CN100528134C - 凹凸棒除烟渍牙膏的生产方法 - Google Patents
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Abstract
本发明公开了一种凹凸棒除烟渍牙膏的生产方法，其技术方案的要点是，凹凸棒除烟渍牙膏的生产方法是配料、低速搅拌、研磨、高速搅拌、真空脱气、罐装为凹凸棒除烟渍牙膏的成品。凹凸棒除烟渍牙膏由膏状凹凸棒石粘土、十二烷基硫酸钠、单氟磷酸钠、柠檬酸锌、水杨酸甲酯、山梨酸钾、薄荷油和去离子水组成。凹凸棒除烟渍牙膏能直接吸附和清除口腔中的多种异臭味，增强和再生牙齿表面的珐琅质，提高牙齿抗酸能力，能预防和阻止牙结石的形成，抑制烟斑、茶斑等色素在牙齿表面的粘附，清除沉积于牙齿表面的烟锈、污渍、斑釉等色斑。本发明适用于生产凹凸棒除烟渍牙膏、中草药牙膏和其它药物牙膏。
Description
技术领域：
本发明涉及牙膏，具体涉及一种凹凸棒除烟渍牙膏的生产方法。
背景技术：
牙齿上烟渍、茶渍、咖啡渍等牙渍，由于影响“启齿”的美观而令人烦恼，这些牙渍的形成原因，是由于人的口腔环境是酸性，长期与口腔内的食物残渣发生化学反应形成牙渍。
处理牙齿上烟渍、茶渍、咖啡渍等牙渍，也有选用洗牙+抛光+喷砂的方法，虽然能取得较好的美观、清洁效果，但是费用较高。
除烟渍牙膏常用的摩擦剂有碳酸钙、二水合磷酸氢钙、无水合磷酸氢钙、焦磷酸钙、无水二氧化硅、氢氧化铝等，由于这些摩擦剂硬度高，颗粒粗糙，没有黏性，吸附性能差，长期使用易对牙齿表面的珐琅质造成磨损。
发明内容：
本发明的目的是克服现有技术中不足之处，提供一种凹凸棒除烟渍牙膏的生产方法。
凹凸棒除烟渍牙膏的生产方法是：配料、低速搅拌、研磨、高速搅拌、真空脱气、罐装为凹凸棒除烟渍牙膏的成品。
凹凸棒除烟渍牙膏由膏状凹凸棒石粘土、十二烷基硫酸钠、单氟磷酸钠、柠檬酸锌、水杨酸甲酯、山梨酸钾、薄荷油和去离子水组成。
凹凸棒石粘土是一种含水富镁纳米级多孔纤维状硅酸盐粘土矿物，当凹凸棒石粘土中的凹凸棒含量≥80％以上时，其比表面积较大，可达500m2/g以上，大部分的阳离子、水分子和一定大小的有机分子均可直接被吸附进孔道中，其吸水性可达150％以上；使用凹凸棒矿造浆生产工艺，将凹凸棒石粘土中的水云母、石英、蛋白石和碳酸盐等矿物筛选去除掉，得到一种膏状凹凸棒石粘土，具有超细微粒、摩擦硬度小、无砂粒感和柔软细腻无异味的特点；膏状凹凸棒石粘土经过高速强力搅拌，成为一种触变性和胶黏性特好的天然凝胶体，粘度高达10000mPa·s以上，吸附性能和保湿性能都得到了进一步的提高，高速搅拌后的凹凸棒石粘土，具有摩擦剂、胶黏剂和保湿剂的共有特性。
单氟磷酸钠突出优点是易溶于水，稳定性好，防龋齿效果显著，毒性小，没有副作用，没有锈蚀作用，其化合物稳定，兼容性好，有显著杀菌作用。牙膏中的氟离子被牙齿表面吸收后，能增强和再生牙齿表面的珐琅质，以修补因每天咀嚼食物而磨损的牙齿表面，提高牙齿抗酸能力。
柠檬酸锌能在刷牙后滞留在牙龈沟中，然后在唾液中缓慢溶解，逐步释放出锌离子，以阻止牙结石的形成，抑制烟斑、茶斑等色素在牙齿表面的粘附。
水杨酸甲酯有特殊香气，味甜而辣，微溶于水，有极强的渗透性，能有效的清除沉积于牙齿表面的烟锈、污渍、斑釉等色斑。
十二烷基硫酸钠属阴离子表面活性剂，易溶于水，与阴离子、非离子复配伍性好，具有良好的乳化、发泡、渗透、去污和分散性能，发泡力强。
山梨酸钾能有效地抑制霉菌，酵母菌和好氧性细菌的活性，还能防止肉毒杆菌、葡萄球菌、沙门氏菌等有害微生物的生长和繁殖，其抑止发育的作用比杀菌作用更强，从而达到有效地延长牙膏的保存时间，并保持牙膏的风味。其防腐效果是同类产品苯甲酸钠的5-10倍。
薄荷油具有纯馥的薄荷香气，辛辣而清凉爽口，有强烈的窜透性，具有防腐消炎止痛的作用。
本发明通过下述技术方案予以实现：
凹凸棒除烟渍牙膏的生产方法，其特征在于，①将凹凸棒除烟渍牙膏的配料加入搅拌机内进行低速搅拌混合，搅拌机的速度控制在500～800转/分钟，搅拌时间控制在5～15分钟，低速搅拌的目的是可以使各种配料搅拌均匀；②将步骤①获得的混合物输入多功能胶体磨中进行研磨为糊状混合物，颗粒细度小于0.025毫米，多功能胶体磨的速度控制在2900转/分钟；多功能胶体磨具有湿式处理流体超微粒粉碎、研磨、乳化、分散、均质、搅拌、混合等功能，可代替并优于石磨，砂磨机、球磨机、乳匀机、剪切分散泵，均质乳化机、三辊机、组织捣碎机等工作效率；③将步骤②获得的研磨后的糊状混合物，输入超高速搅拌机中进行高速强力搅拌为膏状半成品，超高速搅拌机的速度控制在4000～11000转/分钟，高速搅拌时间控制在5～30分钟；超高速搅拌机具有独特的叶片设计和无级调速装置，可依生产工艺要求选择最适合的速度，研磨后的糊状混合物经过超高速搅拌后，粘度高达10000mPa·s以上；④将步骤③获得的膏状半成品进行真空脱气工艺处理，罐装为凹凸棒除烟渍牙膏的成品。
所述凹凸棒除烟渍牙膏的配料，按重量百分比由下列组分组成：膏状凹凸棒石粘土42～60％、十二烷基硫酸钠0.2～2.5％、单氟磷酸钠0.05～1.0％、柠檬酸锌0.05～1.0％、水杨酸甲酯0.05～0.5％、山梨酸钾0.05～0.5％、薄荷油0.05～0.5％和去离子水35～55％。
所述膏状凹凸棒石粘土的生产工艺：将凹凸棒矿输入搅拌机内搅拌，经挤出机挤压成片状后，再次输入搅拌机内搅拌，经挤出机挤压成片状后自然晾晒，晾干的凹凸棒矿输送到原料池中浸泡，用气泵冲翻，沉淀后放出浸泡水，筛去杂质，输入半成品池中，重新加水浸泡，用气泵冲翻，沉淀后放出浸泡水，并将沉淀后的泥浆输送到成品池内，即为膏状凹凸棒石粘土。
本生产工艺是采用由本发明人于2004年1月6日申请的“凹凸棒矿造浆生产工艺”，中国专利授权公告号为：CN1287965C，授权公告日：2006年12月6日。
所述膏状凹凸棒石粘土按重量百分比由下列组分组成：凹凸棒石粘土15～35％，水65～85％。
凹凸棒石粘土是含水富镁纳米级纤维状硅酸盐粘土矿物，不需要另外添加摩擦剂、胶黏剂和保湿剂，不但能提高牙膏的质量，还能大大降低生产成本。
凹凸棒除烟渍牙膏膏体洁净、柔软细腻、发泡力强、清凉爽口、稳定性好；膏体不溢出管口，不分离出水，香味色泽正常，玻片无划痕。
凹凸棒除烟渍牙膏能直接吸附和清除口腔中的多种异臭味，增强和再生牙齿表面的珐琅质，提高牙齿抗酸能力，能预防和阻止牙结石的形成，抑制烟斑、茶斑等色素在牙齿表面的粘附，清除沉积于牙齿表面的烟锈、污渍、斑釉等色斑。
本发明适用于生产凹凸棒除烟渍牙膏、中草药牙膏和其它药物牙膏。
具体实施方式：
下面结合实施例对本发明作进一步的描述：
凹凸棒除烟渍牙膏的生产方法，其特征在于，①将凹凸棒除烟渍牙膏的配料加入搅拌机内进行低速搅拌混合，搅拌机的速度控制在600转/分钟，搅拌时间控制在8分钟；②将步骤①获得的混合物输入多功能胶体磨中进行研磨为糊状混合物，颗粒细度小于0.015毫米，多功能胶体磨的速度控制在2900转/分钟；③将步骤②获得的研磨后的糊状混合物，输入超高速搅拌机中进行高速强力搅拌为膏状半成品，超高速搅拌机的速度控制在5000转/分钟，高速搅拌时间控制在20分钟；④将步骤③获得的膏状半成品进行真空脱气工艺处理，罐装为凹凸棒除烟渍牙膏的成品。
所述凹凸棒除烟渍牙膏的配料，按重量百分比由下列组分组成：膏状凹凸棒石粘土55.0％、十二烷基硫酸钠1.5％、单氟磷酸钠0.75％、柠檬酸锌0.25％、水杨酸甲酯0.2％、山梨酸钾0.2％、薄荷油0.1％和去离子水42.0％；
所述膏状凹凸棒石粘土的生产工艺：将凹凸棒矿输入搅拌机内搅拌，经挤出机挤压成片状后，再次输入搅拌机内搅拌，经挤出机挤压成片状后自然晾晒，晾干的凹凸棒矿输送到原料池中浸泡，用气泵冲翻，沉淀后放出浸泡水，筛去杂质，输入半成品池中，重新加水浸泡，用气泵冲翻，沉淀后放出浸泡水，并将沉淀后的泥浆输送到成品池内，即为膏状凹凸棒石粘土。
所述膏状凹凸棒石粘土按重量百分比由下列组分组成：凹凸棒石粘土30％，水70％。
主要理化指标检测结果
Claims (1)
1、一种凹凸棒除烟渍牙膏的生产方法，其特征在于，①将凹凸棒除烟渍牙膏的配料加入搅拌机内进行低速搅拌混合，搅拌机的速度控制在500～800转/分钟，搅拌时间控制在5～15分钟；②将步骤①获得的混合物输入多功能胶体磨中进行研磨为糊状混合物，颗粒细度小于0.025毫米，多功能胶体磨的速度控制在2900转/分钟；③将步骤②获得的研磨后的糊状混合物，输入超高速搅拌机中进行高速强力搅拌为膏状半成品，超高速搅拌机的速度控制在4000～11000转/分钟，高速搅拌时间控制在5～30分钟；④将步骤③获得的膏状半成品进行真空脱气工艺处理，罐装为凹凸棒除烟渍牙膏的成品；
所述凹凸棒除烟渍牙膏的配料，按重量百分比由下列组分组成：膏状凹凸棒石粘土42～60％、十二烷基硫酸钠0.2～2.5％、单氟磷酸钠0.05～1.0％、柠檬酸锌0.05～1.0％、水杨酸甲酯0.05～0.5％、山梨酸钾0.05～0.5％、薄荷油0.05～0.5％和去离子水35～55％；
所述膏状凹凸棒石粘土的生产工艺：将凹凸棒矿输入搅拌机内搅拌，经挤出机挤压成片状后，再次输入搅拌机内搅拌，经挤出机挤压成片状后自然晾晒，晾干的凹凸棒矿输送到原料池中浸泡，用气泵冲翻，沉淀后放出浸泡水，筛去杂质，输入半成品池中，重新加水浸泡，用气泵冲翻，沉淀后放出浸泡水，并将沉淀后的泥浆输送到成品池内，即为膏状凹凸棒石粘土；
所述膏状凹凸棒石粘土按重量百分比由下列组分组成：凹凸棒石粘土15～35％，水65～85％。
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