 seconds under the conditions of 130-140 DEG C of temperature.
9. preparation process described in -8 according to claim 1, which is characterized in that the fabric is C/N blended fabric.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811600397.2A CN109680483A (en) | 2018-12-26 | 2018-12-26 | A kind of washable, antibacterial, the preparation process of inflaming retarding fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811600397.2A CN109680483A (en) | 2018-12-26 | 2018-12-26 | A kind of washable, antibacterial, the preparation process of inflaming retarding fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109680483A true CN109680483A (en) | 2019-04-26 |
Family
ID=66189579
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811600397.2A Pending CN109680483A (en) | 2018-12-26 | 2018-12-26 | A kind of washable, antibacterial, the preparation process of inflaming retarding fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109680483A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111501340A (en) * | 2020-05-29 | 2020-08-07 | 江苏雷鸟伪装纺织新材料有限公司 | Preparation process of flame-retardant antibacterial coating |
| CN115434057A (en) * | 2021-06-02 | 2022-12-06 | 利郎(中国)有限公司 | Dyeing and printing integrated blended fabric |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101381958A (en) * | 2008-11-06 | 2009-03-11 | 浙江美欣达印染集团股份有限公司 | Fire retardant finish material and method for finishing fabric using the material |
| CN103061000A (en) * | 2013-01-16 | 2013-04-24 | 江苏悦达纺织集团有限公司 | Coal mine protective clothing fabric and preparation method thereof |
| CN107254720A (en) * | 2017-07-04 | 2017-10-17 | 北京赛欧兰阻燃纤维有限公司 | A kind of far-infrared anti-biotic organic silazane fire resistance fibre and its production method |
| CN107829298A (en) * | 2017-11-09 | 2018-03-23 | 新乡市新科防护科技有限公司 | A kind of flame-proof antibiotic polyester cotton blending fabric and preparation method thereof |
-
2018
- 2018-12-26 CN CN201811600397.2A patent/CN109680483A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101381958A (en) * | 2008-11-06 | 2009-03-11 | 浙江美欣达印染集团股份有限公司 | Fire retardant finish material and method for finishing fabric using the material |
| CN103061000A (en) * | 2013-01-16 | 2013-04-24 | 江苏悦达纺织集团有限公司 | Coal mine protective clothing fabric and preparation method thereof |
| CN107254720A (en) * | 2017-07-04 | 2017-10-17 | 北京赛欧兰阻燃纤维有限公司 | A kind of far-infrared anti-biotic organic silazane fire resistance fibre and its production method |
| CN107829298A (en) * | 2017-11-09 | 2018-03-23 | 新乡市新科防护科技有限公司 | A kind of flame-proof antibiotic polyester cotton blending fabric and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 何丽清 等: ""抗菌防臭整理的方法及SCJ-2000整理剂的应用"", 《化纤与纺织技术》 * |
| 刘玉勇 等: ""异噻唑啉酮类抗菌整理剂的制备及应用"", 《印染助剂》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111501340A (en) * | 2020-05-29 | 2020-08-07 | 江苏雷鸟伪装纺织新材料有限公司 | Preparation process of flame-retardant antibacterial coating |
| CN115434057A (en) * | 2021-06-02 | 2022-12-06 | 利郎(中国)有限公司 | Dyeing and printing integrated blended fabric |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101974857B (en) | Process for preparing polyester fabrics | |
| CN107956141B (en) | Fluorescein dyeing fabric and fire-retardant production technology | |
| CN106544867B (en) | Coloured flame-retardant polyester-cotton fabric and preparation method thereof | |
| CN104611928A (en) | Flame-proof treatment method of pure cotton or cotton blended fabric | |
| CN104727145A (en) | Preparation method and application of cotton environment-friendly flame retardant | |
| CN104233581A (en) | Preparation method of waterproof anti-static flame-retardant blended printed fabric | |
| CN106192423A (en) | A kind of fire-retardant preparation method refusing profit anti-static fabric and electrostatic fabric | |
| CN109853218A (en) | A kind of processing method that lyocell standard type fabric lining promotes washing fastness | |
| CN109680483A (en) | A kind of washable, antibacterial, the preparation process of inflaming retarding fabric | |
| CN106996038A (en) | A kind of production technology of fire-proof function fabric | |
| CN105926312A (en) | Printing and dyeing method for anti-ant antibacterial anti-infrared camouflage fabric and camouflage fabric | |
| CN102337667B (en) | Textile with flame retardancy and water repellency, and production method thereof | |
| CN105839387A (en) | Crease-resistant deformation-preventing finishing process for cotton fabric | |
| CN104452280A (en) | Preparation method of novel flame-retardant antibacterial acrylic fabric | |
| CN106149404A (en) | The dyeing method of a kind of multi-functional anti-infrared fan's fabric and camouflage facing material | |
| CN101613935B (en) | Organic boron antiflaming finishing agent for fabrics and preparation method thereof | |
| CN109371660A (en) | A kind of flame-retardant silk and its preparation method and application | |
| CN107938107A (en) | A kind of nitrile cotton anti-static inflaming-retarding fabric and its manufacture method | |
| CN105113211A (en) | Preparation method and application of efficient flame retardation after-finishing agent | |
| CN105113205A (en) | Flame retardant tidying method for purified cotton or blended cotton textile fabric | |
| CN106012507A (en) | Printing and dyeing method for anti-infrared, waterproof, oilproof and anti-fouling camouflage fabric and camouflage fabric | |
| CN104762724B (en) | Grease proofing polyester-cotton blend fiber crops blend fabric refusing water of a kind of anti-static inflaming-retarding and preparation method thereof | |
| CN106120377A (en) | A kind of anti-infrared moisture absorption is breathed freely the dyeing method of camouflage facing material and camouflage facing material | |
| CN109680489A (en) | A kind of fire retarding treating liquid and flame-proof finishing process for the blended fabric containing Fypro | |
| CN107034669B (en) | Method for crease-resistant finishing of cotton fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190426 |
|
| RJ01 | Rejection of invention patent application after publication |