CN100490650C - Power for preventing and killing crawl pest - Google Patents
Power for preventing and killing crawl pest Download PDFInfo
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- CN100490650C CN100490650C CNB2006100583316A CN200610058331A CN100490650C CN 100490650 C CN100490650 C CN 100490650C CN B2006100583316 A CNB2006100583316 A CN B2006100583316A CN 200610058331 A CN200610058331 A CN 200610058331A CN 100490650 C CN100490650 C CN 100490650C
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- crawl
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- pest
- power
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Abstract
The subject of the invention is to provide a powder for notable preventing and killing crawl pests as follows, which is prepared by adding cyfluthrin as a dimethrin kind of components for preventing and killing crawl pests into mineral substance carriers. The invention provides the powder for notable preventing and killing crawl pests to solve the problems. The powder for notable preventing and killing crawl pests is characterized in that: the mineral substance carriers contains cyfluthrin as components for preventing and killing crawl pests with a total amounts of 0.1 to 0.5 wt.%, ground cinnamon as lustrating components for crawl pests with total amounts of 0.05 to 1.0 wt.%, and dipropylene glycol and/or tripropylene glycol with total amounts of 1.0 to 9.0 wt.% relative to the total amounts of the powder.
Description
Technical field
The present invention relates to a kind of insect-pest exterminating pulvis, specifically, relate to the improvement of the preventive effect of cyfloxylate pulvis.
Background technology
All the time, in mineral carrier, cooperate the pulvis of pyrethroid insecticidal constituent, be widely used in indoor, outdoor insect-pest exterminating.Pulvis is easy-to-use formulation, and on the other hand, the pyrethroid insecticidal constituent decomposes because of the surface-active of mineral carrier easily, so the stabilisation of preparation is the problem that often needs research.For example, open in the clear 63-290803 communique the spy, disclose that " a kind of stable agricultural chemicals solid pharmaceutical preparation; it is combined with at least a compound with polyoxyethylene groups in following solid pharmaceutical preparation, described solid pharmaceutical preparation are to contain the benzyl ester class synthetic pyrethroid that has cyano group in the α position and organophosphorus ester compound to be supported on the mineral carrier as active ingredient and with them and to form.
In addition, known is the exterminator of active ingredient with the essential oil that is extracted by natural frond a lot.Wherein, about at the expellent of ant class as the insect that creeps, open the spy and to disclose the technology of utilizing the cinnamon oil in these plant corpus essential oils in the flat 8-119819 communique, open the technology that discloses the expellent that relates to the ant class that is combined with cinnamon leaves oil and cockroach class in the flat 10-130114 communique the spy.Open flat 6-286104 communique and put down in writing such cinnamic acid though be contained in the principal component of these cinnamon spirit oils and be the spy, the general deficient in stability of aldehyde compound, oxidation easily, and chemical constitution is changed, also lose its chemical property.Therefore, the expeling composition that contains with aldehydes is the exterminator of the plants essential oil of principal component, even be dispersed in the place of indoor, outdoor generation insect, also be subjected to the influence of light, airborne oxygen and oxidation and sex change easily owing to drive away composition, effect, its continuation that can not say so as expellent are can gratifying exterminator.These derived essential oils are methods of utilizing steam distillation and solvent extraction etc., the artificially is by the material that extracts in the bark of plant corpus, leaf, seed, root etc., in these leaching process, the aldehydes composition, the sex change because its part amount is oxidized, so be contained in the expeling composition of this plant corpus, as the active ingredient of exterminator, existence can not be effectively and the problem that is utilized efficiently.
[patent documentation 1] spy opens clear 63-290803 communique
[patent documentation 2] spy opens flat 8-119819 communique
[patent documentation 3] spy opens flat 10-130114 communique
Summary of the invention
The object of the present invention is to provide a kind of technology that significantly improves the preventive effect of following power for preventing and killing crawl pest, described power for preventing and killing crawl pest is combined with the cyfloxylate as the pyrethroid insecticidal constituent in mineral carrier.
Present inventors are in order to solve above-mentioned problem, based on being coupled to the insect pest control agent of creeping that forms in the mineral carrier together as the cyfloxylate of pyrethroid insecticidal constituent with by the pest repelling composition of creeping that plant corpus modulates, the method that improves its preventive effect various researchs have been carried out, found that, as the pest repelling composition of creeping that modulates by plant corpus, what preferably adopt is not the essential oil of this plant corpus, but the plant bark powder that the bark of this plant corpus is ground into itself, especially preferably adopt ground cinnamon, and with these two kinds of components matching in this mineral carrier the time, as solvent, when using dipropylene glycol and/or tripropylene glycol, each effect of above-mentioned two kinds of compositions produces synergy, and the preventive effect of this pulvis significantly improves, thereby has finished the present invention.
That is, the present invention adopts following such formation.
(1) a kind of power for preventing and killing crawl pest, it is characterized in that, be will be as the cyfloxylate of pyrethroid insecticidal constituent, as the reply that modulates by plant corpus creep insect the expeling composition ground cinnamon and, dipropylene glycol and/or tripropylene glycol are coupled in the mineral carrier and form.
(2) as above-mentioned (1) described power for preventing and killing crawl pest, it is characterized in that, be combined with respect to the pulvis total amount be 0.1～0.5 weight % cyfloxylate, be the ground cinnamon of 0.05～1.0 weight %, be dipropylene glycol and/or the tripropylene glycol of 1.0～9.0 weight % with respect to the pulvis total amount with respect to the pulvis total amount.
As above-mentioned (1) or (2) described power for preventing and killing crawl pest, it is characterized in that (3) dipropylene glycol and/or tripropylene glycol are tripropylene glycol.
As each described power for preventing and killing crawl pest of above-mentioned (1)～(3), it is characterized in that (4) insect that creeps is the ant class.
Power for preventing and killing crawl pest of the present invention, be to mix as the cyfloxylate of pyrethroid insecticidal constituent and the mineral carrier that lefts in the amount of cyfloxylate excessively, by merging to cooperate to contain the pyrethroid insecticidal constituent had the more powder of the plant bark of the organic matter of high-affinity, the pyrethroid insecticidal constituent is supported in this plant corpus bark fines effectively, therefore, the surface-active institute of the mineral carrier of initiated oxidation decomposition directly effect reduces, and its stability improves.Accompany therewith, the preventive effect at the insect that creeps of this pulvis, its stability improve.
In addition, in mineral carrier, be combined with under the situation of existing exterminator of plants essential oil, owing to drive away the direct contact mineral matter of composition carrier, so there is easily because of the surface-active of mineral carrier is decomposed, sex change the tendency of dispel effect inactivation; Power for preventing and killing crawl pest of the present invention, not from contain the plant corpus bark of driving away composition, to extract to drive away composition but directly pulverizing, this powder is coupled in the mineral carrier, therefore this expeling composition that is in the state that supports in bark fines is reduced by the surface-active influence degree of mineral carrier, and dispel effect, its stability improve.
The present invention will be coupled to the power for preventing and killing crawl pest that forms in the mineral carrier together as the cyfloxylate of pyrethroid insecticidal constituent with as the creep ground cinnamon of expeling composition of insect of the reply that is modulated by plant corpus, but, when they were cooperated, using dipropylene glycol and/or tripropylene glycol as solvent was constitutive requirements of the present invention.These solvents not only with cyfloxylate, mineral carrier, and also high with the compatibility of ground cinnamon, therefore can be judged, they have the excellent composition of will above-mentioned two kinds preventing and kill off and are distributed to the performance of mineral powder in all equably.In addition, new discovery, these solvents not only have the surface-active that suppresses mineral carrier, prevent the decomposition of cyfloxylate, ground cinnamon, the effect of sex change, and cause the effective synergy of cyfloxylate and ground cinnamon.
By the present invention, in mineral carrier, cooperate the power for preventing and killing crawl pest that forms as the cyfloxylate of pyrethroid insecticidal constituent, can significantly improve effect of pest control, so its practicality is very high.
Embodiment
As the pyrethroid insecticides that uses among the present invention, can list, cyfloxylate, phenothrin, cyphenothrin, permethrin, cypermethrin, fenpropathrin etc., but from the creep aspect of preventive effect of insect of reply, adopt cyfloxylate.Cyfloxylate is suitably for 0.01～1.0 weight % with respect to the use level of pulvis total amount, if consider preventive effect, economy, then is preferably 0.1～0.5 weight %.If use level is less than 0.1 weight %, then preventive effect is poor, in addition, even cooperate greater than 0.5 weight %, can not obtain higher effect, may cause waste economically.
As the creep expeling composition of insect of the reply of using among the present invention that modulates by plant corpus, can list the expeling composition that in cypress, cassia bark, chinaberry, Chinese cassia tree, eucalyptus, bergamot etc., contains.In the present invention, not that composition is driven away in form distillation or the extraction with essential oil from these plant corpuss, but peel off the bark of this plant corpus, use the powder of pulverizing.If using the dried powder of cassia bark, Chinese cassia tree is ground cinnamon, then can bring into play simultaneously as the effect of the cyfloxylate of pyrethroid insecticidal constituent with as the effect of the cinnamic acid of the expeling composition that contains in the ground cinnamon, therefore preferred.Contain 1～3% essential oil in cassia bark, this essential oil contains 80～90% cinnamic acid.In addition, in Ceylon cinnamon, contain 1～2% essential oil, this essential oil contains 40～70% cinnamic acid.
Ground cinnamon is suitably for 0.01～3.0 weight % with respect to the use level of pulvis total amount, if consider preventive effect, economy, then is preferably 0.05～1.0 weight %.If less than 0.05 weight %, then preventive effect is poor, cooperate even surpass 1.0 weight %, the tendency that can not expect further to improve preventive effect is also arranged.
Of the present invention is constitutive requirements to cooperate dipropylene glycol and/or tripropylene glycol further.Difference still with respect to the pulvis total amount, is generally about 0.5～10.0 weight % its use level along with the difference of the kind of the carrier that uses, brand etc., is preferably 1.0～9.0 weight %.Dipropylene glycol and/or tripropylene glycol are strong to the dissolving power of cyfloxylate, ground cinnamon, as solvent is preferred, and owing to have the creep effect of preventive effect of insect of the reply that improves these two kinds of compositions synergistically, so be effective especially in the present invention.
As the mineral carrier of using among the present invention, can list, kaolin, clay, talcum, bentonite, zeolite, Zeeklite (ジ-Network ラ イ ト), Carprex etc., in general, the kaolin, talcum, the clay that do not contain arsenic are suitable for pulvis of the present invention.In addition, as required, can also cooperate various surfactants, dispersant, for example the stabilizing agent of the fluidity amendment of PAP etc., insecticidal constituent, cosolvent etc.
In power for preventing and killing crawl pest of the present invention, and then, also can obtain the more excellent pulvis of effect by adding other insecticides, miticide, bactericide, insect pheromone, having insect pheromone composition, insect information exchange upset agent, other active components of activity like that.
The power for preventing and killing crawl pest of the present invention of Huo Deing can be filled in any material, shapes of containers, the bag like this, carry out goodsization.At indoor or outdoors, at common every 1m
2During loose powder 1～100g,, can bring into play preventive effect to the insect various beastly that sanitary insect pest, armadillidum vulgare, damp worm, centipede, the perfume (or spice) of cockroach, acarid, bedbug etc. prolongs worm, caterpillar, common house centipede dragonfly, ant, death watch beetle etc.Wherein, the preventive effect excellence of reply ant class, therefore preferred reply ant class.Specifically can list Japanese mountain ant (Formica japonica), crosspointer ant, Japan hair ant (Lasius japonicus), plain tube coloured glaze ant, Japanese hunchbacked ant (Camponotus japonicus), monomorium pharaonis (Monomorium pharaonis) etc., but so long as the ant class, just there is no particular limitation.
Below, based on specific embodiment, illustrate in greater detail power for preventing and killing crawl pest of the present invention.
[embodiment 1]
The cyfloxylate of 0.4 weight portion fully is dissolved in the tripropylene glycol of 3.0 weight portions and forms solution, in this solution, mix the ground cinnamon of 0.2 weight portion, then, further add the kaolin of 96.4 weight portions, pulverize mixing with blender, obtain insect-pest exterminating pulvis of the present invention.This pulvis of 10.0g is mixed in the commercially available river sand of 755.0g, fully stirs, then its 75.5g is evenly spread in the petri diss of nitre system.Spreading have sand middle position part, the resinous tube of internal diameter 8cm, high 7cm is set, in this, put into 20 Japanese mountain ants of arresting from the field.After 10 minutes, the inside of the tube that observation post is provided with, result Japan mountain ant is all escaped, and confirms that insect-pest exterminating of the present invention has very high preventive effect with pulvis.
[embodiment 2]
Based on embodiment 1, the various power for preventing and killing crawl pest shown in the modulomenter 1 carry out the preventive effect test.Its result is suitable for table 1 in the lump.TPG in the table represents the tripropylene glycol as the solvent use.In addition, DPG represents dipropylene glycol equally.In tube, put into the individuality of 20 Japanese mountain ants, in the inspection section, come the result of evaluation effect test with following benchmark after 10 minutes.
++: the individual all escapes in the tube.
+: 5～10 individuality is paced up and down in tube.
-: the individuality that is placed in the tube is all paced up and down in tube.
[table 1]
TPG: tripropylene glycol
DPG: dipropylene glycol
The result of test can distinguish, by the present invention, will be coupled to as the cyfloxylate of pyrethroid insecticidal constituent in the mineral carrier and the power for preventing and killing crawl pest that forms, can significantly improve preventive effect.Even it is such shown in the comparative example 1 and 2 of table 1, in the cyfloxylate pulvis that with the mineral matter is carrier, the plants essential oil that adds as existing exterminator composition is a cinnamon essential oil in the lump, can not expect effective effect of pest control, if but add Chinese cassia tree plant bark powder is ground cinnamon rather than cinnamon essential oil, then can confirm the tendency that preventive effect improves.And then, if with the present invention 2 and 4 and comparative example 1 compare, then when being coupled in mineral carrier with ground cinnamon above-mentioned cyfloxylate,, can distinguish that then preventive effect improves with multiplying each other if merge dipropylene glycol, the tripropylene glycol that cooperates as solvent.In addition, shown in the present invention 2 and 4, like that, adopt a side of the tripropylene glycol in these two kinds of solvents to have the tendency that preventive effect further improves.In addition, according to the present invention 1, as the mineral carrier of using among the present invention, except kaolin, also can be talcum, if with the present invention 2 and 4 and comparative example 3 compare, then as can be known, adopting is not under the situation of dipropylene glycol as solvent of inscape of the present invention, can not expect the raising of satisfied preventive effect.
The industry utilizability
The present invention, by with the weight ratio in the certain limit, with pyrethroid insecticides with contain The plant bark powder of pest repelling composition of creeping is coupled to that to form the insect that creeps in the mineral carrier anti-Except using pulvis, in this power for preventing and killing crawl pest further with the weight ratio in the certain limit, close And cooperate specific solvent, and can significantly improve the effect of pest control of above-mentioned two kinds of compositions, also can Expectation is applied to the insecticidal constituent beyond the pyrethroid.
Claims (3)
1. power for preventing and killing crawl pest, it is characterized in that, be will be as the cyfloxylate of pyrethroid insecticidal constituent, as the creep ground cinnamon of expeling composition of insect of the reply that modulates by plant corpus, be coupled to dipropylene glycol and/or tripropylene glycol and form in the mineral carrier, be combined with respect to the pulvis total amount be 0.1～0.5 weight % cyfloxylate, be the ground cinnamon of 0.05～1.0 weight %, be dipropylene glycol and/or the tripropylene glycol of 1.0～9.0 weight % with respect to the pulvis total amount with respect to the pulvis total amount.
2. power for preventing and killing crawl pest as claimed in claim 1 is characterized in that, dipropylene glycol and/or tripropylene glycol are tripropylene glycol.
3. power for preventing and killing crawl pest as claimed in claim 1 or 2 is characterized in that, the insect that creeps is the ant class.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2005308616A JP4813870B2 (en) | 2005-10-24 | 2005-10-24 | 粉 Pest control powder |
| JP308616/2005 | 2005-10-24 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1954673A CN1954673A (en) | 2007-05-02 |
| CN100490650C true CN100490650C (en) | 2009-05-27 |
Family
ID=38062376
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100583316A Active CN100490650C (en) | 2005-10-24 | 2006-03-03 | Power for preventing and killing crawl pest |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP4813870B2 (en) |
| CN (1) | CN100490650C (en) |
| HK (1) | HK1099176A1 (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009084580A1 (en) * | 2007-12-28 | 2009-07-09 | Dainihon Jochugiku Co., Ltd. | Repellent for grape pest, and method for repelling grape pest |
| CN101589729B (en) * | 2009-07-03 | 2013-06-12 | 中国热带农业科学院环境与植物保护研究所 | Cinnamomum zeylanicum extract and use thereof in acaricide |
| CN102742592B (en) * | 2011-04-18 | 2014-12-10 | 大日本除虫菊株式会社 | Powder used for creeper pest control |
| JP5749101B2 (en) * | 2011-04-18 | 2015-07-15 | 大日本除蟲菊株式会社 | 粉 Pest control powder |
| CN102979190B (en) * | 2012-12-21 | 2015-05-20 | 上海蒂锦特环保技术服务有限公司 | Insect attack isolation control method for building |
| JP5989915B2 (en) * | 2013-09-20 | 2016-09-07 | 大日本除蟲菊株式会社 | 粉 Pest control powder |
| CN104920511A (en) * | 2015-05-08 | 2015-09-23 | 吴持跃 | Ant repellent, and preparation method and application thereof |
| CN105613488A (en) * | 2015-12-30 | 2016-06-01 | 湖南华望熏蒸消毒有限公司 | Pesticide powder, preparation method and control method of tobacco pests |
| CN106259530A (en) * | 2016-08-03 | 2017-01-04 | 北海市白蚁防治管理所 | Traditional-Chinese-medicine-type red fire ant poison bait and preparation method thereof |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01132505A (en) * | 1987-11-17 | 1989-05-25 | Mikasa Kagaku Kogyo Kk | Insect pest expellent |
| JPH037554A (en) * | 1989-06-05 | 1991-01-14 | House Food Ind Co Ltd | Method for repelling vermin of guinea pepper |
| JP3556981B2 (en) * | 1994-10-27 | 2004-08-25 | フマキラー株式会社 | Ant repellent |
| JP3848412B2 (en) * | 1996-10-31 | 2006-11-22 | フマキラー株式会社 | Ant repellent |
| JP4424944B2 (en) * | 2003-09-01 | 2010-03-03 | 大日本除蟲菊株式会社 | Stable pest control powder |
-
2005
- 2005-10-24 JP JP2005308616A patent/JP4813870B2/en active Active
-
2006
- 2006-03-03 CN CNB2006100583316A patent/CN100490650C/en active Active
-
2007
- 2007-06-18 HK HK07106519.2A patent/HK1099176A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JP2007112773A (en) | 2007-05-10 |
| CN1954673A (en) | 2007-05-02 |
| JP4813870B2 (en) | 2011-11-09 |
| HK1099176A1 (en) | 2007-08-10 |
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